scholarly journals Influence of Annealing on Zn1-XCuxo (X=6.27%) Thin Films by Sol-gel Method

2015 ◽  
Vol 9 (1) ◽  
pp. 91-94
Author(s):  
Wang Xiaoyang ◽  
Ren Keming ◽  
Zhou Zhen
Keyword(s):  
Annealing Temperature ◽  
Sol Gel ◽  
Visible Region ◽  
Peak Position ◽  
Zno Films ◽  
Light Spectrum ◽  
Gel Method ◽  
Sol Gel Method ◽  
Luminescence Peak ◽  
Photoluminescence Peak

The ZnCuO (x=6.27%) films under different annealing were prepared by the sol-gel method on grass. Using the X-ray diffraction (XRD), atomic force microscopy to study the influence of annealing on the microstructure and surface morphology of the film, the result of which shows that the annealing temperature did not change the wurtzite structure of ZnO and the film density under 400 degree annealing is evened out and is the best one.In the transmission spectra of zinc oxide (ZnO) films, the transmittance in the visible light range changes little with the shift of the annealing temperature, and the absorption edge assumes a hypsochromic shift. From the point of light spectrum at room temperature, annealing temperature changes photoluminescence peak position, not significantly changing the luminescence peak position of ZnO film, but make zinc deficiency increased with annealing and the obvious enhancement in the visible region photoluminescence peak.

Effect of annealing temperature on optical properties of Er-doped ZnO films prepared by sol–gel method

2008 ◽  
Vol 148 (1-3) ◽  
pp. 35-39 ◽  
Author(s):  
Fanyong Ran ◽  
Lei Miao ◽  
Sakae Tanemura ◽  
Masaki Tanemura ◽  
Yongge Cao ◽  
...  
Keyword(s):  
Optical Properties ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Zno Films ◽  
Gel Method ◽  
Sol Gel Method ◽  
Doped Zno ◽  
Er Doped

Influence of Annealing Temperature on Structural and Optical Properties of Undoped and Al-Doped Nano-ZnO Films Prepared by Sol–Gel Method

2016 ◽  
Vol 8 (4) ◽  
pp. 878-883 ◽  
Author(s):  
Vladimir Gevorgyan ◽  
Anna Reymers ◽  
Mikayel Arzakantsyan ◽  
Kilbock Lee ◽  
Jinho Ahn ◽  
...  
Keyword(s):  
Optical Properties ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Zno Films ◽  
Structural And Optical Properties ◽  
Nano Zno ◽  
Gel Method ◽  
Sol Gel Method

Structural, Optical and Electrical Properties of ZnO Films by Sol-Gel Method

2004 ◽  
Vol 449-452 ◽  
pp. 1009-1012 ◽  
Author(s):  
Cheng Zhu Lu ◽  
Jung Yohn Cho ◽  
Ho Jung Chang ◽  
Sang Woo Joo ◽  
Yong Sheng Wang
Keyword(s):  
Electrical Properties ◽  
Oxygen Vacancies ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Zno Films ◽  
Optical And Electrical Properties ◽  
Gel Method ◽  
Sol Gel Method ◽  
Glass Substrates ◽  
Zno Nanocrystal

We synthesized ZnO nanocrystal colloids adopting sol-gel method using zinc acetate dehydrate as precursor, and prepared ZnO films on glass substrates by a spin-coating technique. The effect of annealing temperature on the structure, optical and electrical properties has been studied. The crystallinity and morphologies were improved by the annealing. All film samples show high transmittance of above 80% in the wavelength ranging from 400nm to 1000nm. A minimum resistivity of 5.5x10-3 cm was obtained for the film annealed at 500oC. The crystallinity, oxygen vacancies, and nanocrystalline boundaries seems likely to be crucial factors for these properties

OPTICAL AND ELECTRICAL PROPERTIES OF ZINC OXIDE THIN FILMS DIP-COATED OF SOL–GEL METHOD

2005 ◽  
Vol 12 (05n06) ◽  
pp. 697-701 ◽  
Author(s):  
M. RUSOP ◽  
K. UMA ◽  
T. SOGA ◽  
T. JIMBO
Keyword(s):  
Thin Films ◽  
Electrical Properties ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Film Deposition ◽  
Zno Films ◽  
Optical And Electrical Properties ◽  
Gel Method ◽  
Sol Gel Method ◽  
Higher Temperature

The transparent c-axis oriented ZnO thin films have been prepared by sol–gel method using zinc acetate as cations source, 2-mrthoxiethanol as solvent and monoethanolamine as sol stabilizer. Film deposition was performed by dip coating technique at a withdrawal rate of 10 mm/min on quartz and silicon substrates. The effect of annealing temperature in air ambient from 100 to 800°C on the structural, optical and electrical properties of the films is discussed. ZnO films annealed with higher temperature showed an extremely sharp (002) peak in the XRD patterns, indicates increased crystallization. The optical transmittance spectra of the films is found to change with annealing temperature and showed a very good transmittance (between 80 to 90%) with the films prepared at 600°C showed highest optical transparency within the visible wavelength region. The absorption edge analysis revealed that the optical band gap is found to increase with annealing temperature up to 3.5 eV at 600°C and decreased with higher temperature. Electronic transition was found to be direct transition type. The minimum electrical resistivity of 55 Ω-cm was obtained for the films annealed at 600°C.

Annealing Effects on the Physical and Magnetic Properties of Tb1.5Y1.5Fe5O12 Films Nanoparticles Prepared by Sol-Gel Method

2013 ◽  
Vol 756 ◽  
pp. 91-98 ◽  
Author(s):  
Ftema W. Aldbea ◽  
Noor Bahyah Ibrahim ◽  
Mustafa Hj. Abdullah
Keyword(s):  
Particle Size ◽  
Magnetic Properties ◽  
Annealing Temperature ◽  
Quartz Substrate ◽  
Sol Gel ◽  
Lattice Parameter ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Iron Garnet

Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900 °C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900°C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-raySpectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealingtemperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. Normal 0 21 false false false MS X-NONE X-NONE MicrosoftInternetExplorer4 Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900°C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900 °C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-ray Spectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealing temperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. st1\:*{behavior:url(#ieooui) } /* Style Definitions */ table.MsoNormalTable {mso-style-name:"Table Normal"; mso-tstyle-rowband-size:0; mso-tstyle-colband-size:0; mso-style-noshow:yes; mso-style-priority:99; mso-style-qformat:yes; mso-style-parent:""; mso-padding-alt:0cm 5.4pt 0cm 5.4pt; mso-para-margin:0cm; mso-para-margin-bottom:.0001pt; mso-pagination:widow-orphan; font-size:11.0pt; font-family:"Calibri","sans-serif"; mso-ascii-font-family:Calibri; mso-ascii-theme-font:minor-latin; mso-fareast-font-family:"Times New Roman"; mso-fareast-theme-font:minor-fareast; mso-hansi-font-family:Calibri; mso-hansi-theme-font:minor-latin; mso-bidi-font-family:"Times New Roman"; mso-bidi-theme-font:minor-bidi;}

Effect of annealing temperature on the structural and optical properties of ZnO thin films prepared by sol–gel method

Ionics ◽  
2010 ◽  
Vol 16 (9) ◽  
pp. 815-820 ◽  
Author(s):  
Yidong Zhang ◽  
Wenjun Fa ◽  
Fengling Yang ◽  
Zhi Zheng ◽  
Pingyu Zhang
Keyword(s):  
Thin Films ◽  
Optical Properties ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Zno Thin Films ◽  
Structural And Optical Properties ◽  
Gel Method ◽  
Sol Gel Method
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