scholarly journals Synthesis and characterization of some new heterocyclic compounds from α, β- unsaturated carbonyl system

2021 ◽  
pp. 56-63
Author(s):  
Muna A. Othman Salem ◽  
Hana A. A. Mageed ◽  
Huda S. Muftah ◽  
Reda F. El- Ezabi ◽  
Fayrouz A. Khaled
Keyword(s):  
Heterocyclic Compounds ◽  
Heterocyclic Ring ◽  
Solvent Free ◽  
Synthesis And Characterization ◽  
One Pot ◽  
Ring Systems ◽  
One Pot Synthesis ◽  
Solvent Free Conditions

An efficient and facile one pot synthesis of 3,4-dihydropyrimidinones (Belinelli compound) from furfural, acetylacetone and urea under solvent free conditions was performed, resulted in promising yield. These compounds reacted with benzaldehyde and furfural to give the corresponding chalcones. Chalcones are used to synthesize several derivatives like pyrazolines isoxazoles and pyrimidines having different heterocyclic ring systems. Keywords: Belinelli compounds; Chalcone; Pyrazolines isoxazoles; Pyrimidines

scholarly journals Tandem Fries Reaction–Conjugate Addition under Microwave Irradiation in Dry Media; One-pot Synthesis of Flavanones

1999 ◽  
Vol 23 (9) ◽  
pp. 574-575
Author(s):  
Firouz Matloubi Moghaddam ◽  
Mohammad Ghaffarzadeh ◽  
Seyed Hossein Abdi-Oskoui
Keyword(s):  
Microwave Irradiation ◽  
Silica Gel ◽  
Conjugate Addition ◽  
Solvent Free ◽  
Naphthalene Derivatives ◽  
One Pot ◽  
Fries Rearrangement ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Fries Reaction

An AICl3–ZnCl2 mixture supported on silica gel is found to be an efficient medium for the Fries rearrangement of acyloxybenzene or naphthalene derivatives in solvent-free conditions under microwave irradiation.

scholarly journals Synthesis of 2,4,6-triarylpyridines Using AlPO4 Under Solvent-free Conditions

2010 ◽  
Vol 2 (2) ◽  
pp. 337-342 ◽  
Author(s):  
P. Rajput ◽  
N. J. P. Subhashini ◽  
Shiva Raj
Keyword(s):  
Heterogeneous Catalyst ◽  
Simple Procedure ◽  
Reaction Times ◽  
Aluminum Phosphate ◽  
Solvent Free ◽  
One Pot ◽  
One Pot Synthesis ◽  
Solvent Free Conditions

A series of 2,4,6-triarylpyridines have been prepared using a variety of aromatic and heteroaromatic aldehydes in the presence of aluminum phosphate (AlPO4) as a heterogeneous catalyst at 120 oC under solvent-free conditions. The present methodology offers several advantages such as excellent yields, simple procedure, shorter reaction times, milder conditions and the catalyst exhibited remarkable reusable activity. Keywords: Aluminum phosphate; 2,4,6-triarylpyridines; One-pot synthesis; Shorter reaction times;  Reusable activity.  © 2010 JSR Publications. ISSN: 2070-0237 (Print); 2070-0245 (Online). All rights reserved. DOI: 10.3329/jsr.v2i2.3859               J. Sci. Res. 2 (2), 337-342 (2010) 

Solvent-free, one-pot synthesis of 2,4,6-triarylpyridines using trichloroisocyanuric acid or N-bromosuccinimide as a novel and neutral catalyst

2011 ◽  
Vol 76 (11) ◽  
pp. 1307-1315 ◽  
Author(s):  
Behrooz Maleki ◽  
Hafezeh Salehabadi ◽  
Zeinalabedin Sepehr ◽  
Mina Kermanian
Keyword(s):  
Ammonium Acetate ◽  
Solvent Free ◽  
One Pot ◽  
Aryl Aldehydes ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Trichloroisocyanuric Acid

A simple and benign protocol has been explored for the preparation of 2,4,6-triarylpyridines by a one-pot reaction between aryl aldehydes, enolizable ketones and ammonium acetate in the presence of N-bromosuccinimide or trichloroisocyanuric acid as green and neutral catalysts. The reactions proceed smoothly at 130 °C under solvent-free conditions to provide 2,4,6-triarylpyridines in good yields.

A Novel L-Proline Catalyzed Biginelli Reaction: One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones under Solvent-Free Conditions

2004 ◽  
Vol 33 (9) ◽  
pp. 1168-1169 ◽  
Author(s):  
J. S. Yadav ◽  
S. Praveen Kumar ◽  
G. Kondaji ◽  
R. Srinivasa Rao ◽  
K. Nagaiah
Keyword(s):  
Biginelli Reaction ◽  
Solvent Free ◽  
One Pot ◽  
One Pot Synthesis ◽  
Solvent Free Conditions

scholarly journals An Efficient One-Pot Synthesis of Tetrahydrobenzo Xanthen-11-one Derivatives Catalyzed by P2O5 under Solvent Free Conditions

2018 ◽  
Vol 30 (4) ◽  
pp. 804-806 ◽  
Author(s):  
Krishna Kanth Garlapati ◽  
Siva Sankar Babu ◽  
N. Srinivasu ◽  
T. Murthy Chavali
Keyword(s):  
Solvent Free ◽  
One Pot ◽  
One Pot Synthesis ◽  
Solvent Free Conditions
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