Electrophoretic Deposition of Nanostructured Titania-Bioactive Glass/Alginate Coatings on Stainless Steel

2015 ◽  
Vol 654 ◽  
pp. 159-164 ◽  
Author(s):  
Luis Cordero-Arias ◽  
Sandra Cabanas-Polo ◽  
Sannakaisa Virtanen ◽  
Aldo Roberto Boccaccini

An alginate (Alg) based coating containing nanoparticles of titania (nTiO2) and bioactive glass 45S5 (nBG) was deposited on stainless steel substrates by electrophoretic deposition (EPD). The composite nTiO2-nBG/Alg coating developed for potential biomedical applications, was produced from a stable ethanol/water suspension (ζ–potential of-53±13mV) using 7V of deposition potential and 1min of deposition time as optimal conditions. Morphology and composition of the coatings were studied by FTIR, EDX, SEM and XRD, showing that all components were successfully deposited on the final coating. According to TG analysis the coatings presents a 62.4wt% of ceramic phase and 37.6wt% polymer. The coating shows corrosion protection properties compared with the bare uncoated material when analyzed via polarization curves in Dulbecco ́s MEM.

2012 ◽  
Vol 507 ◽  
pp. 127-133 ◽  
Author(s):  
Sigrid Seuss ◽  
Tayyab Subhani ◽  
Min Yi Kang ◽  
Kenji Okudaira ◽  
Isaac E. Aguilar Ventura ◽  
...  

Electrophoretic deposition (EPD) has been successfully used to deposit composite coatings composed of polyetheretherketone (PEEK) and titanium dioxide (TiO2) nanoparticles on 316L stainless steel substrates. The suspensions of TiO2 nanoparticles and PEEK microparticles for EPD were prepared in ethanol. PEEK-TiO2 composite coatings were optimized using suspensions containing 6wt% PEEK-TiO2 in ethanol with a 3:1 ratio of PEEK to TiO2 in weight and by applying a potential difference of 30 V for 1 minute. A heat-treatment process of the optimized PEEK-TiO2 composite coatings was performed at 335°C for 30 minutes with a heating rate of 10°Cminto densify the deposits. The EPD coatings were microstructurally evaluated by scanning electron microscopy (SEM). It was demonstrated that EPD is a convenient and rapid method to fabricate PEEK/TiO2 coatings on stainless steel which are interesting for biomedical applications.


Surfaces ◽  
2020 ◽  
Vol 3 (2) ◽  
pp. 237-250 ◽  
Author(s):  
Yusra Ahmed ◽  
Muhammad Yasir ◽  
Muhammad Atiq Ur Rehman

Stainless steel is renowned for its wide use as a biomaterial, but its relatively high corrosion rate in physiological environments restricts many of its clinical applications. To overcome the corrosion resistance of stainless steel bio-implants in physiological environments and to improve its osseointegration behavior, we have developed a unique zein/hydroxyapatite (HA) composite coating on a stainless steel substrate by Electrophoretic Deposition (EPD). The EPD parameters were optimized using the Taguchi Design of experiments (DoE) approach. The EPD parameters, such as the concentration of bio-ceramic particles in the polymer solution, applied voltage and deposition time were optimized on stainless steel substrates by applying a mixed design orthogonal Taguchi array. The coatings were characterized by using scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX) and wettability studies. SEM images and EDX results indicated that the zein/HA coating was successfully deposited onto the stainless steel substrates. The wettability and roughness studies elucidated the mildly hydrophilic nature of the zein/HA coatings, which confirmed the suitability of the developed coatings for biomedical applications. Zein/HA coatings improved the corrosion resistance of bare 316L stainless steel. Moreover, zein/HA coatings showed strong adhesion with the 316L SS substrate for biomedical applications. Zein/HA developed dense HA crystals upon immersion in simulated body fluid, which confirmed the bone binding ability of the coatings. Thus the zein/HA coatings presented in this study have a strong potential to be considered for orthopedic applications.


Coatings ◽  
2017 ◽  
Vol 7 (11) ◽  
pp. 199 ◽  
Author(s):  
Kyotaro Kawaguchi ◽  
Masahiro Iijima ◽  
Kazuhiko Endo ◽  
Itaru Mizoguchi

2001 ◽  
Vol 70 (3) ◽  
pp. 269-275 ◽  
Author(s):  
German P. Hernandez ◽  
Xavier Mathew ◽  
J.Pantoja Enriquez ◽  
N.R. Mathews ◽  
P.J. Sebastian

2013 ◽  
Vol 113 (1) ◽  
pp. 42-49 ◽  
Author(s):  
L. Cordero-Arias ◽  
S. Cabanas-Polo ◽  
J. Gilabert ◽  
O. M. Goudouri ◽  
E. Sanchez ◽  
...  

2018 ◽  
Vol 344 ◽  
pp. 553-563 ◽  
Author(s):  
Svenja Heise ◽  
Tobias Wirth ◽  
Michael Höhlinger ◽  
Yadir Torres Hernández ◽  
Jose Antonio Rodriquez Ortiz ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-7 ◽  
Author(s):  
Bizuneh Workie ◽  
Brian E. McCandless ◽  
Zewdu Gebeyehu

We have studied electrophoretic deposition of AlN from its suspension in acetylacetone with I2as an additive. AlN powder with particle size <10 μm is dispersed to produce a positive charge and deposited on the cathode by applying fields greater than 10 V/cm between the electrodes. X-ray diffraction and FTIR studies indicate that the AlN before and after deposition has the same composition and structure. An increase in the amount of AlN in the suspension, the deposition potential, and the deposition time results in a linear increase in the weight of the AlN deposited. Electrophoretic deposition from 10 g/L AlN suspension shows an initial increase in the weight of AlN deposited with the concentration of I2, and the weight of AlN decreases after reaching a maximum at 0.20 g/L I2.


2010 ◽  
Vol 139-141 ◽  
pp. 145-148 ◽  
Author(s):  
Hamimah Abd Rahman ◽  
Andanastuti Muchtar ◽  
Norhamidi Muhamad ◽  
Huda Abdullah

2014 ◽  
Vol 40 (6) ◽  
pp. 7879-7888 ◽  
Author(s):  
Ramin Rojaee ◽  
Mohammadhossein Fathi ◽  
Keyvan Raeissi ◽  
Mohamadhassan Taherian

Sign in / Sign up

Export Citation Format

Share Document