Synthesis of 5-nitro 2-diethylamino 6-methyl pyridine Organic Crystal By Nitration of 2-diethylamino 6-methyl Pyridine With H2SO4/HNO3

2021 ◽  
Vol 2 (2) ◽  
pp. 070
Author(s):  
Linsheng Wang
Keyword(s):  
Organic Crystal ◽  
Methyl Pyridine

scholarly journals A Novel 3E Method for Synthesis of 5-nitro 2-diethylamino 6-methyl pyridine Organic Crystal by Nitration of 2-diethylamino 6-methyl pyridine with H2SO4/HNO3

2021 ◽  
Vol 11 (4) ◽  
pp. 4131-4138
Keyword(s):  
Organic Synthesis ◽  
Innovation Process ◽  
Separation Process ◽  
Organic Crystal ◽  
Synthesis Process ◽  
The Novel ◽  
Chromatography Column ◽  
Column Separation ◽  
Energy Consuming ◽  
Methyl Pyridine

4-nitro 2-diethylamino 5-methyl pyridine (P-NitroC10N2H16) as an organic crystal which is the useful intermediate for pharmaceutical synthesis and for production of organic materials, which was usually synthesized by nitration of 2-diethylamino 5-methyl pyridine with H2SO4/HNO3 mixtures, followed by extraction, chromatography column separation and recrystallization three-step procedures. Here an innovation process for synthesizing 4-nitro 2-diethylamino 5-methyl pyridine crystal from the nitration of C10N2H16 without needing chromatography column separation step is presented. The novel organic synthesis process is more ecologic, economical, and environmentally-friendly (3E) than the traditional organic synthesis process since the chromatography column separation process is a material-consuming and energy-consuming step, which needs to dispose of a large amount of wasted silica beads.

Progress in Organic Crystal Transistors for High-Performance Organic Electronics

2008 ◽  
Author(s):  
Jun Takeya ◽  
Takafumi Uemura ◽  
M. Uno ◽  
Masakazu Yamagishi ◽  
Yukihiro Tominari
Keyword(s):  
Organic Electronics ◽  
High Performance ◽  
Organic Crystal

RETRACTED: Determination of Co(II) in water and soil samples using spectrophotometry coupled with preconcentration on 4-amino methyl pyridine anchored silica gel column

2007 ◽  
Vol 146 (1-2) ◽  
pp. 137-141 ◽  
Author(s):  
C. Sivani ◽  
G. Ramakrishna Naidu ◽  
J. Narasimhulu ◽  
D. Rekha ◽  
J. Dilip Kumar ◽  
...  
Keyword(s):  
Silica Gel ◽  
Soil Samples ◽  
Water And Soil Samples ◽  
Methyl Pyridine

A Multidirectional Superelastic Organic Crystal by Versatile Ferroelastical Manipulation

2020 ◽  
Vol 59 (11) ◽  
pp. 4340-4343 ◽  
Author(s):  
Toshiyuki Sasaki ◽  
Shunichi Sakamoto ◽  
Yuichi Takasaki ◽  
Satoshi Takamizawa
Keyword(s):  
Organic Crystal

A plastically bendable and polar organic crystal

CrystEngComm ◽  
2021 ◽  
Author(s):  
Sotaro Kusumoto ◽  
Akira Sugimoto ◽  
Daisuke Kosumi ◽  
Yang Kim ◽  
Yoshihiro Sekine ◽  
...  
Keyword(s):  
Mechanical Stress ◽  
Polar Space ◽  
Organic Crystal ◽  
Space Group ◽  
High Dielectric

In this communication, an organic crystal of the polar space group Pc that is capable of plastically bending in response to external mechanical stress is reported, and its high dielectric...

High photo-stability of single molecules in an organic crystal at room temperature observed by scanning confocal optical microscopy

1998 ◽  
Vol 95 (6) ◽  
pp. 1333-1338 ◽  
Author(s):  
LUDOVIC FLEURY ◽  
BEATE SICK ◽  
GERT ZUMOFEN ◽  
BERT HECHT ◽  
URS P. WILD
Keyword(s):  
Optical Microscopy ◽  
Room Temperature ◽  
Single Molecules ◽  
Organic Crystal ◽  
Photo Stability

Chaotic Organic Crystal Phosphorescent Patterns for Physical Unclonable Functions

2021 ◽  
pp. 2102542
Author(s):  
Healin Im ◽  
Jinsik Yoon ◽  
Jinho Choi ◽  
Jinsang Kim ◽  
Seungho Baek ◽  
...  
Keyword(s):  
Organic Crystal ◽  
Physical Unclonable Functions
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