On the Longtime Stability of a Copper Rolling Texture Analysed by Neutron Diffraction Pole Figures

1998 ◽  
Vol 278-281 ◽  
pp. 502-507
Author(s):  
E. Jansen ◽  
Wolfgang Schäfer ◽  
A. Kirfel ◽  
J. Palacios
Keyword(s):  
Neutron Diffraction ◽  
Rolling Texture ◽  
Pole Figures

scholarly journals The Development of Rolling Texture in α-Brass Determined by Neutron Diffraction

Texture ◽  
1974 ◽  
Vol 1 (4) ◽  
pp. 211-231 ◽  
Author(s):  
J. Tobisch ◽  
A. Mücklichf
Keyword(s):  
Neutron Diffraction ◽  
Three Dimensional ◽  
Rolling Texture ◽  
Orientation Distribution ◽  
Zinc Alloy ◽  
Tube Axis ◽  
Pole Figures ◽  
Cold Rolled

The three-dimensional orientation distribution was calculated from neutron diffraction pole figures for a copper 27.2% zinc alloy cold rolled to different degrees of deformation. The results agree qualitatively with those of other authors. There are however differences in the quantitative respect which influence the conclusions to be drawn. For rolling degrees lower than about 70% the texture exhibits an orientation tube similar to that of the copper type, but with a significantly different distribution along the tube axis. For rolling degrees larger than 70% the texture can be described by the orientation {110}〈112〉. The deformation is assumed to occur according to the Wassermann model and the Hu model respectively in these two ranges.

The development of the rolling texture in copper measured by neutron diffraction

1971 ◽  
Vol 4 (4) ◽  
pp. 303-310 ◽  
Author(s):  
H. J. Bunge ◽  
J. Tobisch ◽  
W. Sonntag
Keyword(s):  
Neutron Diffraction ◽  
Texture Component ◽  
Deformation Mechanism ◽  
Three Dimensional ◽  
Rolling Texture ◽  
Orientation Distribution ◽  
Distribution Functions ◽  
Anisotropic Hardening ◽  
Pole Figures ◽  
Cold Rolled

Three-dimensional orientation distribution functions of the crystallites in copper sheets, cold rolled to different degrees of reduction, have been determined using neutron diffraction pole figures. The main features of the textures may be represented by the orientation `tube' already described in prior publications. Two ranges of rolling reduction can be distinguished, a lower one (30 to 50%) and a higher one (70 to 95%) the texture changes of which correspond to those calculated after the Taylor theory. In an intermediate range (50 to 70%) a different deformation mechanism occurs which leads to an intermediate (001) [110] texture component. It is supposed that anisotropic hardening may have occurred in this range.

Use of Neutron Diffraction for Describing Texture of Isostatically-Pressed Molybdite Powders

2005 ◽  
Vol 105 ◽  
pp. 83-88 ◽  
Author(s):  
H. Sitepu ◽  
Heinz Günter Brokmeier
Keyword(s):  
Crystal Structure ◽  
Neutron Diffraction ◽  
Powder Diffraction ◽  
Quantitative Description ◽  
Neutron Powder Diffraction ◽  
Powder Diffraction Data ◽  
Neutron Powder Diffraction Data ◽  
Pole Figures ◽  
Diffraction Patterns ◽  
Excellent Tool

The modelling and/or describing of texture (i.e. preferred crystallographic orientation (PO)) is of critical importance in powder diffraction analysis - for structural study and phase composition. In the present study, the GSAS Rietveld refinement with generalized spherical harmonic (GSH) was used for describing isostatically-pressed molybdite powders neutron powder diffraction data collected in the ILL D1A instrument. The results showed that for texture in a single ND data of molybdite the reasonable crystal structure parameters may be obtained when applying corrections to intensities using the GSH description. Furthermore, the WIMV method was used to extract the texture description directly from a simultaneous refinement with 1368 whole neutron diffraction patterns taken from the sample held in a variety of orientations in the ILL D1B texture goniometer. The results provided a quantitative description of the texture refined simultaneously with the crystal structure. Finally, the (002) molybdite pole-figures were measured using the GKSS TEX2 texture goniometer. The results showed that neutron diffraction is an excellent tool to investigate the texture in molybdite.

scholarly journals Approximation of the Orientation Distribution of Grains in Polycrystalline Samples by Means of Gaussians

1992 ◽  
Vol 19 (1-2) ◽  
pp. 9-27 ◽  
Author(s):  
D. I. Nikolayev ◽  
T. I. Savyolova ◽  
K. Feldmann
Keyword(s):  
Rolling Texture ◽  
Expansion Method ◽  
Operating Mode ◽  
Orientation Distribution ◽  
New Method ◽  
Gaussian Distributions ◽  
Positivity Condition ◽  
The Central Limit Theorem ◽  
Pole Figures ◽  
Series Expansion Method

The orientation distribution function (ODF) obtained by classical spherical harmonics analysis may be falsified by ghost influences as well as series truncation effects. The ghosts are a consequence of the inversion symmetry of experimental pole figures which leads to the loss of information on the “odd” part of ODF.In the present paper a new method for ODF reproduction is proposed. It is based on the superposition of Gaussian distributions satisfying the central limit theorem in the SO(3)-space as well as the ODF positivity condition. The kind of ODF determination offered here is restricted to the fit of Gaussian parameters and weights with respect to the experimental pole figures. The operating mode of the new method is demonstrated for a rolling texture of copper. The results are compared with the corresponding ones obtained by the series expansion method.

scholarly journals Volume Texture of a Deformed Quartzite Observed With U-Stage Microscopy and Neutron Diffractometry

1999 ◽  
Vol 31 (4) ◽  
pp. 239-248 ◽  
Author(s):  
H. Ghildiyal ◽  
E. Jansen ◽  
A. Kirfel
Keyword(s):  
Neutron Diffraction ◽  
Pole Figure ◽  
North West ◽  
Pole Figures ◽  
Slip Planes ◽  
Subsequent Calculation ◽  
Kaoko Belt ◽  
Universal Stage ◽  
Active Slip

The volume texture of a naturally deformed quartzite from the Kaoko belt, North-West Namibia, has been analysed by both universal stage microscopy and neutron diffraction. Universal stage microscopy is restricted to the determination of the base pinacoid preferred orientation in quartzite. For a more complete description of the texture, the orientations of additional crystal planes, such as first and second order prisms as well as positive and negative rhombs, must be known. Neutron methods allow the evaluation of pole figures of all Bragg reflecting planes, of which those of the first order prisms being considered to be the most active slip planes, are of particular interest. Drawbacks of neutron diffraction, i.e. the faking of an eventually absent inversion centre and lack of resolution, can be overcome by pole figure inversion and subsequent calculation of desired pole figures. Both, universal stage microscopy and neutron diffraction yield well comparable results, of course only with respect to the pole figure of the c-axis.

scholarly journals Texture Analysis of a Zinc Layer on a Steel Substrate Using Neutron Diffraction

1993 ◽  
Vol 21 (2-3) ◽  
pp. 71-78
Author(s):  
H.-G. Brokmeier
Keyword(s):  
Distribution Function ◽  
Neutron Diffraction ◽  
Texture Analysis ◽  
Orientation Distribution Function ◽  
Steel Substrate ◽  
Orientation Distribution ◽  
Pole Figures ◽  
Iron And Zinc

This paper describes the application of neutron diffraction to investigate the texture of a zinc layer 8 μm in thickness. In a nondestructive way both the texture of the zinc layer as well as the texture of the steel substrate were studied. Therefore, pole figures of iron ((110), (200) and (211)) and of zinc ((0002), (101¯0), (101¯1); and (101¯3)/(112¯0)) were measured; additionally the orientation distribution function of iron and zinc were calculated.

Quantitative Texture Analysis and Phase Fraction of Nickel-Titanium Shape Memory Alloys by Means of Neutron Diffraction

2004 ◽  
Vol 443-444 ◽  
pp. 267-270 ◽  
Author(s):  
H. Sitepu ◽  
Heinz Günter Brokmeier
Keyword(s):  
Neutron Diffraction ◽  
Shape Memory Alloys ◽  
Shape Memory ◽  
Orientation Distribution ◽  
Nickel Titanium ◽  
Phase Fraction ◽  
Polycrystalline Nickel ◽  
Minor Variation ◽  
Pole Figures ◽  
Niti Shape Memory Alloys

The orientation distribution function (ODF) of the textured polycrystalline nickel titanium (NiTi) shape memory alloys (SMAs) was determined from the measured austenitic (B2)pole-figures by neutron diffraction. The texture results showed that neutron diffraction is an excellent tool to investigate the minor variation in the texture of NiTi alloys, which is very sensitive to the variation of the content of nickel in the materials. Moreover, the alloys crystallographic phase fraction and texture were calculated from Rietveld refinement with generalized spherical harmonic (GSH) description for the measured complete neutron powder diffraction (ND) spectrum, rather than a few isolated peaks, during in-situ temperature-induced martensitic transformation. The phase fraction results are consistent with the differential scanning calorimeter (DSC) curves.

scholarly journals A Note on the Rolling Texture of Nickel-Iron-Niobium Alloy

1981 ◽  
Vol 4 (3) ◽  
pp. 153-157 ◽  
Author(s):  
L. C. Tai ◽  
Zen-Jue Tan
Keyword(s):  
Rolling Texture ◽  
Niobium Alloy ◽  
Cold Reduction ◽  
X Ray ◽  
Nickel Iron ◽  
Mechanical Hardness ◽  
Pole Figures ◽  
The Difference

The nickel-iron-niobium alloy containing about 79% Ni, 8% Nb and 13% Fe in sheet form has been prepared and fabricated. The rolling texture of the alloy after cold reduction of 50 and 94% has been determined by using X-ray counter diffractometer and the results are presented in pole figures. In comparison with Ni-Fe-Mo, the results are discussed from a view of the difference of mechanical hardness between these two categories of alloys.

Lattice Strain Pole Figures Analysis in Titanium during Uniaxial Deformation

2017 ◽  
Vol 905 ◽  
pp. 74-80
Author(s):  
David Gloaguen ◽  
Baptiste Girault ◽  
Jamal Fajoui ◽  
Vincent Klosek ◽  
Marie José Moya
Keyword(s):  
Experimental Data ◽  
Neutron Diffraction ◽  
Lattice Strain ◽  
Pure Titanium ◽  
Tensile Load ◽  
Uniaxial Tensile ◽  
Lattice Strains ◽  
Pole Figures ◽  
In Situ Neutron Diffraction

A theoretical and experimental study was carry out to investigate deformation mechanisms in a textured titanium alloy. In situ neutron diffraction measurements were performed to analyze different {hk.l} family planes ({10.0}, {10.1}, {11.0} and {00.2}) and determine the corresponding internal strain pole figures. This method was applied to a pure titanium (a-Ti) submitted to a uniaxial tensile load up to 2 %. The experimental data was then used to validate the EPSC model in order to predict the distribution of lattice strains determined by neutron diffraction for various diffraction vector directions. This comparison reveals that the model results were in good agreement with the experimental data and the simulations reproduced the lattice strain development observed on the strain pole figures determined by neutron diffraction.

Neutron Diffraction Texture Analysis of Grain-Oriented Steel Sheets

2005 ◽  
Vol 105 ◽  
pp. 175-180 ◽  
Author(s):  
Stanislav Vratislav ◽  
Maja Dlouhá ◽  
Ladislav Kalvoda
Keyword(s):  
Neutron Diffraction ◽  
Cold Rolling ◽  
Texture Analysis ◽  
Volume Fraction ◽  
Rolling Direction ◽  
Orthorhombic Symmetry ◽  
Automatic Data ◽  
Cubic Symmetry ◽  
Steel Sheets ◽  
Pole Figures

Our laboratory developed and tested experimental and calculation techniques for quantitative texture analysis based on the ODF combined with the diffraction of thermal neutrons. In our work the texture of the Fe-3%Si sheets was investigated after different stages of their processing, i.e. hot-rolled strips, first cold rolling, first inter-annealing, second cold rolling, second annealing and secondary recrystallisation. The texture experiments were carried out on the KSN-2 diffractometer which is equipped with the TG-1 texture goniometer with automatic data collection for transmission and reflection geometry. TODFND (the cubic symmetry of the crystals and orthorhombic symmetry of the specimen) was used and the ODF values were obtained together with all texture characteristics (pole figures, inverse pole figures, ODF - f (g) values, fibre texture with <110> and <001> axis parallel to rolling direction, parameters of the ideal orientations (HKL)<uvw>, texture index J, volume fraction coefficient f. The comparison of the texture parameters of the six samples with the different technologic history is given and the magnetic anisotropy of all measured samples was determined by means of the quantitative texture analysis (ODF-the matrix Cl nµ) for all samples. Results achieved in our study confirm that the quantitative texture analysis in connection with neutron diffraction can help to improve the technology of the preparation of oriented magnetic steel sheets.

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