scholarly journals Automated Scanning Electron Microscope Based Mineral Liberation Analysis An Introduction to JKMRC/FEI Mineral Liberation Analyser

Author(s):  
Ying Gu
Minerals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1038
Author(s):  
Jie Deng ◽  
Kecheng Zhang ◽  
Dongsheng He ◽  
Hengqin Zhao ◽  
Rachid Hakkou ◽  
...  

Checking the presence of sesquioxide (Fe2O3, Al2O3) is helpful for its removal in advance. Therefore, the occurrence of sesquioxide in a mid-low grade calcareous-siliceous collophane ore (massive carbonate-apatite, also known as francolite) from Guizhou, China was determined by X-ray fluorescence spectroscopy (XRF), X-ray diffraction (XRD), field emission scanning electron microscope-energy dispersive X-ray spectrometry (FESEM-EDX) and Mineral Liberation Analyzer (MLA). The results show that iron mainly occurs as pyrite FeS2, goethite FeO(OH) and as substitution within dolomite Ca(Mg,Fe)(CO3)2, while aluminum is enriched in muscovite KAl2(AlSi3O10)(OH)2 and also found in apatite (F,CO3)CaPO4 and calcite CaCO3 due to isomorphism or adsorption. All these minerals are fine-grained, among which pyrite and goethite tend to be enriched in larger particles. Intergrowth is predominant in the six minerals’ locking. Pyrite is mainly intergrown with calcite, biotite and also included in apatite and muscovite, while the monomer pyrite appears as semi-automorphic fine grain with the liberation of 56.1%. Apatite particles are mainly intergrown with quartz and calcite. Most of goethite, dolomite, muscovite and calcite form intergrowth with apatite, with contents of 21.7%, 11.1%, 19.5% and 41%, respectively. The removal of pyrite, goethite, dolomite, muscovite and calcite in the ore is the key to reduce the contents of Fe2O3 and Al2O3. In the subsequent beneficiation, the ore must be fully ground. In addition to flotation, magnetic separation can also be considered to remove part of iron in ore. For the removal of aluminum from apatite, leaching method can be considered.


Author(s):  
S. Pignolet-Brandom ◽  
K. J. Reid

QEM*SEM, or quantitative evaluation of materials by scanning electron microscopy, is a fully automated scanning electron microscope system that was designed and engineered by CSIRO in Australia for applications to the minerals industry. It is an integrated system in which the computer and its associated hardware and software control SEM operations. Minerals can be identified in point, linear or area scans. Depending on the type of scan, information is extracted from the data files and summarized in tables and graphs covering mineral abudances, associations, sizes, free surface area and the degree of liberation. In addition, area scans can be replayed on a graphics monitor to produce QEM*SEM mineral species maps.The QEM*SEM system consists of an International Scientific Instruments SX-40 scanning electron microscope with a specially designed sample chamber that permits 100 mm movement of the stage. The EDS units were designed for rapid collection of x-ray spectra and consist of four lithium drifted silicon detectors each with a separate preamplifier.


Author(s):  
R. E. Ferrell ◽  
G. G. Paulson

The pore spaces in sandstones are the result of the original depositional fabric and the degree of post-depositional alteration that the rock has experienced. The largest pore volumes are present in coarse-grained, well-sorted materials with high sphericity. The chief mechanisms which alter the shape and size of the pores are precipitation of cementing agents and the dissolution of soluble components. Each process may operate alone or in combination with the other, or there may be several generations of cementation and solution.The scanning electron microscope has ‘been used in this study to reveal the morphology of the pore spaces in a variety of moderate porosity, orthoquartzites.


Author(s):  
C. T. Nightingale ◽  
S. E. Summers ◽  
T. P. Turnbull

The ease of operation of the scanning electron microscope has insured its wide application in medicine and industry. The micrographs are pictorial representations of surface topography obtained directly from the specimen. The need to replicate is eliminated. The great depth of field and the high resolving power provide far more information than light microscopy.


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