Technology of Ti-Al-Nb Obtaining by Use of Spark Plasma Sintering Method

2017 ◽  
Vol 743 ◽  
pp. 41-44
Author(s):  
Ernat Kozhahmetov ◽  
Batyrzhan Karakozov ◽  
Sherzod Rustambekovich Kurbanbekov
Keyword(s):  
Spark Plasma Sintering ◽  
Phase Changes ◽  
Effective Control ◽  
Optimal Regime ◽  
Plasma Sintering ◽  
Diffusion Controlled ◽  
Spark Plasma ◽  
New Type ◽  
Sintering Method ◽  
Resistance To Heat

This method grants effective control of the porosity of the sintering materials and ability to obtain compactly packed samples, where simple pressing is not feasible. Spark plasma sintering is one of the probable methods that could lead to larger energy efficiency in material manufacturing. Upon use of SPS, there is no need to “pre-heat” the material by use of pressure or additional use of connecting agents or components. Manufacture of the components is being finished at the instant. Initial microstructure of the powder is being saved. Besides, with use of analyzing method, it is possible to obtain material of the new type, ones that are have resistance to heat. Use of SPS technology could imply lesser time of sintering for highly packed specimens. Decrease of time implies decrease of microstructural changes as a result of diffusion controlled phase changes. Taking into account what has been mentioned above, choosing the best suitable regime for Ti-Al-Nb proposes a variety of intermetallic junctions and could be used for creation of alloys with different physical-mechanical properties. This study concentrates on optimal regime of obtaining intermetallic junction based on Ti-Al-Nb with use of spark plasma sintering.

Preparation of MoSi2-SiB6 oxidation inhibition coating on graphite by spark plasma sintering method

2021 ◽  
Vol 405 ◽  
pp. 126511
Author(s):  
Weisheng Liu ◽  
Xuanru Ren ◽  
Hongao Chu ◽  
Menglin Zhang ◽  
Qingqing Yang ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method

scholarly journals Fabrication of ZnO Ceramics with Defects by Spark Plasma Sintering Method and Investigations of Their Photoelectrochemical Properties

Nanomaterials ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 2506
Author(s):  
Liren Zheng ◽  
Mu Liu ◽  
Haipeng Zhang ◽  
Zhaoke Zheng ◽  
Zeyan Wang ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Oxygen Vacancies ◽  
Photoelectrochemical Properties ◽  
Interstitial Zinc ◽  
Photoelectric Properties ◽  
Oxygen Defects ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method ◽  
Zno Ceramics

ZnO, as an important semiconductor material, has attracted much attention due to its excellent physical properties, which can be widely used in many fields. Notably, the defects concentration and type greatly affect the intrinsic properties of ZnO. Thus, controllable adjustment of ZnO defects is particularly important for studying its photoelectric properties. In this work, we fabricated ZnO ceramics (ZnO(C)) with different defects through spark plasma sintering (SPS) process by varying sintering temperature and using reduction environment. The experimental results indicate that the changes of color and light absorption in as-prepared ZnO originate from the different kinds of defects, i.e., oxygen vacancies (VO), interstitial zinc (Zni), and Zinc vacancies (VZn). Moreover, with the increase in calcination temperature, the concentration of oxygen defects and interstitial zinc defects in the ceramics increases gradually, and the conductivity of the ceramics is also improved. However, too many defects are harmful to the photoelectrochemical properties of the ceramics, and the appropriate oxygen defects can improve the utilization of visible light.

Biodegradable Fiber Reinforced Ti Composite Fabricated by Spark Plasma Sintering Method

2007 ◽  
pp. 3201-3206
Author(s):  
Hisashi Sato ◽  
Seiichiro Umaoka ◽  
Yoshimi Watanabe ◽  
Ick Soo Kim ◽  
Masakazu Kawahara ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Fiber Reinforced ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Sintering Method

scholarly journals Microstructure Evolution of Mg96.9Gd2.7Zn0.4 Alloy Containing Multiple Phases Prepared by Spark Plasma Sintering Method

Metals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1355
Author(s):  
Zhiyong Xue ◽  
Xiuzhu Han ◽  
Wenbo Luo ◽  
Zhiyong Zhou ◽  
Zhizhong Cheng ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Rapid Solidification ◽  
High Performance ◽  
Aging Treatment ◽  
Lpso Phase ◽  
Β Phase ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Molten Liquid ◽  
Sintering Method

The synergic strengthening of multiple phases is an essential way to achieve high-performance Mg alloys. Herein, Mg-Gd-Zn alloy containing four phases was prepared by rapid solidification (RS) ribbons and spark plasma sintering (SPS). The microstructure of the alloy consisted of α-Mg, nanosized β1 phase particles, lamellar long period stacking ordered (LPSO) phase, and β′ phase precipitates. The microstructural evolution was also investigated. The results show that the metastable β1 phase was formed in the as-cast solidification through rapid solidification, because both Zn atoms and the short holding-time at molten liquid facilitated the formation of the β1 phase. The β1 phase grew from 35.6 to 154 nm during the sintering process. Meanwhile, the fine lamellar LPSO phase was simultaneously formed after the Zn-Gd clusters were generated from the supersaturated solid solution, and the width of the LPSO phase was only in the range of 2–30 nm. The third strengthening phase, the metastable β′ phase, was obtained by aging treatment. The results of hardness testing implied that the hardness of the alloy containing the aforementioned three nanosized strengthening phases significantly improved about 47% to 126 HV compared with that of the as-cast ingot.

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