There are several obstacles encountered during combustion in Supersonic Combustion Ramjet (SCRAMJET) engines such as mixing, ignition, and flame holding. In order to overcome these difficulties, a new type of fuel is generated with the use of combination of two methods namely an effervescent (barbotage) and thermal pyrolysis of the fuel. In the first step of the process, during effervescent method, small gas bubbles are introduced into liquid fuel to improve the spraying characteristics of the fuel. At the second stage, long-chain hydrocarbons are broken down into short-chain hydrocarbons that burn faster. An experimental facility has been designed and developed to study the underlying physics in each process.