The Abnormal Grain Growth of P/M Nickel-Base Superalloy: Strain Storage and CSL Boundaries

2014 ◽  
Vol 1064 ◽  
pp. 49-54 ◽  
Author(s):  
Shuang Fang ◽  
Yun Peng Dong ◽  
Shu Yun Wang

The Nickel-base superalloy samples were prepared by the isothermal forging in different strain rates at 1070°C. The isothermal deformation tests were carried out at constant strain rate in a vacuum environment using the Thermecmastor (Fuji Electronic Industrial Co., Japan) with a capacity of 30 ton compressive force. All the samples were deformed to a true strain of 1.04 at deformation temperature 1070°C and strain rate 0.001s-1~0.1s-1 respectively. The result is The deformation strain rate determine the position and domain of AGG and the temperature determine the severity of AGG by deformation temperature and temperature rise. The most serious region of AGG is related to the specific CSL boundaries. The fraction of Ʃ3 boundary reaches the peak point value and fraction of Ʃ7 boundary reaches the valley point value in all the samples with different strain rates. The most serious region of AGG is also related to the residual strain. In the most serious region of AGG, more dislocation is used to prefer grain growth to recrystallization, which can refine grain.

2015 ◽  
Vol 710 ◽  
pp. 37-43 ◽  
Author(s):  
Shuang Fang ◽  
Min Cong Zhang ◽  
Yun Peng Dong ◽  
Shu Yun Wang

The samples with a length of 50mm and cross section area of 20mm2 were machined from extruded P/M Nickel-base superalloy billet and the isothermal deformation tests were carried out at constant strain rate in a vacuum environment using the Thermecmastor. All the samples were deformed to a true strain of 1.04 at deformation temperature 1070°C and 1100°C and strain rate 0.001s-1~1s-1 respectively. The result is the deformation strain rate determine the position and the deformation temperature determine the severity of abnormal grain growth (AGG). The initial grain size and dislocation density is not the only reason to AGG. The AGG is related the recrystallization nucleation process is inhibited in the heat treatment. The AGG region usually has more low energy and low migration rate boundary than other regions.


2013 ◽  
Vol 834-836 ◽  
pp. 432-436 ◽  
Author(s):  
Fu Wei Kang ◽  
Xue Min Zhang ◽  
Jian Fei Sun ◽  
Jun Ling Zhao

The hot deformation behaviors of the nickel-base superalloy GH4169 have been studied by isothermal constant true strain rate compression testing at 950°C-1150°C, 0.01s-1-10s-1and the height reduction 50%. The processing maps of GH4169 alloy have been constructed at different strains on the basis of testing data using a dynamic materials modeling. The maps exhibited two domains: the first at 950°C - 1100°C and strain rate higher than 0.1s-1, with a peak efficiency of power dissipation of 0.1, and the second at 950°C-1100°C and strain rate lower than 1s-1, with a peak efficiency of power dissipation of 0.4 and the strain rate of 0.01s-1. On the basis of microstructure observations, the first exhibits adiabatic shear bands, which called instability domain, the second represents fine recrystallized grain structures, which called stability domain. The optimal hot-working parameters are at 1050°C, 0.01s-1.


Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2652
Author(s):  
Meng Liu ◽  
Quanyi Wang ◽  
Yifan Cai ◽  
Dong Lu ◽  
Tianjian Wang ◽  
...  

Tensile deformation behavior and microstructure of nickel-base superalloy Inconel 625 are investigated under different strain rates of 5 × 10−4 s−1 and 5 × 10−5 s−1. According to the experimental results, yield strength and ultimate tensile strength of the alloy increase with the increase in strain rate in room temperature. Microstructure results indicate that the size of dimples is smaller in the tensile fracture surface at low strain rate than the high strain rate, and the number of dimples is also related to the strain rates and twins appear earlier in the specimens with higher strain rates. Apart from Hollomon and Ludwik functions, a new formula considering the variation trend of strength in different deformation stages is deduced and introduced, which fit closer to the tensile curves of the 625 alloy used in the present work at both strain rates. Furthermore, the Schmid factors of tensile samples under two strain rates are calculated and discussed. In the end, typical work hardening behavior resulting from the dislocations slip behavior under different strain rates is observed, and a shearing phenomenon of slip lines cross through the δ precipitates due to the movement of dislocations is also be note.


2019 ◽  
Vol 179 ◽  
pp. 142-157 ◽  
Author(s):  
Jinghao Xu ◽  
Hans Gruber ◽  
Dunyong Deng ◽  
Ru Lin Peng ◽  
Johan J. Moverare

2016 ◽  
Vol 34 (3) ◽  
pp. 157-165 ◽  
Author(s):  
Jianjun Wang ◽  
Wei-Guo Guo ◽  
Penghui Li ◽  
Ping Zhou

1980 ◽  
Vol 14 (6) ◽  
pp. 577-581 ◽  
Author(s):  
R. Angers ◽  
K. Hajmrle

2014 ◽  
Vol 1077 ◽  
pp. 50-55
Author(s):  
Shuang Fang ◽  
Min Cong Zhang ◽  
Qiu Ying Yu ◽  
Shu Yun Wang ◽  
Chun Xiao Cao

The Nickel-base superalloy samples were prepared by the isothermal forging in strain rate 1s-1 at deformation temperature 1070°C with different strain levels. The EBSD was carried out in order to investigate the microstructural changes that took place due to strain level. The result is the samples has no apparent dynamic recrystallization behavior in hot deformation in 1s-1 at 1070°C. The true stress-true strain curve has two peak values in the strain level of 20% and 60%, and one valley value in the strain level of 50%. The first peak value is result in the activation of slip system and the beginning of recrystallization and the second peak value of the true stress-true strain curve is result in the inhibition of activation of slip system and grain growth by the dislocation density. The work hardening behavior of P/M Nickel-base superalloy may be related to the size ratio of γ’ phase with grain size.


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