scholarly journals Effect of Ball Milling Parameters on the Refinement of Tungsten Powder

Metals ◽  
2018 ◽  
Vol 8 (4) ◽  
pp. 281 ◽  
Author(s):  
Zaoming Wu ◽  
Yanxia Liang ◽  
Engang Fu ◽  
Jinlong Du ◽  
Peipei Wang ◽  
...  
2010 ◽  
Vol 660-661 ◽  
pp. 329-334 ◽  
Author(s):  
Railson Bolsoni Falcão ◽  
Edgar Djalma Campos Carneiro Dammann ◽  
Cláudio José da Rocha ◽  
Ricardo Mendes Leal Neto

This work reports the efforts to obtain TiFe intermetallic compound by high-energy ball milling of Ti and Fe powder mixtures. This process route has been used to provide a better hydrogen intake in this compound. Milling was carried out in a SPEX mill at different times. Strong adherence of material at the vial walls was seen to be the main problem at milling times higher than 1 hour. Attempts to solve this problem were accomplished by adding different process control agents, like ethanol, stearic acid, low density polyethylene, benzene and cyclohexane at variable quantities and keeping constant other milling parameters like ball to powder ration and balls size. Better results were attained with benzene and cyclohexane, but with partial formation of TiFe compound even after a heat treatment (annealing) of the milled samples.


2018 ◽  
Vol 339 ◽  
pp. 256-263 ◽  
Author(s):  
Z.M. Wu ◽  
Y.X. Liang ◽  
Y. Fan ◽  
P.P. Wang ◽  
J.L. Du ◽  
...  
Keyword(s):  

2013 ◽  
Vol 807-809 ◽  
pp. 2707-2712 ◽  
Author(s):  
Shi Jian Yan ◽  
Xin Wei Zou ◽  
Min Gang Zhang

LaNi5-xwt%Mg hydrogen storage alloys with different Mg content were made from pure La, Mg and Ni metal powder by mechanical alloying, selecting appropriate ball-milling parameters in 0.4MPa hydrogen atmosphere. The characterizations for hydrogen storage alloy show that a multi-phase alloy composed of MgH2, LaH3, Mg2NiH4 and Ni was obtained, the alloy have two hydrogen desorption temperature range, and the alloy with 25wt% Mg content can desorb hydrogen up to 4.02wt%.


2001 ◽  
Vol 377 ◽  
pp. 63-70 ◽  
Author(s):  
S. Ruggeri ◽  
C. Lenain ◽  
L. Roué ◽  
Houshang Alamdari ◽  
Guo Xian Liang ◽  
...  

2012 ◽  
Vol 581-582 ◽  
pp. 616-619
Author(s):  
Lian Ping Chen ◽  
Yuan Hong Gao ◽  
Bai Tao Su

Hydrogen is widely used to prepare tungsten from tungsten oxides. Such a gas is combustible and strict measures must be taken. However, assisted by Mg or Li3N, tungsten can be prepared through the ball milling at room temperature. The reduction of WO3by Al powder is investigated thermodynamically. Simulations on the loss of Gibbs energy of these hypothetic reactions reveal that the reduction of WO3and WO2(OH)2(or H2WO4) is feasible when Al powder is used; and it is more difficult to generate the intermediate tungsten oxides such as WO2, WO2.72and WO2.9. In addition, it is better to prepare tungsten powder in vacuum containers in view of economy.


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