scholarly journals Resistance to compression and microstructure of concrete manufactured with supersulfated cements-based materials of volcanic origin exposed to a sulphate environment

2018 ◽  
Vol 9 (1) ◽  
pp. 106-116
Author(s):  
Erick Edgar Maldonado Bandala ◽  
Karina Cabrera Luna ◽  
José Ivan Escalante García ◽  
Demetrio Nieves Mendoza

This research presents the results of concretes made with supersulfated cements (SSC) volcanic material bases. The concretes were cured under two regimes one for 24 h at 25 ° C and one for 22 h at 60 ° C and then at 25 ° C. The specimens were exposed to two conditions, dry under laboratory conditions and immersed in a solution with 3.5% CaSO 4 at 25 ° C for up to 180 days. After 180 days, the concrete with a 5% An-10% PC-10% CaO-75% PM cementant exposed to the CaSO4 solution achieved a compressive strength of 46 MPa and 44 MPa dry under conditions of laboratory. The microstructure was analyzed by scanning electron microscopy, energy dispersive spectroscopy and XRD, showing that the main hydration products are C-S-H and ettringite.

2010 ◽  
Vol 8 (1) ◽  
pp. 753
Author(s):  
Muhammad Muhammad

Implantasi ion dapat meningkatkan sifat mekanik seperti kekerasan bahan yang akan digunakan untuk komponen dan peralatan proses manufaktur. Implantasi ion dipengaruhi oleh jenis ion dopan, waktu dan energi yang digunakan. Penelitian ini dilakukan untuk mengetahui pengaruh energi dan waktu implantasi ion titanium nitrida terhadap kekerasan dan struktur mikro pada baja VCL 140. Implantasi dilakukan pada arus berkas tetap 10 yA. Variasi waktu 60, 70, 80, 90, 100, 110, 120 menit, energi 75 keV dan variasi energi 15, 30, 45, 60, 75, 90 dan 100 keV dengan waktu implantasi 100 menit dilakukan untuk mendapatkan kekerasan optimum. Uji Kekerasan menggunakan metode Vickers dengan beban 10 gram dan waktu 10 detik. Topografi dari lapisan TIN diamati menggunakan scanning electron microscopy (SEM) dan komposisi kimia dari lapisan TIN dianalisa menggunakan energy dispersive spectroscopy (EDS).Kata kunci : Implantasi ion, VCL 140, kekerasan


2011 ◽  
Vol 17 (S2) ◽  
pp. 250-251
Author(s):  
M Pendleton ◽  
B Pendleton ◽  
E Ellis ◽  
G Peterson ◽  
F Chito ◽  
...  

Extended abstract of a paper presented at Microscopy and Microanalysis 2011 in Nashville, Tennessee, USA, August 7–August 11, 2011.


1991 ◽  
Vol 249 ◽  
Author(s):  
Ming Xu ◽  
J. Polonka ◽  
A. I. Goldman ◽  
D. K. Finnemore ◽  
Qiang Li ◽  
...  

ABSTRACTThe melting of Bi2Sr2CaCu2Ox material has been studied by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) in order to study the phases that formed in the high temperature regions. Two distinct phases of (Sr1-xCax)CuO2 and (Sr1-xCax)2CuO3 have been observed in the Bi-rich matrix depending upon quenching temperatures. Crystallization from the melt by fast cooling usually produce the co-existence of Bi (2201) and these Sr-Ca-Cu-O phases.


2011 ◽  
Vol 194-196 ◽  
pp. 1012-1016
Author(s):  
Xin Yu Zhang ◽  
Emmanuel Gallucci ◽  
Karen Scrivener

Alkali aggregate reaction (AAR) is known leading to great damage in concrete, both in compressive strength and in durability. In this study, a backscattered scanning electron microscopy with energy dispersive spectroscopy is adopted to diagnose AAR reaction. The results show that the type of AAR reaction and reaction products can be easily identified and the method is precise and fast.


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