scholarly journals Micellar Liquid Chromatography Coupled with Fluorometric Detection for the Determination of Terbinafine in Dosage Forms and Plasma

2016 ◽  
Vol 08 (06) ◽  
Author(s):  
Belal F ◽  
Sharaf El-Din MK ◽  
Eid MI ◽  
El-Gamal RM
Keyword(s):  
Liquid Chromatography ◽  
Dosage Forms ◽  
Micellar Liquid Chromatography ◽  
Fluorometric Detection

Determination of Menbutone in Bovine Milk and Meat Using Micellar Liquid Chromatography: Application to Injectable Dosage Forms

2015 ◽  
Vol 9 (3) ◽  
pp. 638-645 ◽  
Author(s):  
F. Belal ◽  
Sawsan A. Abd El-Razeq ◽  
Manal M. Fouad ◽  
S. Zayed ◽  
Fatma A. Fouad
Keyword(s):  
Liquid Chromatography ◽  
Bovine Milk ◽  
Dosage Forms ◽  
Micellar Liquid Chromatography ◽  
Injectable Dosage

scholarly journals A new stability-indicating RP-HPLC method for the determination of dicyclomine hydrochloride and dimethicone combination in tablet dosage forms

2021 ◽  
Vol 7 (1) ◽  
Author(s):  
J. Saroja ◽  
Anantha Lakshmi P.V. ◽  
Y. Rammohan ◽  
D. Divya Reddy
Keyword(s):  
Liquid Chromatography ◽  
Dosage Forms ◽  
Flow Speed ◽  
Hplc Method ◽  
Stability Indicating ◽  
Simultaneous Quantification ◽  
Rp Hplc ◽  
Tablet Formulations ◽  
Tablet Dosage

Abstract Background We describe a “stability-indicating liquid chromatography” technique for the estimation of dimethicone (DEC) and dicyclomine hydrochloride (DEH) in the established tablet formulations. Individual quantification of DEH and DEC was reported. But simultaneous quantification of DEH and DEC was lacking. DEH and DEC were analysed on an “XTerra C18 column (250 mm × 4.6 mm, 5 μm)” with the mobile phase solvent run isocratically with 0.1M K2HPO4-acetonitrile (55:45, v/v) on a flow speed of 1.0 mL/min. Results The chromatographic run period for the DEC and DEH assay was 6.0 min with retention times of 2.134 and 2.865 min, respectively. The method was validated for accuracy (99.453 to 100.417% and 99.703 to 100.303% recovery values for DEH and DEC, respectively), precision (RSV value 0.135% for DEC and 0.171% for DEH), linearity (5–15 μg/mL for DEH and 20–60 μg/mL for DEC), selectivity (no hinderance from excipients) and specificity (no hinderance from degradants) recovery. Conclusion The developed stability-indicating liquid chromatography process was well applied to established tablet formulations.

Determination of ciprofloxacin and enoxacin in human serum samples by micellar liquid chromatography

2004 ◽  
Vol 516 (1-2) ◽  
pp. 135-140 ◽  
Author(s):  
José Luis Vı́lchez ◽  
Lilia Araujo ◽  
Avismelsi Prieto ◽  
Alberto Navalón
Keyword(s):  
Liquid Chromatography ◽  
Human Serum ◽  
Micellar Liquid Chromatography ◽  
Serum Samples ◽  
Human Serum Samples
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