Deformation Features of a High Mo Nickel-Based Single Crystal Superalloy during Creep at High Temperature

2019 ◽  
Vol 795 ◽  
pp. 35-42
Author(s):  
Hua Jin Yan ◽  
Su Gui Tian ◽  
Guo Qi Zhao ◽  
Shun Ke Zhang

The deformation and damage features of a high Mo single crystal Ni-based superalloy during creep at high temperature are investigated by means of measuring creep properties and observing microstructure. Results show that, compared to 4%Mo single crystal nickel-based superalloy, the 6%Mo superalloy displays a better creep resistance, and the creep life of 6%Mo single crystal superalloy at 1040°C/137MPa is measured to be 556 h. In the ranges of applied temperatures and stresses, the creep activation energy of the alloy is measured to be 484.7kJ/mol. Wherein, the deformation mechanisms of the 6%Mo superalloy during steady state creep are dislocations slipping in ϒ matrix and climbing over the rafted ϒ' phase. In the later stage of creep, the deformation mechanism of alloy is dislocations shearing into the rafted ϒ' phase, the alternate activation of dislocations slipping results in the twisted of the rafted ϒ'/ϒ phases, as the creep goes on, to promote the initiation and propagation of cracks along the interface of the twisted ϒ/ϒ' phase perpendicular to the stress axis, up to creep fracture, which is thought to be the damage and fracture features of the alloy during creep at high temperature.

2019 ◽  
Vol 795 ◽  
pp. 123-129
Author(s):  
Guo Qi Zhao ◽  
Su Gui Tian ◽  
Shun Ke Zhang ◽  
Ning Tian ◽  
Li Rong Liu

By means of creep properties measurement, microstructure observation and contrast analysis of dislocation configuration, the creep behavior of a 4.5%Re/3.0%Ru-containing single crystal nickel-based superalloy at elevated temperature is investigated. Results show that the creep life of the alloy at 1040°C/160MPa is measured to be 725h to exhibit a better creep resistance at high temperature. In the primary stage of creep at high temperature, the γ phase in alloy has transformed into the N-type rafted structure along the direction vertical to the stress axis, the deformation mechanism of alloy during steady state creep is dislocations slipping in γ matrix and climbing over the rafted γ phase. In the latter period of creep, the deformation mechanism of alloy is dislocations slipping in γ matrix and shearing into the rafted γ phase. Wherein the dislocations shearing into the γ phase may cross-slip from {111} to {100} planes for forming the K-W locks to restrain the slipping and cross-slipping on {111} plane, which is thought to be the main reason of the alloy having a better creep resistance. As the creep goes on, the alternate slipping of dislocations results in the twisted of the rafted γ phase to promote the initiation and propagation of the cracks along the interfaces of γ/γ phase up to creep fracture, which is thought to be the damage and fracture mechanism of alloy during creep at high temperature.


2015 ◽  
Vol 750 ◽  
pp. 139-144 ◽  
Author(s):  
De Long Shu ◽  
Su Gui Tian ◽  
Xin Ding ◽  
Jing Wu ◽  
Qiu Yang Li ◽  
...  

By means of heat treatment and creep property measurement, an investigation has made into the creep behaviors of a containing 4.5% Re nickel-base single crystal superalloy at high temperature. Results show that the elements W, Mo and Re are enriched in the dendrite arm regions, the elements Al, Ta, Cr and Co are enriched in the inter-dendrite region, and the segregation extent of the elements may be obviously reduced by means of heat treatment at high temperature. In the temperature ranges of 1070--1100 °C, the 4.5% Re single crystal nickel-based superallloy displays a better creep resistance and longer creep life. The deformation mechanism of the alloy during steady state creep is dislocations slipping in the γ matrix and climbing over the rafted γ′ phase. In the later stage of creep, the deformation mechanism of alloy is dislocations slipping in the γ matrix, and shearing into the rafted γ′ phase, which may promote the initiation and propagation of the micro-cracks at the interfaces of γ/γ′ phases up to the occurrence of creep fracture.


2018 ◽  
Vol 720 ◽  
pp. 69-74 ◽  
Author(s):  
YuZhang Lu ◽  
Guang Xie ◽  
Dong Wang ◽  
ShaoHua Zhang ◽  
Wei Zheng ◽  
...  

2014 ◽  
Vol 788 ◽  
pp. 459-465 ◽  
Author(s):  
De Long Shu ◽  
Su Gui Tian ◽  
Jing Wu ◽  
Zhong Ge Guo

The deformation and damage behaviors of a 4.5% Re nickel-based single crystal superalloy during creep at medium temperature were conducted by means of creep properties measurement and microstructure observation in the present investigation. The results show that the creep life of the superalloy was measured to be 226h at 820MPa/820oC, displaying a better creep resistance. After the alloy crept up to fracture, the γ′ phase in the region near fracture was contorted and coarsened, which is attributed to the severe plastic deformation. In the latter stage of creep, the main/secondary slipping systems were alternately activated to twist the γ′ and γ phases, which promoted the initiation of the cracks along the interfaces of γ′ /γ phases. And the micro-cracks may be propagated both along the direction vertical to the stress axis and along the direction of slipping traces, which is thought to be the main deformation and fracture mechanisms of the alloy in the latter stage of the creep.


2014 ◽  
Vol 788 ◽  
pp. 466-472 ◽  
Author(s):  
Shuang Liang ◽  
Su Gui Tian ◽  
Zhong Ge Guo ◽  
Yong Chao Xue ◽  
De Long Shu

The creep behavior of a Re-free single crystal Ni-base superalloy at high temperature has been investigated by means of creep property measurement and microstructure observation. The experimental results show that the creep life of the alloy under the testing condition of 1040 oC/137 MPa was measured to be 556h. In the primary stage of creep, the deformation mechanism of the alloy is dislocations slipping within the γ matrix, and the γ′ phase in the alloy is transformed into the rafted structure along the direction vertical to the stress axis. In the latter stage of creep, the alternate activation of the main/secondary slipping dislocations may twist the rafted γ′ phase to promote the initiation and propagation of the cracks along the interfaces of γ′/γ phases up to the creep fracture. And the various configurations of the rafted γ′ phase appeared in the different regions of the sample, thereinto, the coarsening and twisting of the rafted γ′ phase in the regions near the fracture may be attributed to the bigger plastic deformation.


2014 ◽  
Vol 783-786 ◽  
pp. 1188-1194 ◽  
Author(s):  
Su Gui Tian ◽  
Zhong Ge Guo ◽  
De Long Shu ◽  
Jun Xie

By means of creep properties measurement and microstructure observation, an investigation has been made into the damage and fracture mechanism of a nickel-based single crystal superalloy during creep at moderate temperature. Results show that the deformation mechanism of the alloy in the latter stage of creep is that the primary-secondary slipping systems are alternately activated, and the micro-crack is firstly initiated on the γ′/γ phases interface in the intersection regions of two slip systems. As creep goes on, the micro-crack is propagated along the γ′/γ interface, which is perpendicular to stress axis, to form the square-like cleavage plane on the (001) plane. Thereinto, the propagation of the cracks on (001) plane is intersected with {111} cleavage plane which is secondly activated, which may terminate the propagation of the crack to form the cleavage plane with square-like feature on (001) plane along the <110> directions. Due to the multi-cracks may be propagated on different cross-section of the alloy during creep, and the tearing edge or secondary cleavage plane are formed along the direction with bigger shearing stress at the crack tip, which makes the multi-cracks connected each other until the occurrence of creep fracture, this is thought to be the main reason of the creep fracture having the uneven and multi-level cleavage characteristics.


China Foundry ◽  
2021 ◽  
Vol 18 (3) ◽  
pp. 185-191
Author(s):  
Xu-dong Wang ◽  
Zhong Yang ◽  
Qiang Gao ◽  
Li-rong Liu

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