Effect of Solution Treatment on Microstructure and Properties of the SAF2507 Super Duplex Stainless Steel

2012 ◽  
Vol 724 ◽  
pp. 3-6 ◽  
Author(s):  
Jin Ming Liu ◽  
Jie Liu ◽  
Guang Wei Fan ◽  
Dong Fang Du ◽  
Guo Ping Li ◽  
...  

Effect of solution treated temperature at 5001100°C on ferrite/austenite ratio and σ phase precipitation has been studied in this paper, and the tensile properties after solution treatment at 950°C and 1050°C is compared. The results shows that the ferrite/austenite ratio treated 1050~1100°C is about 1:1; and the formation of σ phase occurs in the ferrite or at ferrite - austenite boundary. The quantity of the σ phase precipitation increases firstly and then decreases with increase of the solution treatment temperature, reaching the maximum at 900°C, and disperse at above 1050°C. Tensile tests show that the fracture is brittle divided and stretched by ductile belt at 950°C, and ductile at 1050°C.

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1481
Author(s):  
Junhe Li ◽  
Wei Shen ◽  
Ping Lin ◽  
Fuming Wang ◽  
Zhanbing Yang

The changes of microstructures, element distribution, and comprehensive properties were studied to explore their interactions with each other, induced by solution treatment of UNS S32750 super duplex stainless steel. The results showed that the ferrite content improved, while the austenite content declined as the temperature increased. From 900 to 1000 °C, the σ phase existing at α/γ grain boundaries and in ferrite grains gradually dissolved. At 1050 °C, the microstructures consisted of only ferrite and austenite. From 1050 to 1300 °C, the Cr2N precipitated in ferrite and gradually grew and coarsened. The impact energy and pitting potential of UNS S32750 first improved and then weakened, while the hardness is the opposite, owing to the combined effects of element distribution, microstructures, and precipitates. In the presence of the σ phase, the corrosion resistance and mechanical properties of UNS S32750 correspond directly to the σ phase fraction. Subsequently, the rise in temperature promoted γ → α phase transformation, and the elements partitioning ratios of Cr and Mo declined, resulting in reduced toughness and corrosion resistance and a rise in hardness. Consequently, when the solution treatment temperature is 1050 °C, the α/γ ratio of UNS S32750 approached 1:1, with excellent overall properties.


2013 ◽  
Vol 711 ◽  
pp. 87-90
Author(s):  
Yin Hui Yang

A commercial 2507 duplex stainless steel with different solution treatments followed by aging at 850°C has been investigated. At the early aging time of 850°C, the σ-phase precipitate was predominantly distributed at the δ/γ interface, as the isothermal aging time was increased to 150 min, more σ-phase precipitate formed in ferrite and became coarser by a eutectoid reaction δσ+γ2. The amount of δ-ferrite decreased rapidly at the beginning of aging for 80 minutes, increasing solution treatment temperature from 1060°C to 1230°C delayed decomposition of δ-ferrite due to lowering σ-phase formation element (Cr). The reaction rate K and σ-phase precipitation rate were lowered by increasing solution treatment temperature from 1060°C to 1230°C.


2010 ◽  
Vol 146-147 ◽  
pp. 818-824
Author(s):  
Hong Liang Xiang ◽  
Dong Liu ◽  
Fu Shan He

In this paper, effects of solid solution treatment temperature on microstructure and tensile properties of casting SAF 2507 super duplex stainless steel were researched by means of optical microscope (OM), scanning electron microscope (SEM), energy dispersive spectrometer (EDS) and tensile test. The results indicate that the amount of γ phase increases according to a linear relationship f(g ) = -0.134T +159.94 during the temperatures from 1100°C to 1250°C. Tensile properties of casting SAF 2507 super duplex stainless steel fluctuate with solution temperature change. Austenitic grain size and morphology are the most important factors on tensile property. The tensile strength is the highest owing to the finest austenitic grain at the solution temperature of 1150°C. The elongation is related to the fracture mode. At 1100 , elongation ration is highest because of the ductile fracture.


2010 ◽  
Vol 658 ◽  
pp. 380-383 ◽  
Author(s):  
Ying Han ◽  
De Ning Zou ◽  
Wei Zhang ◽  
Jun Hui Yu ◽  
Yuan Yuan Qiao

Specimens of 2507 super-duplex stainless steel aging at 850°C for 5 min, 15 min and 60 min were investigated to evaluate the pitting corrosion resistance in 3.5% NaCl solution at 30°C and 50°C. The results are correlated with the microstructures obtained with different aging time. The precipitation of σ phase remarkably decreases the pitting corrosion resistance of the steel and the specimen aged for 60 min presents the lowest pitting potential at both 30°C and 50°C. With increasing the ambient temperature from 30°C to 50°C, the pitting potential exhibits a reduction tendency, while this tendency is less obviously in enhancing the ambient temperature than in extending the isothermal aging duration from 5 to 60 min. SEM analysis shows that the surrounding regions of σ phase are the preferable sites for the formation of corrosion pits which grew up subsequently. This may be attributed to the lower content of corrosion resistance elements in these regions formatted with σ phase precipitation.


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