Determination of Ni(II) in Water Using Nanometer Attapulgite Adsorption via FAAS

2012 ◽  
Vol 599 ◽  
pp. 96-99
Author(s):  
Yan Min Hou ◽  
Xiao Jun Zhao ◽  
Ji Min Xie
Keyword(s):  
Detection Limit ◽  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Environmental Water ◽  
Regression Equation ◽  
Experimental Results ◽  
Hydrochloric Acid Concentration ◽  
Elution Volume ◽  
Adsorbent Dosage

nanometer attapulgite is a fine adsorptive reagent to Ni(II) in specific pH,adsorbent dosage , surging and depositing time, hydrochloric acid concentration, elution volume , surging and depositing time for the recovery and static adsorptive capability. The experimental results show that Zn(II)、Co(II)、K+、Cu(II)、Na+、Mn(II)、Pb(II)、Hg(II) 、SiO32- 、WO42- 、MoO42- 、HPO42-、VO3- didn’t interfere the adsorption to Ni(Ⅱ). the linear range is 0.10~1.5ug/mL, the regression equation is A=0.0476C+0.0084 r=0.9996 .the detection limit is 0.190μg/mL for Ni(II),recovery is 86.7.5%-102.5%. This method can be used to the determination of Ni(II) in environmental water.

ORGANIC REAGENTS FOR PLATINUM METALS: I. THE DETERMINATION OF PALLADIUM WITH 1,10-PHENANTHROLINE

1949 ◽  
Vol 27b (2) ◽  
pp. 67-71 ◽  
Author(s):  
D. E. Ryan ◽  
P. Fainer
Keyword(s):  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Volumetric Method ◽  
Hydrochloric Acid Concentration ◽  
Platinum Metals ◽  
Chloride Solutions ◽  
Organic Reagents

Palladium may be precipitated quantitatively with 1,10-phenanthroline from palladous chloride solutions; variations in the hydrochloric acid concentration from 1 to 20% had no effect on the precipitation. The reagent yields no precipitates with other platinum metals under similar conditions; slightly high results, however, were obtained when palladium was precipitated from solutions containing these metals. The precipitate has the composition C12H8N2PdCl2 and may be used as a weighing form for palladium. A micro-volumetric method for palladium using 1,10-phenanthroline is described. Small amounts of platinum (as Pt+4) do not interfere.

Determination of Chitosan Oligosaccharide Content by Acetylacetone Spectrophotometry Method

2012 ◽  
Vol 503-504 ◽  
pp. 543-547 ◽  
Author(s):  
Ze Ping Xu ◽  
Chuan Lun Yang ◽  
Xin Qing Zhang ◽  
Xiu Zhi Wang ◽  
Bao Sheng Huang
Keyword(s):  
Hydrochloric Acid ◽  
Linear Relationship ◽  
Regression Equation ◽  
Common Method ◽  
Chitosan Oligosaccharide ◽  
Average Recovery ◽  
Good Linear ◽  
Good Linear Relationship

Objective: To establish a common method to detect the content of chitosan oligosaccharide. Methods: Chitosan oligosaccharide was hydrolyzed completely by concentrated hydrochloric acid, and the solution was regulated into neutral with NaOH. Then, determined the absorbance in 525nm, and substituted into the regression equation to determine the results. Results: The results showed there was a good linear relationship when the concentration of chitosan oligosaccharide ranged from 0.02 mg/mL to 0.12 mg/mL, r2 = 0.999. The average recovery of chitosan oligosaccharide samples was 99.25%. Conclusion: The method is sensitive, accurate and simple. It is applied to determine of the content of chitosan oligosaccharide.

Experimental Study on Concentrating Scandium by Leaching from Associated Scandium Ore

2013 ◽  
Vol 734-737 ◽  
pp. 1033-1036
Author(s):  
Gui Fang Zhang ◽  
Peng Yan ◽  
Qing Rong Yang
Keyword(s):  
Experimental Study ◽  
Particle Size ◽  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Hydrochloric Acid Concentration ◽  
Leaching Rate ◽  
Optimal Conditions ◽  
Research Results ◽  
Solid Ratio ◽  
Leaching Residue

Based on the benefication of the complex silicate ore containing scandium, the research about aid-leaching agent used in the leaching of the scandium concentrate was been conducted. And the suitable leaching agent and aid-leaching agent which the useful ions entered into leaching liquid and the harmful ions were kept in leaching residue were been found according to the experiment results. For the scandium of sample existed various complex silicate ore as isomorphism form, the research has adopted hydrochloric acid with aid-leaching agent to dissociate the silicate ore and make scandium entering into solution. The research results has shown that the scandium leaching rate could reach 92.06% under the optimal conditions which the hydrochloric acid concentration is 22.8%, the dosage of aid leaching agent is 6%, liquid solid ratio is 4:1, particle size of leaching material totally is less than 0.15mm and leaching time is 8h.

Effects of high hydrochloric acid concentration on aniline chemical polymerization

Polymer ◽  
1997 ◽  
Vol 38 (20) ◽  
pp. 5247-5250 ◽  
Author(s):  
Gustavo M. Morales ◽  
Marcos Llusa ◽  
Maria C. Miras ◽  
Cesar Barbero
Keyword(s):  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Hydrochloric Acid Concentration ◽  
Chemical Polymerization

Extraction of Tin (Sn) from Solder Dross by Using Hydrochloric Acid Leaching Treatment

2015 ◽  
Vol 754-755 ◽  
pp. 567-570
Author(s):  
Syarifah Aminah Ismail ◽  
Noorina Hidayu Jamil ◽  
Kamarudin Hussin ◽  
Mohd Arif Anuar Mohd Salleh
Keyword(s):  
Aqueous Solution ◽  
Particle Size ◽  
Hydrochloric Acid ◽  
Acid Concentration ◽  
Acid Leaching ◽  
Experimental Results ◽  
Solution Temperature ◽  
Hydrochloric Acid Leaching ◽  
Stirring Time ◽  
Acid Aqueous Solution

This project deals with the experimental results of leaching of Sn from solder dross by means of leaching using different concentration of hydrochloric acid (HCl). Solder dross was sieved to obtain a mean particle size of 75 μm. The solder dross powder obtained was leached by using HCl acid aqueous solution. To optimize the parameter required for recovery of Sn from solder dross, initially the bench scale studies were carried out using varying acid concentration, stirring time and temperature. The experimental indicate that 98.7% of Sn was leached out from solder dross using 0.1M of HCl, 24 hours of stirring time at60°C solution temperature.

scholarly journals Sorption and Preconcentration of Lead on Silica Nanoparticles Modified with Resacetophenone

2009 ◽  
Vol 6 (3) ◽  
pp. 633-638 ◽  
Author(s):  
Anupreet Kaur ◽  
Usha Gupta
Keyword(s):  
Detection Limit ◽  
Hydrochloric Acid ◽  
Adsorption Equilibrium ◽  
Sample Volume ◽  
Factor Effect ◽  
Optimum Ph ◽  
Batch Technique ◽  
Preconcentration Factor ◽  
Interfering Ions

The silica-resacetophenone (SiO2-RATP) nanoparticles were used as a new sorbent for extraction of trace amounts of Pb(II) by batch technique. Conditions of the analysis such as preconcentration factor, effect of pH, sample volume, shaking time, elution conditions and effects of interfering ions for the recovery of analyte were investigated. The adsorption capacity of nanometer SiO2-RATP was found to be 167.24 µ mol/g at optimum pH and the detection limit (3σ) was 0.58 µg/L. The adsorption equilibrium of Pb(II) on nanometer SiO2-RATP was achieved in 20 min. Adsorbed Pb(II) was easily eluted with 5 mL of 0.5 M hydrochloric acid. The maximum preconcentration factor was 60. The method was applied for the determination of trace amounts of Pb(II) in various natural water rivers.

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