Creep Damage of a Re/Ru-Containing Single Crystal Nickel-Based Superalloy at Elevated Temperature

2019 ◽  
Vol 795 ◽  
pp. 123-129
Author(s):  
Guo Qi Zhao ◽  
Su Gui Tian ◽  
Shun Ke Zhang ◽  
Ning Tian ◽  
Li Rong Liu

By means of creep properties measurement, microstructure observation and contrast analysis of dislocation configuration, the creep behavior of a 4.5%Re/3.0%Ru-containing single crystal nickel-based superalloy at elevated temperature is investigated. Results show that the creep life of the alloy at 1040°C/160MPa is measured to be 725h to exhibit a better creep resistance at high temperature. In the primary stage of creep at high temperature, the γ phase in alloy has transformed into the N-type rafted structure along the direction vertical to the stress axis, the deformation mechanism of alloy during steady state creep is dislocations slipping in γ matrix and climbing over the rafted γ phase. In the latter period of creep, the deformation mechanism of alloy is dislocations slipping in γ matrix and shearing into the rafted γ phase. Wherein the dislocations shearing into the γ phase may cross-slip from {111} to {100} planes for forming the K-W locks to restrain the slipping and cross-slipping on {111} plane, which is thought to be the main reason of the alloy having a better creep resistance. As the creep goes on, the alternate slipping of dislocations results in the twisted of the rafted γ phase to promote the initiation and propagation of the cracks along the interfaces of γ/γ phase up to creep fracture, which is thought to be the damage and fracture mechanism of alloy during creep at high temperature.

2019 ◽  
Vol 795 ◽  
pp. 35-42
Author(s):  
Hua Jin Yan ◽  
Su Gui Tian ◽  
Guo Qi Zhao ◽  
Shun Ke Zhang

The deformation and damage features of a high Mo single crystal Ni-based superalloy during creep at high temperature are investigated by means of measuring creep properties and observing microstructure. Results show that, compared to 4%Mo single crystal nickel-based superalloy, the 6%Mo superalloy displays a better creep resistance, and the creep life of 6%Mo single crystal superalloy at 1040°C/137MPa is measured to be 556 h. In the ranges of applied temperatures and stresses, the creep activation energy of the alloy is measured to be 484.7kJ/mol. Wherein, the deformation mechanisms of the 6%Mo superalloy during steady state creep are dislocations slipping in ϒ matrix and climbing over the rafted ϒ' phase. In the later stage of creep, the deformation mechanism of alloy is dislocations shearing into the rafted ϒ' phase, the alternate activation of dislocations slipping results in the twisted of the rafted ϒ'/ϒ phases, as the creep goes on, to promote the initiation and propagation of cracks along the interface of the twisted ϒ/ϒ' phase perpendicular to the stress axis, up to creep fracture, which is thought to be the damage and fracture features of the alloy during creep at high temperature.


2011 ◽  
Vol 689 ◽  
pp. 276-281 ◽  
Author(s):  
Su Gui Tian ◽  
Ben Jiang Qian ◽  
Fu Shun Liang ◽  
An An Li ◽  
Xing Fu Yu

By the measurement of creep curves and microstructure observation, an investigation has been made into the creep behaviors and microstructure evolution of a single crystal nickel-based superalloy containing 4.2%Re. Results show that the superalloy displays an obvious sensibility on the applied temperatures and stresses in the range of the applied temperatures and stresses. During the initial creep, the cubical g¢ phase in the alloy is transformed into an N-type rafted structure along the direction vertical to the applied stress axis. After crept up to fracture, the rafted g¢ phase in the region near fracture is transformed into a twisted configuration. The dislocation climbing over the rafted g¢ phase is considered to be the main deformation mechanism of the alloy during the steady creep state, and dislocations shear into the rafted g¢ phase is the main deformation mechanism of the alloy in the later stage of creep.


Crystals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 646
Author(s):  
Jiachun Li ◽  
Ning Tian ◽  
Ping Zhang ◽  
Fang Yu ◽  
Guoqi Zhao ◽  
...  

Through creep performance tests, microstructural observations, and contrast analysis of the dislocation configuration, the deformation and damage mechanism of the directionally solidified nickel-based superalloy during creep at moderate temperatures was investigated. The findings suggested that the deformation of the alloy in the late stage of creep at moderate temperatures involved dislocations slipping in the γ matrix and shearing into the γ′ phase. The super-dislocations sheared into the γ′ phase could either be decomposed to form a <112> super-Shockley incomplete dislocation plus superlattice intrinsic stacking fault (SISF) configuration, or it could slip from the {111} plane to the {100} plane and decompose to form a dislocation configuration of the Kear–Wilsdorf (K-W) lock plus antiphase domain boundary (APB). The configurations of the dislocations could inhibit the slipping and cross-slipping of dislocations to enhance the alloy creep strength, which is thought to be one reason that the alloy displayed good creep resistance. In the late creep stage, the primary/secondary slipping systems were alternately activated, and the interaction of the slipping traces caused micro-holes to appear on the interface of the γ/γ′ phases at the intersection areas of the two slipping systems. The micro-holes gathered and grew to form micro-cracks, which extended along the grain boundary at 45° to the stress axis until creep rupture occurred. These were the damage and fracture characteristics of the alloy in the late stage of creep at moderate temperatures.


2012 ◽  
Vol 706-709 ◽  
pp. 2474-2479 ◽  
Author(s):  
Su Gui Tian ◽  
Ben Jiang Qian ◽  
Yong Su ◽  
Hui Chen Yu ◽  
Xing Fu Yu

By means of calculating stacking fault energy (SFE), measuring creep properties and contrast analysis of dislocation configuration, an investigation has been made into the influence of the stacking fault energy on the creep mechanism of the single crystal nickel-based superalloy. Results show that the alloy at 760¡æ has a lower stacking fault energy (SFE), and the SFE of the alloy increases with the temperatures. The deformed mechanism of the alloy during creep at 760¡æ is the cubical γ′ phase sheared by <110> super-dislocation which may be decomposed to form the configuration of (1/3)<112> super-Shockley partials dislocation plus the superlattice intrinsic stacking fault (SISF). The deformed mechanism of the alloy which possesses the higher SFE at 1070¡æ is the screw or edge super-dislocation shearing into the rafted γ′ phase. The SFE of the alloy at 980¡æ is intervenient between the ones of 760¡æ and 1070¡æ, the deformation mechanism of the alloy during creep is the rafted γ′ phase sheared by <110> screw and edge super-dislocations which may be decomposed into the configuration of (1/2)<110> partial dislocation plus APB.


2015 ◽  
Vol 750 ◽  
pp. 139-144 ◽  
Author(s):  
De Long Shu ◽  
Su Gui Tian ◽  
Xin Ding ◽  
Jing Wu ◽  
Qiu Yang Li ◽  
...  

By means of heat treatment and creep property measurement, an investigation has made into the creep behaviors of a containing 4.5% Re nickel-base single crystal superalloy at high temperature. Results show that the elements W, Mo and Re are enriched in the dendrite arm regions, the elements Al, Ta, Cr and Co are enriched in the inter-dendrite region, and the segregation extent of the elements may be obviously reduced by means of heat treatment at high temperature. In the temperature ranges of 1070--1100 °C, the 4.5% Re single crystal nickel-based superallloy displays a better creep resistance and longer creep life. The deformation mechanism of the alloy during steady state creep is dislocations slipping in the γ matrix and climbing over the rafted γ′ phase. In the later stage of creep, the deformation mechanism of alloy is dislocations slipping in the γ matrix, and shearing into the rafted γ′ phase, which may promote the initiation and propagation of the micro-cracks at the interfaces of γ/γ′ phases up to the occurrence of creep fracture.


2012 ◽  
Vol 9 (1) ◽  
pp. 169-171
Author(s):  
Ram Oruganti

When a material is subjected to temperature and stress, it deforms slowly resulting in permanent shape change. If the same amount of stress were applied at room temperature, the material would not budge. This deformation at high temperature under low stresses is called creep. This phenomenon is important for OEM’S like GE etc. since turbine components are exposed to low stress and high temperature and the resulting shape change is not a desirable consequence. Apart from the change in shape, the components can eventually rupture leading to catastrophic consequences. So it is imperative that the nature of this phenomenon is understood well. Some of the questions to be answered are 1) What makes one material more resistant to creep that the other 2) How can a material’s creep resistance be improved 3) How can the current creep damage in a component be measured 4) Is it possible to say what fraction of the total life of a component has been consumed by creep.


2020 ◽  
Vol 37 (2) ◽  
pp. 139-144 ◽  
Author(s):  
Huajin Yan ◽  
Sugui Tian ◽  
Guoqi Zhao ◽  
Shunke Zhang

1992 ◽  
Vol 7 (10) ◽  
pp. 2724-2732 ◽  
Author(s):  
J. Daniel Whittenberger ◽  
Michael J. Luton

Previous studies of a single lot of NiAl powder which had been ground under high intensity conditions in liquid nitrogen (cryomilling) indicated that this processing leads to a high strength, elevated temperature NiAl–AlN composite. Because this was the first known example of the use of the reaction milling process to produce a high temperature composite, the reproducibility of this technique was unknown. Two additional lots of NiAl powder and a lot of a Zr-doped NiAl powder have been cryomilled, and analyses indicate that AlN was formed within a NiAl matrix in all three cases. Compression testing between 1200 K and 1400 K has shown that the deformation resistance of these heats is similar to that of the first lot of NiAl–AlN; thus cryomilling can improve the creep resistance of NiAl by a factor of six. Based on this work, it is concluded that cryomilling of NiAl powder to form high temperature, high strength NiAl–AlN composites is a reproducible process.


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