Study on Optimization of Cationic Resin Regeneration Conditions

2014 ◽  
Vol 997 ◽  
pp. 851-857
Author(s):  
Ding Hui Fan ◽  
Li Yin ◽  
Jie Liu ◽  
Wei Min Cao ◽  
Zu Yu Liu
Keyword(s):  
Cation Exchange ◽  
Exchange Resin ◽  
Cation Exchange Resin ◽  
Economic Benefits ◽  
Least Square ◽  
Feeding Time ◽  
Cationic Resin ◽  
Acid Consumption ◽  
Regeneration Condition ◽  
Resin Regeneration

In order to optimize the regeneration conditions of cation exchange resin, the paper based on the actual data of production, the cation exchange resin regeneration condition was optimized by the process of mathematical modeling, which achieved good results. Research showed that reducing regeneration acid feeding time could effectively reduce the consumption. It could reduce the production cost and make enterprises obtain more economic benefits. Calculated and measured were agreed showed that the study and calculation on regeneration of cation bed were accord with actual production, and had practical value for ion regeneration process. Through least square fitting showed that the 80min was the best acid feeding time, acid consumption of unit volume of water was the lowest.

Synthesis of 3,4-Dihydropyrano[c]chromenes Using Carbon Microsphere Supported Copper Nanoparticles (Cu-NP/C) Prepared from Loaded Cation Exchange Resin as a Catalyst

2019 ◽  
Vol 16 (2) ◽  
pp. 288-293
Author(s):  
Yogesh W. More ◽  
Sunil U. Tekale ◽  
Nitishkumar S. Kaminwar ◽  
László Kótai ◽  
Tibor Pasinszki ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Cation Exchange ◽  
Copper Nanoparticles ◽  
Exchange Resin ◽  
Cation Exchange Resin ◽  
Environmentally Benign ◽  
High Yield ◽  
Carbon Microsphere ◽  
Catalytic Material ◽  
Operational Simplicity

Aim and Objective: The present study was performed with the aim to develop an efficient and environmentally benign protocol for the synthesis of biologically siginifcant 3, 4-dihydropyrano[c]chromenes using a new catalytic material. The protocol involves the use of a reusable, environment friendly materials and solvents with operational simplicity. Materials and Methods: Carbon microsphere supported copper nanoparticles (Cu-NP/C) prepared from loaded cation exchange resin were synthesized, characterized with well versed analytical techniques such as XRD, SEM and Raman spectroscopy and the synthesized material was used as a catalyst for the environmentally benign synthesis of 3,4-dihydropyrano[c]chromenes. Results: The formation of carbon microsphere supported copper nanoparticles (Cu-NP/C) prepared from loaded cation exchange resin was confirmed by XRD, SEM and Raman spectroscopy which was employed as a heterogeneous material for the synthesis of 3,4-dihydropyrano[c]chromenes. The products formed were characterized by the analysis of spectroscopic data - NMR, IR and mass. The safe catalytic system offers several advantages including operational simplicity, environmental friendliness, high yield, and reusability of catalyst and green chemical transformation. Conclusion: Herein we report an easy and efficient protocol for the one-pot synthesis of dihydropyrano[ c]chromenes using environmentally benign MCR approach in ethanol as the green solvent. The method developed herein constitutes a valuable addition to the existing methods for the synthesis of titled compounds.

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