Comparision of The Histologic Response to Different Bulking Materials Used in Endoscopic Vesicoureteral Reflux Surgery

Tool materials used in ultramicrotomy are glass, developed by Latta and Hartmann (1) and diamond, introduced by Fernandez-Moran (2). While diamonds produce more good sections per knife edge than glass, they are expensive; require careful mounting and handling; and are time consuming to clean before and after usage, purchase from vendors (3-6 months waiting time), and regrind. Glass offers an easily accessible, inexpensive material ($0.04 per knife) with very high compressive strength (3) that can be employed in microtomy of metals (4) as well as biological materials. When the orthogonal machining process is being studied, glass offers additional advantages. Sections of metal or plastic can be dried down on the rake face, coated with Au-Pd, and examined directly in the SEM with no additional handling (5). Figure 1 shows aluminum chips microtomed with a 75° glass knife at a cutting speed of 1 mm/sec with a depth of cut of 1000 Å lying on the rake face of the knife.

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High Voltage Transmission Microscopy of Surveyor III Camera Shrouds

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100064748 ◽

1971 ◽

Vol 29 ◽

pp. 138-139

Author(s):

W. R. Duff ◽

L. E. Thomas ◽

R. M. Fisher ◽

S. V. Radcliffe

Keyword(s):

Alloy Sheet ◽

Transmission Microscopy ◽

Television Camera ◽

Window Method ◽

Transmission Electron ◽

Microstructural Effects ◽

Lunar Environment ◽

Successful Retrieval ◽

Materials Used ◽

Abrasive Paper

Successful retrieval of the television camera and other components from the Surveyor III spacecraft by the Apollo 12 astronauts has provided a unique opportunity to study the effects of a known and relatively extensive exposure to the lunar environment. Microstructural effects including those produced by micro-meteorite impact, radiation damage (by both the solar wind and cosmic rays) and solar heating might be expected in the materials used to fabricate the spacecraft. Samples received were in the form of 1 cm2 of painted unpainted aluminum alloy sheet from the top of the camera visor (JPL Code 933) and the sides (935,936) and bottom (934) of the lower camera shroud. They were prepared for transmission electron microscopy by first hand-grinding with abrasive paper to a thickness of 0.006". The edges were lacquered and the sample electropolished in 10% perchloric methanol using the “window” method, to a thickness of ~0.001". Final thinning was accomplished by polishing 3 mm punched disks in an acetic-phosphoric-nitric acid solution.

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Structure-property relationships of PE/PP sandwiched films

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100126998 ◽

1987 ◽

Vol 45 ◽

pp. 454-455

Author(s):

J. Petermann ◽

G. Broza ◽

U. Rieck ◽

A. Jaballah ◽

A. Kawaguchi

Keyword(s):

Mechanical Tests ◽

Polymer Materials ◽

Ionic Crystals ◽

Structure Property ◽

Polymer Systems ◽

Structure Property Relationships ◽

Oriented Films ◽

Materials Used ◽

Polymer Laminates ◽

Heated Glass

Oriented overgrowth of polymer materials onto ionic crystals is well known and recently it was demonstrated that this epitaxial crystallisation can also occur in polymer/polymer systems, under certain conditions. The morphologies and the resulting physical properties of such systems will be presented, especially the influence of epitaxial interfaces on the adhesion of polymer laminates and the mechanical properties of epitaxially crystallized sandwiched layers.Materials used were polyethylene, PE, Lupolen 6021 DX (HDPE) and 1810 D (LDPE) from BASF AG; polypropylene, PP, (PPN) provided by Höchst AG and polybutene-1, PB-1, Vestolen BT from Chemische Werke Hüls. Thin oriented films were prepared according to the method of Petermann and Gohil, by winding up two different polymer films from two separately heated glass-plates simultaneously with the help of a motor driven cylinder. One double layer was used for TEM investigations, while about 1000 sandwiched layers were taken for mechanical tests.

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