The effect of second-phase particles on grain refinement during equal-channel angular pressing in an Al–Cu–Mg–Ag alloy

2014 ◽  
Vol 50 (2) ◽  
pp. 990-1005 ◽  
Author(s):  
M. Gazizov ◽  
S. Malopheyev ◽  
R. Kaibyshev
Keyword(s):  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
Second Phase ◽  
Angular Pressing ◽  
Second Phase Particles

scholarly journals Dissolution of the second phase particles in the course of the equal channel angular pressing of diluted Cu‑Cr‑Zr alloy

2018 ◽  
Vol 8 (1) ◽  
pp. 110-114 ◽  
Author(s):  
I. A. Faizov ◽  
R. R. Mulyukov ◽  
D. A. Aksenov ◽  
S. N. Faizova ◽  
N. V. Zemlyakova ◽  
...  
Keyword(s):  
Equal Channel Angular Pressing ◽  
Second Phase ◽  
Angular Pressing ◽  
Second Phase Particles ◽  
Zr Alloy

Noncombustible Magnesium Alloy Processed by Rotary-Die Equal Channel Angular Pressing Method

2007 ◽  
Vol 544-545 ◽  
pp. 419-422 ◽  
Author(s):  
Akira Watazu ◽  
Ichinori Shigematsu ◽  
Xin Sheng Huang ◽  
Kazutaka Suzuki ◽  
Naobumi Saito
Keyword(s):  
Magnesium Alloy ◽  
Equal Channel Angular Pressing ◽  
Raw Materials ◽  
The Other ◽  
Raw Material ◽  
Second Phase ◽  
Pressing Method ◽  
Angular Pressing ◽  
Second Phase Particles ◽  
The Matrix

Noncombustible Mg-8Al-2Ca rods were processed by RD-ECAP. The magnesium alloy rod had Mg matrix and Al2Ca second phase. Grains with about 20 μm in diameter were observed in the matrix of the raw materials. The grains in matrix had no anisotropy. On the other hand, positions of second phase particles had anisotropy and the second phase particles formed lines. The samples processed by RD-ECAP had no crack and the samples had 20mm diameter. Grains in matrix of the 4 pass RD-ECAP sample had no anisotropy and the grains had under about 5 μm in diameter. The second phase particles had round shapes and were uniformly distributed as compared with the raw material rod. Therefore, the RD-ECAP is useful for forming noncombustible Mg-8Al-2Ca alloy with fine-grains.

Recrystallization in Ultra-Fine Grain Structures of AA3104 Alloy Processed by ECAP and HPT

2012 ◽  
Vol 715-716 ◽  
pp. 346-353
Author(s):  
H. Paul ◽  
T. Baudin ◽  
K. Kudłacz ◽  
A. Morawiec
Keyword(s):  
High Pressure Torsion ◽  
Deformation Mode ◽  
Second Phase ◽  
Orientation Measurement ◽  
Angular Pressing ◽  
Second Phase Particles ◽  
Average Grain Size ◽  
The Matrix ◽  
Electron Microscopes ◽  
Different Strains

The objective of this study was to determine the effect of deformation mode on recrystallization behavior of severely deformed material. Commercial purity AA3104 aluminum alloy was deformed via high pressure torsion and equal channel angular pressing to different strains and then annealed to obtain the state of partial recrystallization. The microstructure and the crystallographic texture were analysed using scanning and transmission electron microscopes equipped with orientation measurement facilities. The nucleation of new grains was observed in bulk recrystallized samples and during in-situ recrystallization in the transmission microscope. Irrespective of the applied deformation mode, a large non-deformable second phase particles strongly influenced strengthening of the matrix through deformation zones around them. It is known that relatively high stored energy stimulates the nucleation of new grains during the recrystalization. In most of the observed cases, the growth of recrystallized grains occurred by the coalescence of neighboring subcells. This process usually led to nearly homogeneous equiaxed grains of similar size. The diameter of grains in the vicinity of large second phase particles was only occasionally significantly larger than the average grain size. Large grains were most often observed in places far from the particles. TEM orientation mapping from highly deformed zones around particles showed that orientations of new grains were not random and only strictly defined groups of orientations were observed.

scholarly journals Grain Refinement by Second Phase Particles under Applied Stress in ZK60 Mg Alloy with Y through Phase Field Simulation

Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1903 ◽  
Author(s):  
Yuhao Song ◽  
Mingtao Wang ◽  
Yaping Zong ◽  
Ri He ◽  
Jianfeng Jin
Keyword(s):  
Grain Refinement ◽  
Applied Stress ◽  
Phase Field ◽  
Phase Particle ◽  
Alloy System ◽  
Second Phase ◽  
Recrystallization Process ◽  
Time Space ◽  
Second Phase Particles ◽  
Zk60 Alloy

Based on the principle of grain refinement caused by the second-phase particles, a phase field model was built to describe the recrystallization process in the ZK60 alloy system with Y added under applied stress between temperatures 573 and 673 K for 140 min duration. The simulation of grain growth with second phase particles and applied stress during annealing process on industrial scale on the condition of real time-space was achieved. Quantitative analysis was carried out and some useful laws were revealed in ZK60 alloy system. The second phase particles had a promoting effect on the grain refinement, however the effect weakened significantly when the content exceeded 1.5%. Our simulation results reveal the existence of a critical range of second phase particle size of 0.3–0.4 μm, within which a microstructure of fine grains can be obtained. Applied stress increased the grain coarsening rate significantly when the stress was more than 135 MPa. The critical size of the second phase particles was 0.4–0.75 μm when the applied stress was 135 MPa. Finally, a microstructure with a grain size of 11.8–13.8 μm on average could be obtained when the second phase particles had a content of 1.5% and a size of 0.4–0.75 μm with an applied stress less than 135 Mpa after 30 min annealing at 573 K.

Influence of Stacking Fault Energy on the Microstructures and Grain Refinement in the Cu-Al Alloys during Equal-Channel Angular Pressing

2010 ◽  
Vol 667-669 ◽  
pp. 379-384 ◽  
Author(s):  
X.H. An ◽  
Shi Ding Wu ◽  
Z.F. Zhang
Keyword(s):  
Grain Size ◽  
Grain Refinement ◽  
Equal Channel Angular Pressing ◽  
Al Alloys ◽  
Stacking Fault ◽  
High Recovery ◽  
Angular Pressing ◽  
High Recovery Rate ◽  
Refinement Mechanism ◽  
Stacking Fault Energies

The microstructural evolution and grain refinement of Cu-Al alloys with different stacking fault energies (SFEs) processed by equal-channel angular pressing (ECAP) were investigated. The grain refinement mechanism was gradually transformed from dislocation subdivision to twin fragmentation with tailoring the SFE of Cu-Al alloys. Concurrent with the transition of grain refinement mechanism, the grain size can be refined into from ultrafine region (1 m~100 nm) to the nanoscale (<100 nm) and then it is found that the minimum equilibrium grain size decreases in a roughly linear way with lowering the SFE. Moreover, in combination with the previous results, it is proposed that the formation of a uniform ultrafine microstructure can be formed more readily in the materials with high SFE due to their high recovery rate of dislocations and in the materials with low SFE due to the easy formation of a homogeneously-twinned microstructure.

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