Study on Bamboo Kraft Pulping with DTPMPA

2013 ◽  
Vol 781-784 ◽  
pp. 2658-2661
Author(s):  
Hong Xia Gao ◽  
Xiu Qiong Guan ◽  
Chun Yue Ding
Keyword(s):  
Phosphonic Acid ◽  
Kraft Pulping ◽  
Kappa Number ◽  
Maximum Temperature ◽  
Pulp Yield ◽  
Waste Liquor ◽  
Diethylene Triamine ◽  
Bamboo Pulp ◽  
Cooking Temperature ◽  
Optimized Conditions

DTPMPA (Diethylene Triamine Penta Methylene Phosphonic Acid) was used as cooking additive in Bamboo pulping. The effect of cooking parameters such as alkali charge, maximum cooking temperature, and time at maximum temperature on bamboo kraft pulping adding additive Diethylene Triamine Penta Methylene Phosphonic Acid was studied. The results show that the optimized bamboo kraft pulping conditions are: alkali charge 17%, maximum cooking temperature 162°C, and time at maximum temperature 60min when DTPMPA dosage is 0.4%. On the optimized conditions of cooking, the highest screened bamboo pulp yield 49.52%, the kappa number of bamboo pulp is 24.68, residual alkali in kraft waste liquor 3.62g/L .

Study on DTPMPA as Cooking Additive in Bamboo Pulping

2013 ◽  
Vol 781-784 ◽  
pp. 2601-2604
Author(s):  
Hong Xia Gao ◽  
Jing Zhang
Keyword(s):  
Phosphonic Acid ◽  
Chelating Agents ◽  
Kraft Pulping ◽  
Maximum Temperature ◽  
Pulp Yield ◽  
K Value ◽  
Diethylene Triamine ◽  
Bamboo Pulp ◽  
Cooking Temperature ◽  
Optimized Conditions

The application of chelating agents DTPMPA (Diethylene Triamine Penta Methylene Phosphonic Acid) as cooking aids in kraft pulping of bamboo was researched. The effect of DTPMPA dosage at different alkali charge was discussed. The results showed that the cooking aids DTPMPA added in bamboo kraft pulping was able to reduce K value of pulp, improve the screened stock yield and brightness and reduce the alkali charge. The optimized bamboo kraft pulping conditions are: DTPMPA dosage 0.4%, alkali charge 19%, when sulfidity was 20%, maximum cooking temperature was 165°C and time at maximum temperature was 90min. Under optimized conditions of cooking, the screened bamboo pulp yield is higher, the K value is lower and the bamboo pulp brightness is higher.

Application of Chelating Agents as Cooking Aids in Bamboo Pulping

2013 ◽  
Vol 750-752 ◽  
pp. 1520-1523
Author(s):  
Hong Xia Gao ◽  
Wen Hua He ◽  
Xiu Qiong Guan ◽  
Chun Liu ◽  
Bo Yuan
Keyword(s):  
Phosphonic Acid ◽  
Chelating Agents ◽  
Kraft Pulping ◽  
Kappa Number ◽  
Pulp Yield ◽  
Diethylene Triamine ◽  
Bamboo Pulp ◽  
Kraft Cooking ◽  
Pulp Strength

The effect of chelating agents Diethylene Triamine Penta Methylene Phosphonic Acid in bamboo kraft cooking was studied. The results show that the bamboo pulp yield was 49.52% when DTPMPA dosage is 0.4%, at the same time the Kappa number was lower. With the increasing of DTPMPA dosage in bamboo kraft pulping, the bamboo pulp strength was increased.

Effect of DTPMPA on Bamboo Kraft Pulping

2014 ◽  
Vol 1033-1034 ◽  
pp. 216-219
Author(s):  
Hong Xia Gao ◽  
Xiu Qiong Guan ◽  
Miao Xu ◽  
Xiong Zhang
Keyword(s):  
Phosphonic Acid ◽  
Kraft Pulping ◽  
Maximum Temperature ◽  
K Value ◽  
Diethylene Triamine ◽  
Bamboo Pulp ◽  
Cooking Temperature ◽  
The Impact

As a cooking additive, the impact of Diethylene Triamine Penta Methylene Phosphonic Acid (DTPMPA) on bamboo kraft pulping was studied. The effect of DTPMPA dosage at different maximum cooking temperature was discussed. The results showed that the cooking aids DTPMPA added in bamboo kraft pulping was able to reduce K value of pulp, improve the screened stock yield and brightness and reduce the alkali charge. The optimized bamboo kraft pulping conditions are: DTPMPA dosage 0.3%, alkali charge 17%, when sulfidity was 20%, maximum cooking temperature was 160°C and time at maximum temperature was 90min. Under the conditions of cooking, the screened yield is 41.53%, the K value is 15.4 and the bamboo pulp brightness is 26.8%.

Research on Kraft Pulping Delignification of Bamboo (Neosinocalamus)

2011 ◽  
Vol 418-420 ◽  
pp. 2241-2244
Author(s):  
Pei Yi Li ◽  
Mei Yun Zhang ◽  
Xin Xing Xia ◽  
Chun Tao Lin
Keyword(s):  
Fiber Material ◽  
Wide Distribution ◽  
Kraft Pulping ◽  
Kappa Number ◽  
Raw Material ◽  
Maximum Temperature ◽  
Pulp Yield ◽  
Oxygen Delignification ◽  
Local Conditions ◽  
Bamboo Pulp

Bamboo, as a kind of non-wood raw material, has a long, thin fiber with wide distribution and rich abundance in China. Its pulping properties are between softwood and hardwood. Adapting to the Chinese situation, developing bamboo pulp industrialization, according to the local conditions, is an available way to solve the shortage of fiber material for paper-making. Delignification of bamboo (Neosinocalamus) was carried out by conventional kraft and soda pulping under varying conditions to determine the relationships between selected cooking parameters (EA 14~20%, sulfidity 0~40%, maximum temperature 160 and 165°C, and time at maximum temperature 60~110 min) and pulp properties (kappa number and yield). Results indicated that in order to obtain relatively low kappa numbers(17~27), high sulfidity(20~40%) at lower EA(14~16%) increased pulp yield compared to the case of low sulfidity(0~10%) at higher EA(16~18%). Pulp with lower kappa numbers (13~15) and acceptable yield can be obtained at a sulfidity level of 20~30% with 18% EA or at a sulfidity level of 10~30% with 20% EA. Meanwhile, bamboo pulp in this condition not only helps to decrease kappa number in the subsequent oxygen delignification process, but also reduces the cost of chemicals in the bleaching process.

Application of Diethylene Triamine Penta Methylene Phosphonic Acid in Bamboo Pulping

2012 ◽  
Vol 550-553 ◽  
pp. 3331-3334
Author(s):  
Hong Xia Gao
Keyword(s):  
Phosphonic Acid ◽  
Kappa Number ◽  
Diethylene Triamine ◽  
Bamboo Pulp ◽  
Kraft Cooking ◽  
Pulp Properties

The effect of Diethylene Triamine Penta Methylene Phosphonic Acid in bamboo kraft cooking was studied. The results show that the bamboo pulp properties are optimal when DTPMPA dosage is 0.4%. The optimal properties are as follows: the kappa number is 16.4, brightness is 37.8%, and the screened yield is 41.9%.

scholarly journals Xylanase pretreatment of mechanically destructured chips of Eucalyptus tereticornis and its effect on kraft pulping

BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 5361-5375
Author(s):  
Laxman Kumar Pandey ◽  
Amit Kumar ◽  
Surendra Pal Singh ◽  
Dharm Dutt
Keyword(s):  
Treated Wood ◽  
Untreated Wood ◽  
Strength Properties ◽  
Kraft Pulping ◽  
Kappa Number ◽  
Wood Chips ◽  
Pulp Yield ◽  
Physical Strength ◽  
Cooking Temperature ◽  
Combined Pretreatment

Mechanical pulping of raw wood material is a highly energy intensive and pollution generating step in the papermaking process. This study focused on combined mechanical and xylanase treatment prior to the kraft pulping of E. tereticornis. A screened pulp yield of 49.1% (on oven-dry wood basis) with a Kappa number of 24.9 was obtained at the optimum cooking temperature of 160 °C without any pretreatment of the wood chips. After mechanical treatment (destructuring), a slightly higher screened pulp yield (49.4%) was obtained with a Kappa number of 24.2 at the cooking temperature of 145 °C with the same active alkali charge (15%). The optimum cooking temperature was further reduced to 140 °C for the destructured xylanase-treated wood chips. The xylanase treatment resulted in a 2% reduction in screened pulp yield due to hydrolysis of xylan. However, the Kappa number was reduced to 18.2 after xylanase pretreatment of the mechanically destructured wood chips. The combined pretreatment (destructured and xylanase treatment) of wood chips resulted in a reduction in cooking temperature by 20°C compared to untreated wood chips. Such a reduction in cooking temperature can effectively reduce steam consumption. The combined pretreatment improved the pulp brightness by 2.0 (ISO points) and physical strength properties, which included the tensile index, tear index, and burst index by 11.06%, 21.72%, and 21.79%, respectively, compared to the control.

Prehydrolysis kraft pulping of jute cutting and caddis mixture for rayon production

TAPPI Journal ◽  
2019 ◽  
Vol 18 (5) ◽  
pp. 287-293 ◽  
Author(s):  
JANNATUN NAYEEM ◽  
M. SARWAR JAHAN ◽  
RAZIA SULTANA POPY ◽  
M. NASHIR UDDIN ◽  
M.A. QUAIYYUM
Keyword(s):  
Kraft Pulping ◽  
Kappa Number ◽  
Pulp Yield ◽  
Solid Residue ◽  
Rayon Production ◽  
Kraft Cooking ◽  
Prehydrolysis Kraft

Jute cutting, jute caddis, and cutting-caddis mixtures were prehydrolyzed by varying time and temperature to get about 90% prehydrolyzed yield. At the conditions of 170°C for 60 min of prehydrolysis, the yield for 100% jute cutting was 76.3%, while the same for jute caddis was only 67.9%. But with prehydrolysis at 150°C for 60 min, the yield was 90% for jute cutting, where 49.94% of original pentosan was dissolved and prehydrolysis of jute caddis at 140°C in 60 min yielded 86.4% solid residue. Jute cutting-caddis mixed prehydrolysis was done at 140°C for 30 min and yielded 92% solid residue for 50:50 cutting-caddis mixtures, where pentosan dissolution was only 29%. Prehydrolyzed jute cutting, jute caddis, and cutting-caddis mixtures were subsequently kraft cooked. Pulp yield was only 40.9% for 100% jute cutting prehydrolyzed at 170°C for 60 min, which was 10.9% lower than the prehydrolysis at 140°C. For jute cutting-caddis mixed prehydrolysis at 140°C for 45 min followed by kraft cooking, pulp yield decreased by 3.3% from the 100% cutting to 50% caddis in the mixture, but 75% caddis in the mixture decreased pulp yield by 6.7%. The kappa number 50:50 cutting-caddis mixture was only 11.3. Pulp bleachability improved with increasing jute cutting proportion in the cutting-caddis mixture pulp.

Kraft pulping and bleaching of Eichhornia crassipes (Mart.) Solms (water hyacinth)

BioResources ◽  
2020 ◽  
Vol 15 (4) ◽  
pp. 9243-9264
Author(s):  
Luis Fernando Pintor-Ibarra ◽  
José de Jesús Rivera-Prado ◽  
Sarai Ramos-Vargas ◽  
Teófilo Escoto-García ◽  
Nancy Eloisa Rodríguez-Olalde ◽  
...  
Keyword(s):  
Water Hyacinth ◽  
Eichhornia Crassipes ◽  
Kraft Pulping ◽  
Kappa Number ◽  
Pulp Yield ◽  
Inorganic Elements ◽  
Wood Fibers ◽  
Pulp Bleaching ◽  
Cellulosic Pulp ◽  
Unbleached Pulp

Eichhornia crassipes (water hyacinth) was pulped by means of a kraft pulping process with reagent loads of 10 and 20% on a dry matter basis to determine yield, rejects, kappa number, and ash. Fiber classification, brightness, opacity, and viscosity were measured in the brown pulp. Bleaching was performed by means of an O1O2D1(PO)D2HD3 sequence. Yield, kappa number, pH, ash, brightness, opacity, and viscosity were evaluated in the bleached pulp. Finally, a microanalysis of inorganic elements was carried out in both the bleached and unbleached pulp ash. The highest kraft pulp yield was 26.4%, with a 10% reagent load at 120 °C and 30 minutes cooking. It was determined that E. crassipes cellulosic pulp contains large amounts of fines. Results of the bleaching sequence indicate low brightness (58.0 %) and low viscosity (6.43 cP). The most abundant inorganic elements in the ash of both bleached and unbleached pulp were Ca, Mg, P, and Si. These results suggest that E. crassipes biomass might complement cellulosic fibers in pulping processes of low yield, such as the wood fibers used to produce handmade paper.

scholarly journals Ozone Oxidation of Kraft Bamboo Pulp for Preparation of Nanofibrillated Cellulose

2018 ◽  
Vol 2018 ◽  
pp. 1-7 ◽  
Author(s):  
Mingyou Liu ◽  
Xia Chen ◽  
Xiaofei Tian
Keyword(s):  
Aspect Ratio ◽  
Nanofibrillated Cellulose ◽  
Kappa Number ◽  
Efficient Production ◽  
Bamboo Pulp ◽  
Alternative Approach ◽  
Carboxylate Content ◽  
Pulp Consistency ◽  
20 Nm ◽  
Optimized Conditions

The influence of ozonation on the homogenization of Kraft bamboo pulp (KBP) for the production of nanofibrillated cellulose (NFC) was studied. Using optimized conditions for ozonation, that is, pulp consistency 35%, ozone dosage 0.87% (v/w), and pH=2.5, the kappa number and viscosity of KBP decreased from 10.8 to 2.8 and from 1024 mL∙g−1 to 258 mL∙g−1, respectively, while the crystallinity and carboxylate content increased from 36.2% to 48% and 0.93 mmol/g to 1.26 mmol/g, respectively. The ozonation-treated KPB was used as the substrate for NFC preparation through homogenization. With a width of 10–20 nm and length≥250 nm, the prepared NFC had a high aspect ratio of length versus width. Ozonation can be used as an alternative approach to promote the efficient production of NFC from KBP.

Optimization of soda pulping process of ligno-cellulosic residues of lemon and sofia grasses produced after steam distillation

BioResources ◽  
2010 ◽  
Vol 6 (1) ◽  
pp. 103-120
Author(s):  
Harjeet Kaur ◽  
Dharm Dutt ◽  
C. H. Tyagi
Keyword(s):  
Steam Distillation ◽  
Strength Properties ◽  
Kappa Number ◽  
Pulp Yield ◽  
Lemon Grass ◽  
Cymbopogon Flexuosus ◽  
Cooking Temperature ◽  
Soda Pulping ◽  
Lignocellulosic Residue ◽  
Better Than

Sofia (Cymbopogon martini), and lemon (Cymbopogon flexuosus) grasses, are exclusively cultivated for extraction of important lemongrass and palma rosa oils. Lignocellulosic residue (LCR) of sofia and lemon grasses left after steam distillation can successfully be used for the production of chemical grade pulp. Steam distillation mitigates the problem of mass transfer, and facilitates the faster penetration of cooking liquor by leaching out a part of extraneous components. Sofia grass produces a pulp yield of 43.7% of kappa number 20 at an active alkali dose of 14% (as Na2O), maximum cooking temperature of 160 oC and cooking time 90 min. Likewise, lemon grass produces a pulp yield of 41.4% of kappa number 12.5 under the same conditions except temperature (150 oC) by a soda pulping process. Addition of 0.1% AQ at optimum cooking conditions reduces kappa number by 26 and 8% for sofia and lemon grasses with insignificant increase in pulp yield i.e. 0.2 and 0.4% for sofia and lemon grasses, respectively. The mechanical strength properties of lemon grass soda-AQ pulp are better than sofia grass. Bauer-McNett fiber classification further validates that +20 fractions are more (62.63%) in lemon grass than in sofia grass (42.72%).

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