scholarly journals Crucial effect of SiC particles on in situ synthesized mullite whisker reinforced Al2O3-SiC composite during microwave sintering

2017 ◽  
Vol 11 (2) ◽  
pp. 106-112 ◽  
Author(s):  
Xudan Dang ◽  
Meng Wei ◽  
Rui Zhang ◽  
Keke Guan ◽  
Bingbing Fan ◽  
...  
Keyword(s):  
Particle Size ◽  
Flexural Strength ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Hot Spot ◽  
Microwave Sintering ◽  
Sic Particles ◽  
Shock Resistance ◽  
Sic Particle

Mullite whisker reinforced Al2O3-SiC composites were in situ synthesized by microwave sintering at 1500?C for 30min. The influence of SiC particle size on heating process and properties of Al2O3-SiC composite were investigated. The XRD and SEM techniques were carried out to characterize the samples. The thermal shock resistance and flexural strength of the samples were examined through water quenching and three-point bending methods, respectively. It was found that the bridging of mullite whisker appeared between Al2O3 and SiC particles which enhanced the thermal shock resistance. A so-called local hot spot effect was proposed dependent on the coupling of SiC particles with microwave, which was the unique feature of microwave sintering. The maximal thermal shock resistance and flexural strength were obtained for the samples with SiC particle size of ~5?m.

Effect of AlF3 Content on Microstructure and Properties of Mullite/Al2O3 Composite Ceramics

2018 ◽  
Vol 922 ◽  
pp. 62-67
Author(s):  
Ke Zheng Sang ◽  
Fan Wang ◽  
De Jun Zeng ◽  
Hong Wei Li
Keyword(s):  
Fracture Toughness ◽  
Flexural Strength ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Diameter Ratio ◽  
Pressureless Sintering ◽  
Composite Ceramics ◽  
Microstructure And Properties ◽  
Shock Resistance ◽  
Mullite Whiskers

To reinforce the mullite/Al2O3 composite ceramics through formation of mullite whiskers, the composite ceramics were prepared by pressureless sintering using different AlF3 content. The microstructure, porosity, fracture toughness and thermal shock resistance of the composite ceramics were investigated. The results show that the addition of AlF3 can promote the mullite whisker formations, and the whiskers with the size of 3～10μm in diameter and a length-diameter ratio of 10～15 are obtained by sintering at 1600°C with the AlF3 content of 5wt%. Fracture toughness and thermal shock resistance of the composite ceramics are improved by the formation of mullite whisker. The fracture toughness of 4.79MPa•m1/2 can be obtained, and the 95.18% flexural strength remained after thermal shock.

Sic Based Ceramic Foams Reinforced by In Situ Mullite Whisker

2009 ◽  
Vol 79-82 ◽  
pp. 1983-1986 ◽  
Author(s):  
Xiao Li Ji ◽  
Fei Xu ◽  
Hai Ya Chen
Keyword(s):  
Compressive Strength ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Ceramic Foams ◽  
Sic Ceramic ◽  
Influence Of Temperature On ◽  
Shock Resistance ◽  
Mullite Whiskers ◽  
Maximum Compressive Strength

Prepared silicon carbide(SiC) ceramic foams combined with mullite whiskers which synthesized by in-situ reaction. Studied on the influence of temperature on the synthesis of mullite whisker, and the influence of mullite content on the compressive strength, thermal shock resistance of SiC ceramic foams. The results indicate that the performance of mullite whiskers synthesized at 1400°Cwere best, when mullite content was 25%, SiC ceramic foams could reach the maximum compressive strength for 1.75MP, the most thermal shock resistance for14 times.

Preparation and Performance of β-Sialon Bonded ZrO2 Composites

2011 ◽  
Vol 415-417 ◽  
pp. 138-141
Author(s):  
Rui Sheng Wang ◽  
Jun Hong Zhao ◽  
Ying Na Wei ◽  
Fu Hua Peng ◽  
Heng Yong Wei
Keyword(s):  
Thermal Expansion ◽  
Flexural Strength ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Reaction Sintering ◽  
Sintering Process ◽  
Carbon Addition ◽  
Shock Resistance ◽  
And Performance ◽  
Sialon Powder

β-Sialon bonded ZrO2 composites were prepared by reaction sintering process using β-Sialon and CaO stabilized ZrO2 powders as raw materials.The effect of β-Sialon powder additions on the properties of the composites was investigated. The results show that the samples with 10 wt% of β-Sialon addition had the lowest apparent porosity (29.80%) and the highest of flexural strength (68.70MPa). The thermal shock resistance in carbon addition of the composites could be improved by addtion of 5wt% β-Sialon. It may be relative with that the sample had the lowest thermal expansion coefficient in vacuum.

The Influence of Particles Size and Composition Variation of NiCr-CrC(20NiCr) Metal Matrix Composites Coatings Properties on Boiler Tubes Application

2017 ◽  
Vol 889 ◽  
pp. 30-35 ◽  
Author(s):  
Erie Martides ◽  
Budi Prawara ◽  
Husaini Ardy ◽  
Endro Junianto ◽  
Budi Priyono
Keyword(s):  
Particle Size ◽  
Thermal Shock ◽  
Metal Matrix ◽  
Thermal Shock Resistance ◽  
Resistance Testing ◽  
Matrix Composites ◽  
Spray Method ◽  
Hvof Thermal Spray ◽  
Boiler Tubes ◽  
Shock Resistance

Deposition of NiCr-CrC(20NiCr) metal matrix composite (MMCs) coating have been applied on the substrate of boiler tubes material with High Velocity Oxygen Fuel (HVOF) thermal spray method and constant parameter. Variation of particle size and composition on MMCs was conducted to determined the optimum conditions for boiler applications. Microvickers hardness, metallography and thermal shock resistance testing were investigated. The best performance for boiler tubes application is MMC NiCr-CrC(20NiCr) with 270 mesh of NiCr particles size and 60:40 of composition as evidence by the highest of hardness value (410 Hv) and slightly of discoloration after thermal shock resistance with two variation cooling medium. While at MMC NiCr-CrC(20NiCr) with 70:30 variation composition, coating hardness value will decrease in line with the smaller of particle size of NiCr.

Preparation of Mullite-Aluminum Titanate-Cordierite Multiphase Ceramics

2013 ◽  
Vol 750-752 ◽  
pp. 484-487
Author(s):  
Ying Na Zhao ◽  
Gang Chang ◽  
Gang Liu ◽  
Hai Bo Song ◽  
Wen Li Zhang
Keyword(s):  
Composite Materials ◽  
Flexural Strength ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Volume Density ◽  
High Alumina ◽  
Aluminum Titanate ◽  
Sinter Property ◽  
Shock Resistance ◽  
Multiphase Ceramics

Mullite-aluminum titanate-cordierite multiphase ceramics were prepared by high alumina clinker, Aluminum Titanate and Cordierite. The sintering property and thermal shock resistance of composite materials were tested. The experimental results show that the sinter property and themal shock resistance of Mullite-aluminum titanate-cordierite multiphase ceramics are relatively preferably, which the materials composition are 30 wt.% high alumina clinker, 60 wt.% cordierite and 10 wt.% aluminum titanate. The component samples show porosity of 33.17%, volume density 1.9 % and normal temperature flexural strength 20.66 MPa. Thermal residual flexural strength of the samples is still as high as 10.29 Mpa by 5 times thermal residual tests, and there are only little flexural strength lower after three times earthquake test.

Thermal shock resistance and oxidation behavior of in-situ synthesized MgAl 2 O 4 –Si 3 N 4 composites used for solar heat absorber

2016 ◽  
Vol 42 (8) ◽  
pp. 10175-10183 ◽  
Author(s):  
Jianfeng Wu ◽  
Yaxiang Zhang ◽  
Xiaohong Xu ◽  
Tengfei Deng ◽  
Xinbin Lao ◽  
...  
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Oxidation Behavior ◽  
Solar Heat ◽  
Heat Absorber ◽  
Shock Resistance
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