Seed-Mediated Synthesis of one-Dimensional Fe3O4 Particles under Magnetic Field

2011 ◽  
Vol 311-313 ◽  
pp. 576-580
Author(s):  
Pei Feng Yu ◽  
Xi Yun Yang ◽  
Hai Wei Yuan

One-dimensional magnetite particles were prepared by a seed-mediated growth method under magnetic field. The amount of seed, seed size, PolyvinylPyrrolidone concentration (PVP) and reaction time have a significant effect on the morphology of the samples. The addition of a small amount of 100nm seeds leads to obtain rod-like particles, while chain-like particles are formed when the seed size is increased to 700 nm. The aspect ratio of the rod is controlled by varying the volume ratio of seed to iron salt. Increasing the reaction time is favorable to the formation of chain-like particles.

2021 ◽  
Vol 1152 ◽  
pp. 338277
Author(s):  
Xiaojuan Zhou ◽  
Qiang Liu ◽  
Xiaoyu Shi ◽  
Chunli Xu ◽  
Baoxin Li

2013 ◽  
Vol 1584 ◽  
Author(s):  
E. K.C. Pradeep ◽  
X. Li ◽  
T. Kawaharamura ◽  
D. Wang ◽  
A. Hatta ◽  
...  

ABSTRACTZnO nanorods were grown up from as-deposited ZnO film on which the zinc self-catalysts generated by a novel reducing method. Well aligned ZnO nanorods with a uniform high aspect ratio were grown up on multi-annealed samples. The length of nanorods depended significantly on the reaction time in the hydrothermal synthesis.


2005 ◽  
Vol 19 (15n17) ◽  
pp. 2757-2762 ◽  
Author(s):  
Y. ZHANG ◽  
R. SHI ◽  
H. Q. XIONG ◽  
Y. ZHAI ◽  
Y. K. SUN

Magnetite chains of spheres with different radii and lengths were prepared by aging ferrous hydroxide gel with 0.2M KNO3 under different external magnetic fields which induced the ultra-fine magnetite particles to combine into chain structure. The magnetite particle size and the chain length could be adjusted by varying the field intensity. The chains could be deposited on silicon substrates to form aligned structure in magnetic field. The hysteresis loops were measured in different directions by a vibrating sample magnetometer (VSM). The structure and magnetic properties were discussed.


2019 ◽  
Vol 2 (22) ◽  
pp. 119-133
Author(s):  
Mahsa Mohammadzadeh ◽  
Mohsen Ashjari ◽  
Davoud Zare

In this paper, nanofluids were prepared based on gold nanorods in basic fluid, water, by single-stage chemical reduction and in different volume fractions and the used gold nanorods were synthesized by seed-mediated growth method in different dimensional ratios. The properties of the prepared nanoparticles, including crystalline size, aspect ratio, surface properties, nanoparticle purity, shape and morphology of nanostructures were investigated using x-ray diffraction, UV-vis spectroscopy, FT-IR, and transmitted electron microscopy. The effect of changing parameters of Nano rod dimensions, changes in Nano rod volume fraction in water and also the effect of temperature on the nanofluid thermal conductivity coefficient were investigated using transient hot wire method. The results showed that reducing the aspect ratio, increasing the volume fraction and increasing the temperature increase the thermal conductivity. In fact, results show that an increase in the nanorods aspect ratio with a constant volume fraction of 1:50 of gold in water nanorod and at room temperature leads to a decrease in the thermal conductivity of the nanofluid. Also, increasing the two parameters of volume fraction and temperature significantly increases the thermal conductivity coefficient.


2011 ◽  
Vol 364 ◽  
pp. 254-259 ◽  
Author(s):  
Sri Nengsih ◽  
Ali Umar Akrajas ◽  
Muhamad Mat Salleh

This paper reports the synthesis of gold nanorod with controlled aspect ratio prepared by varying the concentration of nanoseed addition into the growth solution via seed mediated growth method. In typical process, the gold nanorod with aspect ratio from ca. 1.7 to 3.1 can be successfully obtained. The nanorod seems to be perfect rod morphology instead of bone-like or tear drop structure. Owing to the simplicity in preparing the gold nanorod, the present approach could be used as potential alternative for producing gold nanorod with special properties for used in the currently existing application.


Molecules ◽  
2019 ◽  
Vol 24 (8) ◽  
pp. 1455
Author(s):  
Deeney ◽  
McKiernan ◽  
Belhout ◽  
Rodriguez ◽  
Redmond ◽  
...  

Luminescent carbon nanomaterials are important materials for sensing, imaging, and display technologies. This work describes the use of microwave heating for the template-assisted preparation of luminescent carbon nanofibers (CNFs) from the reaction of a range of beverage-related precursors with the nitrogen-rich polyethyleneimine. Highly luminescent robust carbon fibers that were 10 to 30 m in length and had a diameter of 200 nm were obtained under moderate conditions of temperature (250–260 °C) and a short reaction time (6 min). The high aspect ratio fibers showed wavelength-dependent emission that can be readily imaged using epifluorescence. The development of these multi-emissive one-dimensional (1D) carbon nanomaterials offers potential for a range of applications.


2019 ◽  
Author(s):  
Clara Deeney ◽  
Eoin P. McKiernan ◽  
Samir A. Belhout ◽  
Brian J. Rodriguez

Luminescent carbon nanomaterials are important materials for sensing, imaging, and display technologies. This work describes the use of microwave heating for the template-assisted preparation of luminescent carbon nanofibers (CNFs) from the reaction of a range of beverage-related precursors with the nitrogen-rich polyethyleneimine. Highly luminescent robust carbon fibers that were 10 to 30 μm in length and had a diameter of 200 nm were obtained under moderate conditions of temperature (250–260 °C) and a short reaction time (6 min). The high aspect ratio fibers showed wavelength-dependent emission that can be readily imaged using epifluorescence. The development of these multi-emissive one-dimensional (1D) carbon nanomaterials offers potential for a range of applications.


2015 ◽  
Vol 11 (6) ◽  
pp. 3630-3634
Author(s):  
T.A. Mamedova ◽  
Z.M. Aliyeva ◽  
A.E. Aliyeva ◽  
R.T. Samedov ◽  
V.M. Abbasov ◽  
...  

The process of producing mono-alkyl esters of fatty acids from cottonseed and sunflower oils under the influence of the magnetic field with intensity  15-45 mT  was  investigated . It was revealed that the use of the energy of  magnetic field allows to reduce the reaction time to 10 times, the excess of used alcohol to 2 times while maintaining high yield of the desired product.


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