In Situ Detection of Thermal Cycle in Weld Metal of Cr-Mo Steel

2012 ◽  
Vol 602-604 ◽  
pp. 2061-2064
Author(s):  
Hai Tao Li ◽  
Yong Chang Zhu ◽  
Shou Fan Rong ◽  
Li Jie Qu
Keyword(s):  
Weld Metal ◽  
Thermal Cycle ◽  
Thermal Process ◽  
The Self ◽  
Low Alloy Steel ◽  
Welding Thermal Cycle ◽  
Welding Procedure ◽  
In Situ Detection ◽  
Local Hardening

With the self-designed system of welding thermal cycle test, low alloy steel of Cr-Mo series was welded through proper welding procedure according to the phenomenon of cold crack and local hardening in weld metal, and in-situ detection of thermal cycle for deposit metal was realized. The results show that self-designed system is reliable within the error range, the maximum peak temperature during thermal process was above 1700°C, it is largely improved than reported formerly.

Microstructural evolution and mechanical integrity relationship of dissimilar metal welding between 2205 duplex stainless steel and composite bimetallic plates

2021 ◽  
pp. 095440622110036
Author(s):  
Changqing Ye ◽  
Weiguo Zhai ◽  
Guangyao Lu ◽  
Qingsong Liu ◽  
Liang Ni ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Weld Metal ◽  
Duplex Stainless Steel ◽  
Intergranular Corrosion ◽  
Thermal Cycle ◽  
Filler Metal ◽  
2205 Duplex Stainless Steel ◽  
Welding Thermal Cycle ◽  
Intergranular Corrosion Resistance

In this paper, shielded metal arc welding on the dissimilar joint between 2205 duplex stainless steel and composite bimetallic plates (304 L stainless steel/10CrNi3MoV steel) with a filler metal E2209 was performed. Furthermore, the microstructure, phase, mechanical properties and intergranular corrosion resistance of the joints were investigated and element distributions of the interfaces were characterized. The results show that austenite transformed to ferrite under the influence of welding thermal cycle, and then a large amount of ferrite appeared in heat affected zone (HAZ) of 2205 duplex stainless steel. Coarse bainite grains were formed in HAZ of the 10CrNi3MoV steel near the fusion line with high temperature welding thermal cycle. Fine granular bainite was also generated in HAZ of 10CrNi3MoV steel due to the relatively short exposure time to the active temperature of grain growth. Local peak temperature near the base 10CrNi3MoV steel was still high enough to recrystallize the 10CrNi3MoV steel to form partial-recrystallization HAZ due to phase change. The filler metal was compatible with the three kinds of base materials. The thickness of the elemental diffusion interfaces layers was about 100 µm. The maximum microhardness value was obtained in the HAZ of 2205 duplex stainless steel (287 ± 14 HV), and the minimum one appeared in HAZ of SS304L (213 ± 5 HV). The maximum tensile strength of the welded joint was about 670 ± 6 MPa, and the tensile specimens fractured in ductile at matrix of the composite bimetallic plates. The impact energy of the weld metal and HAZ of the 10CrNi3MoV steel tested at –20 °C were 274 ± 6 J and 308 ± 5 J, respectively. Moreover, the intergranular corrosion resistance of the weldment including 304 L stainless steel, weld metal, HAZs and 2205 duplex stainless steel was in good agreement with the functional design requirements of materials corrosion resistance.

Effect of welding thermal cycle on structural and phase weld metal transformations for heat-resistant Cr–Mo–V steels

2017 ◽  
Vol 8 (6) ◽  
pp. 886-891
Author(s):  
M. N. Timofeev ◽  
G. P. Karzov ◽  
S. N. Galyatkin ◽  
E. I. Mikhaleva
Keyword(s):  
Weld Metal ◽  
Thermal Cycle ◽  
Heat Resistant ◽  
Welding Thermal Cycle

Effect of Welding Thermal Cycle on the Microstructure and Mechanical Properties in Multi-Pass Submerged-Arc Welding

2011 ◽  
Vol 314-316 ◽  
pp. 1163-1166 ◽  
Author(s):  
Zhong Yi Chen ◽  
Yong Lin Ma ◽  
Shu Qing Xing
Keyword(s):  
Mechanical Properties ◽  
Weld Metal ◽  
Arc Welding ◽  
Thermal Cycle ◽  
Welded Joint ◽  
Submerged Arc Welding ◽  
Welding Parameters ◽  
Microstructure And Mechanical Properties ◽  
Welding Thermal Cycle ◽  
Submerged Arc

To research effect of welding thermal cycle on the microstructure and mechanical properties of welded joint, two pieces of 60mm thick plates were welded together using automatic submerged-arc welding (SAW) method with suitable welding parameters. After 17 passes welding, the microstructures and phases of the welded joint was carefully observed and analyzed by using a Carl Zeiss optical microscope in different zones of welded joint, and the surface micro-hardness of the welded joint was measured systematically by using microscopic-hardness tester Lycra. Afterwards, the mechanical properties of the weld metals were measured through stretching. Through a series of measurements and observations, the welding experiment results indicate that effect of welding thermal cycle on the microstructure and mechanical properties of welding joint is great, the grains of the bottom of the weld metal are certainty smaller and more uniform, and the bottom of the weld metal have more excellent mechanical properties.

Correlation between dislocation, grain boundary and interface of duplex SS in stress corrosion cracking(SCC)

1990 ◽  
Vol 48 (4) ◽  
pp. 928-929
Author(s):  
Wang Zheng-fang ◽  
Z.F. Wang
Keyword(s):  
Stainless Steel ◽  
Thermal Cycle ◽  
Secondary Phase ◽  
Corrosion Cracking ◽  
Coarse Grained ◽  
Test Environment ◽  
Fine Grained ◽  
Evaluation Test ◽  
Welding Thermal Cycle ◽  
Micro Analysis

The main purpose of this study highlights on the evaluation of chloride SCC resistance of the material,duplex stainless steel,OOCr18Ni5Mo3Si2 (18-5Mo) and its welded coarse grained zone(CGZ).18-5Mo is a dual phases (A+F) stainless steel with yield strength:512N/mm2 .The proportion of secondary Phase(A phase) accounts for 30-35% of the total with fine grained and homogeneously distributed A and F phases(Fig.1).After being welded by a specific welding thermal cycle to the material,i.e. Tmax=1350°C and t8/5=20s,microstructure may change from fine grained morphology to coarse grained morphology and from homogeneously distributed of A phase to a concentration of A phase(Fig.2).Meanwhile,the proportion of A phase reduced from 35% to 5-10°o.For this reason it is known as welded coarse grained zone(CGZ).In association with difference of microstructure between base metal and welded CGZ,so chloride SCC resistance also differ from each other.Test procedures:Constant load tensile test(CLTT) were performed for recording Esce-t curve by which corrosion cracking growth can be described, tf,fractured time,can also be recorded by the test which is taken as a electrochemical behavior and mechanical property for SCC resistance evaluation. Test environment:143°C boiling 42%MgCl2 solution is used.Besides, micro analysis were conducted with light microscopy(LM),SEM,TEM,and Auger energy spectrum(AES) so as to reveal the correlation between the data generated by the CLTT results and micro analysis.

Rapid quantification and in situ detection of nitrifying bacteria in biofilms by monoclonal antibody method

2000 ◽  
Vol 41 (4-5) ◽  
pp. 301-308 ◽  
Author(s):  
N. Noda ◽  
H. Ikuta ◽  
Y. Ebie ◽  
A. Hirata ◽  
S. Tsuneda ◽  
...  
Keyword(s):  
Monoclonal Antibody ◽  
Monoclonal Antibodies ◽  
Fluorescent Antibody ◽  
Nitrifying Bacteria ◽  
Fluorescent Antibody Technique ◽  
Antibody Technique ◽  
Antibody Method ◽  
In Situ Detection ◽  
Rapid Quantification

Fluorescent antibody technique by the monoclonal antibody method is very useful and helpful for the rapid quantification and in situ detection of the specific bacteria like nitrifiers in a mixed baxterial habitat such as a biofilm. In this study, twelve monoclonal antibodies against Nitrosomonas europaea (IFO14298) and sixteen against Nitrobacter winogradskyi (IFO14297) were raised from splenocytes of mice (BALB/c). It was found that these antibodies exhibited little cross reactivity against various kinds of heterotrophic bacteria. The direct cell count method using monoclonal antibodies could exactly detect and rapidly quantify N. europaea and N. winogradskyi. Moreover, the distribution of N. europaea and N. winogradskyi in a biofilm could be examined by in situ fluorescent antibody technique. It was shown that most of N. winogradskyi existed near the surface part and most of N. europaea existed at the inner part of the polyethylene glycol (PEG) gel pellet, which had entrapped activated sludge and used in a landfill leachate treatment reactor. It was suggested that this monoclonal antibody method was utilized for estimating and controlling the population of nitrifying bacteria as a quick and favorable tool.

scholarly journals Single Step In Situ Detection of Surface Protein and MicroRNA in Clustered Extracellular Vesicles Using Flow Cytometry

2021 ◽  
Vol 10 (2) ◽  
pp. 319
Author(s):  
Hee Cheol Yang ◽  
Won Jong Rhee
Keyword(s):  
Extracellular Vesicles ◽  
Liquid Biopsy ◽  
Molecular Beacon ◽  
Disease Diagnosis ◽  
Single Step ◽  
Flow Cytometer ◽  
Surface Proteins ◽  
Biomarker Detection ◽  
In Situ Detection

Because cancers are heterogeneous, it is evident that multiplexed detection is required to achieve disease diagnosis with high accuracy and specificity. Extracellular vesicles (EVs) have been a subject of great interest as sources of novel biomarkers for cancer liquid biopsy. However, EVs are nano-sized particles that are difficult to handle; thus, it is necessary to develop a method that enables efficient and straightforward EV biomarker detection. In the present study, we developed a method for single step in situ detection of EV surface proteins and inner miRNAs simultaneously using a flow cytometer. CD63 antibody and molecular beacon-21 were investigated for multiplexed biomarker detection in normal and cancer EVs. A phospholipid-polymer-phospholipid conjugate was introduced to induce clustering of the EVs analyzed using nanoparticle tracking analysis, which enhanced the detection signals. As a result, the method could detect and distinguish cancer cell-derived EVs using a flow cytometer. Thus, single step in situ detection of multiple EV biomarkers using a flow cytometer can be applied as a simple, labor- and time-saving, non-invasive liquid biopsy for the diagnosis of various diseases, including cancer.

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