solution treatment
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Author(s):  
Mohammed Gouda ◽  
Salah Salman ◽  
Saad Ebied

Abstract β-titanium alloys are essential in many applications, particularly biomedical applications. Ti-14Mn β-type alloy was produced using an electric arc furnace from raw alloying elements in an inert atmosphere. The alloy was homogenized at 1000 °C for 8 hr to ensure the complete composition distribution, followed by solution treatment at 900 °C, then quenched in ice water. The alloy was subjected to cold deformation via cold rolling with different ratios: 10, 30, and 90%. The phases change, microstructure, mechanical properties, and corrosion resistance of Ti-14Mn alloys were evaluated before and after cold rolling. The results showed that the β-phase is the only existed phase even after a high degree of deformation. The microstructure shows a combination of twinning and slipping deformation mechanisms in the deformed alloy. Microhardness values indicated a linear increase equal to 30% by increasing the ratio of cold deformation due to the strain hardening effect. The corrosion resistance of Ti-14Mn alloy was doubled after 90% cold rolling.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 146
Author(s):  
Tianjiao Luo ◽  
Jianguang Feng ◽  
Chenye Liu ◽  
Cong Wang ◽  
Yingju Li ◽  
...  

In the present work, the effect of heat treatment on the cyclic deformation behavior of as-extruded ZA81M magnesium alloy was investigated. Two heat treatment conditions were applied to the as-extruded ZA81M alloy: a solution treatment (T4, 653 K for 40 h and quenched with 298 K water) and a solution treatment plus artificial aging (T6, 348 K for 32 h (pre-aging at low temperature) and 453 K for 8 h (the second aging) and quenched with 353 K water). The results showed that the fine second phase precipitated after the aging treatment, the tensile yield strength of the T6-treated specimens increased, and the stress amplitude of T6-treated specimens was always higher than that of T4-treated specimens. The T6-treated specimens had a higher total strain energy density and a shorter fatigue life at a strain amplitude of 0.4%, and a lower total strain energy density and a longer fatigue life at a strain amplitude of 0.8%, compared to the T4-treated specimens. All fatigue cracks of the T4 and T6 ZA81M alloy were initiated at the second phase or along the grain boundary and propagated perpendicular to the loading direction.


2022 ◽  
Vol 327 ◽  
pp. 189-196
Author(s):  
Le Cheng ◽  
Hong Xing Lu ◽  
Min Luo ◽  
Xing Gang Li ◽  
Wan Peng Zhang ◽  
...  

The evolution of the microstructure of A356.2 alloys prepared by the rheocasting and squeeze casting during solution heat treatment was investigated. In contrast with the conventional solution heat treatment process (3 hours at 540oC), a short time solution treatment process (less than 1 hour at 540oC) is applied in this paper. The results show that the rheocastings require a shorter solution time than the squeeze-castings to obtain spheroidized Si particles. After solution for 10 min, the X-ray diffraction inspection results show that the Mg2Si phase completely is dissolved in both rheocastings and squeeze-castings. However, a small amount of Mg2Si is found at the edge of the Si particle by scanning electron microscope observation. After solution for more than 20 min, the Mg2Si phase is completely dissolved. Fe-rich phases, including AlSiFeMg and AlFeSi, exist throughout the solution process. The developed T6 heat treatment with a short solution time can effectively improve production efficiency and decrease process cost for the rheocasting process. Key words: A356.2 alloy, microstructure, short solution time, rheocasting, squeeze casting


Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 443
Author(s):  
Mingdong Wu ◽  
Daihong Xiao ◽  
Xinkai Wang ◽  
Lanping Huang ◽  
Wensheng Liu

Combined with microstructure characterization and properties tests, the effects of Zn contents on the mechanical properties, corrosion behaviors, and microstructural evolution of extruded Al–Li–Cu–Mg–Ag alloys were investigated. The results show that the increase in Zn contents can accelerate hardening kinetics and improve the hardness of peak-aged alloys. The Zn-added alloys present non-recrystallization characteristics combined with partially small recrystallized grains along the grain boundaries, while the T1 phase with finer dimension and higher number density could explain the constantly increasing tensile strength. In addition, increasing Zn contents led to a lower corrosion current density and a shallower maximum intergranular corrosion depth, thus improving the corrosion resistance of the alloys. Zn addition, distributed in the central layer of T1 phases, not only facilitates the precipitation of more T1 phases but also reduces the corrosion potential difference between the T1 phase and the matrix. Therefore, adding 0.57 wt.% Zn to the alloy has an excellent combination of tensile strength and corrosion resistance. The properties induced by Zn under the T8 temper (solid solution treatment + water quenching + 5% pre-strain+ isothermal aging), however, are not as apparent as the T6 temper (solid solution treatment + water quenching + isothermal aging).


2022 ◽  
Vol 60 (1) ◽  
pp. 83-93
Author(s):  
Young-We Kim ◽  
Yong-Hee Jo ◽  
Yun-Soo Lee ◽  
Hyoung-Wook Kim ◽  
Je-In Lee

The effects of dissolution of the η′ phase by solution treatment on the mechanical properties of A7075-T6 alloy were investigated. Immediately after solution treatment of the T6 sheet at 450 oC or higher, elongation significantly increased and dissolution of the η′ phase occurred. η′ is the main hardening phase. After natural-aging, GPI, which is coherent with the aluminum matrix, was formed and strength increased. When bake hardening after natural-aging was performed, the yield strength slightly increased due to partial dissolution of the GPI and re-precipitation of the η′ phase. In contrast, after solution treatment at 400 oC, there was less elongation increase due to the precipitation of the coarse η phase at grain boundaries and low dissolution of the η′ phase. In addition, when bake hardening after natural-aging was performed, the yield strength decreased due to insufficient GPI, which is the nucleation site of the η′ phase. To promote reprecipitation of the η′ phase, the solution treatment temperature was set to a level that would increase solubility. As a result, the yield strength was significantly increased through re-precipitation of a large number of fine and uniform η′ phase. In addition, to increase the effect of dissolution, a pre-aging treatment was introduced and the bake hardenability can be improved after dissolution.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 84
Author(s):  
Tingting Liu ◽  
Yanglu Liu ◽  
Lu Xiao ◽  
Shibo Zhou ◽  
Bo Song

Mg–Al binary alloys in the concentration range from 0 to 4.0 wt.% Al have been prepared under conventional casting conditions. The as-cast Mg and Mg–Al alloys after solution treatment were processed via hot extrusion at 350 °C. The results show that Al has a positive influence on grain refinement and solution strengthening. The as-extruded Mg–Al alloys are fully recrystallized, and the tensile yield strength of the binary alloys is two times higher than that of pure Mg. Furthermore, the elongations of Mg–Al alloys are much higher than that of pure Mg. In addition, Mg and Mg–Al alloys were further studied by the viscoplastic self-consistent (VPSC) model to explore the activation and evolution of deformation modes. The simulation results match well with the experimental results.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 92
Author(s):  
Naoto Kirekawa ◽  
Kaisei Saito ◽  
Minho O ◽  
Equo Kobayashi

Natural aging after solution treatment has a negative effect on the precipitation strengthening of Al–Mg–Si alloys since Cluster(1) formed at a room temperature cannot be dissolved or transformed into precipitates during artificial aging at 170 °C. In this study, cold rolling is focused on as an alternative solution to pre-aging, which is a conventional method to prevent Cluster(1) formation. It is known that excess vacancies are necessary for cluster formation. Cold rolling suppresses cluster formation because excess vacancies disappear at dislocations introduced by cold rolling. In addition, it is expected that cold rolling accelerates the precipitation behavior because the diffusion of solute atoms is promoted by introduced lattice defects. The transition of Cluster(1) was evaluated by Micro Vickers hardness tests, tensile tests, electrical conductivity measurements and differential scanning calorimetry analyses. Results showed the negative effect of natural aging was almost suppressed in 10% cold-rolled samples and completely suppressed in 30% cold-rolled samples since Cluster(1) dissolved during artificial aging at 170 °C due to lowering of the temperature of Cluster(1) dissolution by cold rolling. It was found that the precipitation in cold-rolled samples was accelerated since the hardness peak of 10% cold-rolled samples appeared earlier than T6 and pre-aged samples.


Metals ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 71
Author(s):  
Ho-Jung Kang ◽  
Jin-Young Park ◽  
Yoon-Suk Choi ◽  
Dae-Hyun Cho

Heat treatment is widely used to improve the properties of Al–Si–Mg alloys and its outcomes are influenced by the parameters applied during the treatment. This study describes the effect of the solution and artificial aging treatments on the microstructure and mechanical properties of die-cast Al–Si–Mg alloys. The microstructure of the as-cast Al–Si–Mg alloy was mainly composed of α-Al, complex needle-type eutectic Si particles, Mg2Si, and α-AlFeMn. The complex needle-type eutectic Si particles disintegrated into spheroidal morphologies, while the Mg2Si was dissolved due to the solid solution treatment. The maximum yield strength (YS) and ultimate tensile strength (UTS) values were 126.06 and 245.90 MPa at 520 °C after 90 min of solution heat treatment, respectively. Although the YS and UTS values of the Al–Si–Mg alloys reduced due to the solution treatment, the elongation (EL) of the solid solution heat-treated Al–Si–Mg alloys was improved in comparison to that of the as-cast Al–Si–Mg alloy. The maximum YS and UTS of 239.50 and 290.93 MPa were obtained after performing artificial aging at 180 °C for 180 min, respectively. However, the EL of the aging heat-treated alloy was reduced by a minimal value.


Metals ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 66
Author(s):  
Hyeongsub So ◽  
Jae-Hong Shin ◽  
Leeseung Kang ◽  
Chanuk Jeong ◽  
Kyou-Hyun Kim

We investigated the effect of solution temperature (Tsol. = 440–530 °C) on the mechanical properties of the Al–3.4Cu–0.34Mg–0.3Mn–0.17Ag alloy, finding that the investigated Al alloy showed the highest mechanical strength of σUTS = ~329 MPa at a Tsol. value of 470 °C. The microstructural investigation demonstrates that the mechanical properties for different Tsol. values stem from grain growth, precipitation hardening, and the formation of large particles at the grain boundaries. On the basis of Tsol. = 470 °C, the effect of each microstructural evolution is significantly different on the mechanical properties. In this study, the relationships between the microstructural evolution and the mechanical properties were investigated with respect to different values of Tsol.


Metals ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 63
Author(s):  
Sergey Akkuzin ◽  
Igor Litovchenko ◽  
Nadezhda Polekhina ◽  
Kseniya Almaeva ◽  
Anna Kim ◽  
...  

The deformation microstructures formed by novel multistage high-temperature thermomechanical treatment (HTMT) and their effect on the mechanical properties of austenitic reactor steel are investigated. It is shown that HTMT with plastic deformation at the temperature decreasing in each stage (1100, 900, and 600 °C with a total strain degree of e = 2) is an effective method for refining the grain structure and increasing the strength of the reactor steel. The structural features of grains, grain boundaries and defective substructure of the steel are studied in two sections (in planes perpendicular to the transverse direction and perpendicular to the normal direction) by Scanning Electron Microscopy with Electron Back-Scatter Diffraction (SEM EBSD) and Transmission Electron Microscopy (TEM). After the multistage HTMT, a fragmented structure is formed with grains elongated along the rolling direction and flattened in the rolling plane. The average grain size decreases from 19.3 µm (for the state after solution treatment) to 1.8 µm. A high density of low-angle boundaries (up to ≈ 80%) is found inside deformed grains. An additional cold deformation (e = 0.3) after the multistage HTMT promotes mechanical twinning within fragmented grains and subgrains. The resulting structural states provide high strength properties of steel: the yield strength increases up to 910 MPa (at 20 °C) and up to 580 MPa (at 650 °C), which is 4.6 and 6.1 times higher than that in the state after solution treatment (ST), respectively. The formation of deformed substructure and the influence of dynamic strain aging at an elevated tensile temperature on the mechanical properties of the steel are discussed. Based on the results obtained, the multistage HTMT used in this study can be applied for increasing the strength of austenitic steels.


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