Structure and Electrochemical Properties of FeSx Nanoparticles Synthesized by Chemical Vapor Condensation Process

2006 ◽  
pp. 950-953
Author(s):  
Jong Keun Ha ◽  
Kwon Koo Cho ◽  
Ki Won Kim ◽  
Jong Uk Kim ◽  
Yoo Young Kim
Keyword(s):  
Electrochemical Properties ◽  
Chemical Vapor ◽  
Vapor Condensation ◽  
Condensation Process ◽  
Chemical Vapor Condensation

Structure and Electrochemical Properties of FeSx Nanoparticles Synthesized by Chemical Vapor Condensation Process

2006 ◽  
Vol 510-511 ◽  
pp. 950-953 ◽  
Author(s):  
Jong Keun Ha ◽  
Kwon Koo Cho ◽  
Ki Won Kim ◽  
Jong Uk Kim ◽  
Yoo Young Kim
Keyword(s):  
Electron Microscopy ◽  
Electrochemical Properties ◽  
Chemical Vapor ◽  
Spherical Shape ◽  
Iron Pentacarbonyl ◽  
Vapor Condensation ◽  
Condensation Process ◽  
X Ray Diffraction ◽  
Chemical Vapor Condensation ◽  
Transmission Electron

FeSx nanoparticles were synthesized by the chemical vapor condensation (CVC) process using the pyrolysis of iron pentacarbonyl (Fe(CO)5) and sulfur (S). The influence of CVC parameter on the formation of nanoparticle and size distribution was studied. The synthesized nanoparticles consisting of FeS, FeS2 and Fe2O3 were nearly spherical shape and 5~40 nm in mean diameter. Obtained particles were studied by applying the field emission scanning electron microscopy (FESEM) and high resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD) methods. Electrochemical properties of the electrode fabricated with synthesized nanoparticles were evaluated.

One-step synthesis and properties of MnOx/TiO2 nanocomposites prepared by chemical vapor condensation process

2013 ◽  
Vol 233 ◽  
pp. 131-136 ◽  
Author(s):  
Eunseuk Park ◽  
Sungmin Chin ◽  
Yeon Seok Kim ◽  
Gwi-Nam Bae ◽  
Jongsoo Jurng
Keyword(s):  
Chemical Vapor ◽  
Vapor Condensation ◽  
Condensation Process ◽  
Chemical Vapor Condensation ◽  
One Step

Synthesis of Metal Oxide Hollow Nanoparticles by Chemical Vapor Condensation Process

2006 ◽  
Vol 317-318 ◽  
pp. 219-222 ◽  
Author(s):  
C.W. Lee ◽  
S.G. Kim ◽  
Jai Sung Lee
Keyword(s):  
Iron Oxide ◽  
Reaction Temperature ◽  
Chemical Vapor ◽  
Phase Evolution ◽  
Vapor Condensation ◽  
Condensation Process ◽  
Iron Oxide Particles ◽  
Hollow Nanoparticles ◽  
Chemical Vapor Condensation ◽  
Oxide Phases

The influence of reaction temperature on phase evolution of iron oxide hollow nanoparticles during chemical vapor condensation (CVC) process using iron acetylacetonate was investigated. X-ray diffraction (XRD) analyses revealed that three iron oxide phases (α-Fe2O3, γ-Fe2O3, and Fe3O4) and a mixture of β-Fe2O3 and small amount of γ-Fe2O3 were synthesized at 700oC and 900oC, respectively. TEM observation disclosed that the iron oxide particles are almost composed of hollow structured nanoparticles of 10~20 nm in size and 3~5 nm in shell thickness. This result implies that reaction temperature determining various reaction parameters plays an important role for the phase- and structural evolutions of iron oxide hollow nanoparticles. Especially, the present investigation attempted to explain temperature dependence of the phase evolution of β-Fe2O3 hollow nanoparticles in association with the decomposition of iron acetylacetonate.

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