scholarly journals Dissolution of the second phase particles in the course of the equal channel angular pressing of diluted Cu‑Cr‑Zr alloy

2018 ◽  
Vol 8 (1) ◽  
pp. 110-114 ◽  
Author(s):  
I. A. Faizov ◽  
R. R. Mulyukov ◽  
D. A. Aksenov ◽  
S. N. Faizova ◽  
N. V. Zemlyakova ◽  
...  
2007 ◽  
Vol 544-545 ◽  
pp. 419-422 ◽  
Author(s):  
Akira Watazu ◽  
Ichinori Shigematsu ◽  
Xin Sheng Huang ◽  
Kazutaka Suzuki ◽  
Naobumi Saito

Noncombustible Mg-8Al-2Ca rods were processed by RD-ECAP. The magnesium alloy rod had Mg matrix and Al2Ca second phase. Grains with about 20 μm in diameter were observed in the matrix of the raw materials. The grains in matrix had no anisotropy. On the other hand, positions of second phase particles had anisotropy and the second phase particles formed lines. The samples processed by RD-ECAP had no crack and the samples had 20mm diameter. Grains in matrix of the 4 pass RD-ECAP sample had no anisotropy and the grains had under about 5 μm in diameter. The second phase particles had round shapes and were uniformly distributed as compared with the raw material rod. Therefore, the RD-ECAP is useful for forming noncombustible Mg-8Al-2Ca alloy with fine-grains.


2012 ◽  
Vol 715-716 ◽  
pp. 346-353
Author(s):  
H. Paul ◽  
T. Baudin ◽  
K. Kudłacz ◽  
A. Morawiec

The objective of this study was to determine the effect of deformation mode on recrystallization behavior of severely deformed material. Commercial purity AA3104 aluminum alloy was deformed via high pressure torsion and equal channel angular pressing to different strains and then annealed to obtain the state of partial recrystallization. The microstructure and the crystallographic texture were analysed using scanning and transmission electron microscopes equipped with orientation measurement facilities. The nucleation of new grains was observed in bulk recrystallized samples and during in-situ recrystallization in the transmission microscope. Irrespective of the applied deformation mode, a large non-deformable second phase particles strongly influenced strengthening of the matrix through deformation zones around them. It is known that relatively high stored energy stimulates the nucleation of new grains during the recrystalization. In most of the observed cases, the growth of recrystallized grains occurred by the coalescence of neighboring subcells. This process usually led to nearly homogeneous equiaxed grains of similar size. The diameter of grains in the vicinity of large second phase particles was only occasionally significantly larger than the average grain size. Large grains were most often observed in places far from the particles. TEM orientation mapping from highly deformed zones around particles showed that orientations of new grains were not random and only strictly defined groups of orientations were observed.


2012 ◽  
Vol 735 ◽  
pp. 295-300
Author(s):  
Elena Avtokratova ◽  
Oleg Sitdikov ◽  
Michael Markushev ◽  
Radik R. Mulyukov

Unique superplastic elongations up to 4100% were achieved at 450°C in the strain rate range of 10-2-10-1s-1for Al-Mg-Sc-Zr alloy with a grain size ~1 μm processed by warm-to-hot equal channel angular pressing. Such a behavior is attributed to the synergy of complementary factors resulted in high homogeneity and stability of ultrafine-grained microstructure and superplastic flow, involving large proportion of high-angle grain boundaries, presence of dispersoids of aluminides of transition metals and negligible amount of coarse excess phases.


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