scholarly journals High-resolution Laboratory Measurements of K-shell X-Ray Line Polarization and Excitation Cross Sections in Helium-like S XV Ions

2021 ◽  
Vol 914 (1) ◽  
pp. 34
Author(s):  
Chintan Shah ◽  
Natalie Hell ◽  
Antonia Hubbard ◽  
Ming Feng Gu ◽  
Michael J. MacDonald ◽  
...  
1981 ◽  
Vol 34 (2) ◽  
pp. 155 ◽  
Author(s):  
HJ Hay ◽  
LF Pender ◽  
PB Treacy

With a high-resolution Si(Li) X-ray detector, characteristic K X rays have been detected with targets of Cr, Fe, Cu, Ge and Se ombarded by 100 MeV Cu ions, equilibrated by passing through carbon. Cross sections for X-ray production, target-to-projectile vacancy-sharing ratios and K, to K, ratios were measured and compared with predictions of molecular-coupling theories. The results show little greement with existing models based on rotational coupling in molecular-orbital states.


2017 ◽  
Vol 890 ◽  
pp. 223-226 ◽  
Author(s):  
Rıdvan Durak ◽  
Ferdi Akman ◽  
Abdulhalik Karabulut

The Ll, Lα and Lβ X-ray production cross sections for Pr, Nd, Sm, Eu, Gd and Tb elements were determined using a reflection geometry. The excitation was performed with a 241Am radioactive annular source and the L X-rays emitted from targets were counted with a high-resolution Si (Li) detector. The experimental values were compared with other available experimental results and theoretical data. An agreement is observed between the measured and other experimental results or theoretical data.


Author(s):  
O. L. Krivanek ◽  
D. Fathy ◽  
S.L. Fortner ◽  
Z. Liliental ◽  
E.A. Lodge ◽  
...  

The ability to resolve 2-3Å structurally and 20-50Å chemically has made high resolution electron microscopy (HREM) and microanalysis the preferred techniques for a number of interface studies. The interfaces are usually examined in thin cross-sections cut normal to a major crystallographic direction along which the structure at the interface appears particularly simple in projection. A large number of such studies have now been carried out in a number of different laboratories, including the studies of semiconductor-oxide, semiconductor-semiconductor, and semiconductor-metal interfaces. An exciting new aspect of the studies is exploring the chemistry at the interface using a high resolution probe-forming instrument and either energy-dispersive X-ray spectroscopy(EDXS) or electron energy loss spectroscopy(EELS), since these studies can usally be performed on the same specimens as used for HREM, and a good correlation between the detailed atomic structure and the chemical composition can be achieved.


2019 ◽  
Vol 21 (43) ◽  
pp. 23808-23817
Author(s):  
V. Lemelin ◽  
A. D. Bass ◽  
P. Cloutier ◽  
L. Sanche

Absolute vibrational cross sections for low energy (1–19 eV) electron scattering from condensed thymidine using high-resolution electron energy loss spectroscopy.


2020 ◽  
Vol 641 ◽  
pp. A93
Author(s):  
Liyi Gu ◽  
Chintan Shah ◽  
Junjie Mao ◽  
Ton Raassen ◽  
Jelle de Plaa ◽  
...  

The Hitomi results for the Perseus cluster have shown that accurate atomic models are essential to the success of X-ray spectroscopic missions and just as important as the store of knowledge on instrumental calibration and astrophysical modeling. Preparing the models requires a multifaceted approach, including theoretical calculations, laboratory measurements, and calibration using real observations. In a previous paper, we presented a calculation of the electron impact cross sections on the transitions forming the Fe-L complex. In the present work, we systematically tested the calculation against cross-sections of ions measured in an electron beam ion trap experiment. A two-dimensional analysis in the electron beam energies and X-ray photon energies was utilized to disentangle radiative channels following dielectronic recombination, direct electron-impact excitation, and resonant excitation processes in the experimental data. The data calibrated through laboratory measurements were further fed into a global modeling of the Chandra grating spectrum of Capella. We investigated and compared the fit quality, as well as the sensitivity of the derived physical parameters to the underlying atomic data and the astrophysical plasma modeling. We further list the potential areas of disagreement between the observations and the present calculations, which, in turn, calls for renewed efforts with regard to theoretical calculations and targeted laboratory measurements.


1974 ◽  
Vol 18 ◽  
pp. 299-308
Author(s):  
D. I. Bales ◽  
R. R. Landolt ◽  
W. E. Toll

AbstractThe production of characteristic x rays by 100-keV protons has been studied to determine the feasibility of using a Cockcroft- Walton accelerator as an excitation source for x ray fluorescence analysis. Because of the low cross sections at this proton energy, it was necessary to concentrate on characteristic x rays below 6 keV and to use beam currents of 10 to 100 μA. The x rays were measured by a high resolution Si(Li) detector.The preparation of various types of samples and the problems that arise when working at low proton energies and high beam currents are discussed.It was found that the technique is useful for low atomic number elements down to less than 1 ppm in a water sample when there are no other significant impurities. When other elements are present, however, proton absorption becomes an important factor and quantitative determinations become very difficult. Proton absorption and its effect upon the usefulness of the technique are discussed.The precision for the technique was determined and found to be better than 20% for most measurements. This includes errors in sample preparation which was considered to be a significant portion of the uncertainty.


2015 ◽  
Vol 21 (3) ◽  
pp. 695-705 ◽  
Author(s):  
Melanie J. Ceko ◽  
Katja Hummitzsch ◽  
Wendy M. Bonner ◽  
Jade B. Aitken ◽  
Kathryn M. Spiers ◽  
...  

AbstractX-ray fluorescence (XRF) was used to image 40 histological cross-sections of bovine ovaries (n=19), focusing on structures including: antral follicles at different stages of growth or atresia, corpora lutea at three stages of development (II–IV), and capillaries, arterioles, and other blood vessels. This method identified three key trace elements [iron (Fe), zinc (Zn), and selenium (Se)] within the ovarian tissue which appeared to be localized to specific structures. Owing to minimal preprocessing of the ovaries, important high-resolution information regarding the spatial distribution of these elements was obtained with elemental trends and colocalizations of Fe and Zn apparent, as well as the infrequent appearance of Se surrounding the antrum of large follicles, as previously reported. The ability to use synchrotron radiation to measure trace element distributions in bovine ovaries at such high resolution and over such large areas could have a significant impact on understanding the mechanisms of ovarian development. This research is intended to form a baseline study of healthy ovaries which can later be extended to disease states, thereby improving our current understanding of infertility and endocrine diseases involving the ovary.


Author(s):  
Robert A. Grant ◽  
Laura L. Degn ◽  
Wah Chiu ◽  
John Robinson

Proteolytic digestion of the immunoglobulin IgG with papain cleaves the molecule into an antigen binding fragment, Fab, and a compliment binding fragment, Fc. Structures of intact immunoglobulin, Fab and Fc from various sources have been solved by X-ray crystallography. Rabbit Fc can be crystallized as thin platelets suitable for high resolution electron microscopy. The structure of rabbit Fc can be expected to be similar to the known structure of human Fc, making it an ideal specimen for comparing the X-ray and electron crystallographic techniques and for the application of the molecular replacement technique to electron crystallography. Thin protein crystals embedded in ice diffract to high resolution. A low resolution image of a frozen, hydrated crystal can be expected to have a better contrast than a glucose embedded crystal due to the larger density difference between protein and ice compared to protein and glucose. For these reasons we are using an ice embedding technique to prepare the rabbit Fc crystals for molecular structure analysis by electron microscopy.


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