Response surface central composite design optimization of soluos dumpsite leachate treatment using agricultural biowaste

Author(s):  
Lukumon Salami ◽  
Lukman Bakare

Process optimization plays a very important role in the process industries as it helps to miximise desire output by minimizing the cost of process variables. The aim of this work is to carry out response surface central composite design optimization of Soluos dumpsite leachate treatment using agricultural biowaste. Leachate collected from Soluos dumpsite in Lagos was treated using adsorbent prepared from Muas sapientum peels by studying the effects of adsorbent dosage and contact time on the percentage removal of total dissolved solids (TDS) with the aid of design expert software version 10.0.3. The developed second order regression model was adopted in comparison with the linear and two factor interaction ( ) model based on its coefficient of determination (R2) value and its adequacy by analysis of variance (ANOVA). 80.34 percentage removal of TDS was achieved under experimental process at contact time of 120 mins and dosage of 1 g/100mL while 81.134 percentage removal of TDS was obtained under simulation process at contact time of 63.469 mins and dosage of 0.994 g/100 mL. the values obtained under simulation condition were adopted as the optimum conditions. The developed second order regression model predicted the experimental data up to 98.10 percent confidence level hence it is a true representation of the treatment process and can be used to navigate the design space and optimization process of treatment of Soluos dumpsite leachate.

Molecules ◽  
2021 ◽  
Vol 26 (21) ◽  
pp. 6477
Author(s):  
Yohanis Birhanu ◽  
Seyoum Leta

Lead pollution is a severe health concern for humankind. Utilizing water contaminated with lead can cause musculoskeletal, renal, neurological, and fertility impairments. Therefore, to remove lead ions, proficient, and cost-effective methods are imperative. In this study, the Odaracha soil which is traditionally used by the local community of the Saketa District was used as a novel low-cost technology to adsorb lead ions. Odaracha adsorbent was characterized by scanning electron microscopy and Fourier transform infrared spectroscopy. The adsorption process followed the batch adsorption experiment. The response surface method was implemented to derive the operating variables’ binary interaction effect and optimize the process. According to the study’s experimental result, at optimum experimental conditions Odaracha adsorbent removes 98.17% of lead ions. Based on the result of the central composite design model, the Pb2+ ion removal efficiency of Odaracha was 97.193%, indicating an insignificant dissimilarity of the actual and predicted results. The coefficient of determination (R2) for Pb2+ was 0.9454. According to the factors’ influence indicated in the results of the central composite design model, all individual factors and the interaction effect between contact time and pH has a significant positive effect on lead adsorption. However, other interaction effects (contact time with dose and pH with dose) did not significantly influence the removal efficiency of lead ions. The adsorption kinetics were perfectly fitted with a pseudo-second-order model, and the adsorption isotherm was well fitted with the Freundlich isotherm model. In general, this study suggested that Odaracha adsorbent can be considered a potential adsorbent to remove Pb2+ ions and it is conceivable to raise its effectiveness by extracting its constituents at the industrial level.


2012 ◽  
Vol 195-196 ◽  
pp. 360-363
Author(s):  
Chun Gang Chen ◽  
Fen Xia Han ◽  
Yuan Zhang ◽  
Yu Zhong Shi

The extraction of flavonoids from clovers was optimized to maximize flavonoid yield Y in this study. A central composite design of response surface methodology involving extracting time, liquid-solid ratio, extracting temperature and ethanol concentration was used, and second-order model for Y was employed to generate the response surfaces. The optimum condition for Y was determined as follows: extracting time 24min, liquid-solid ratio 20, extracting temperature 80°C, and ethanol concentration 72%. Under the optimum condition, the flavonoid yield was 2.49%.


2011 ◽  
Vol 201-203 ◽  
pp. 2513-2516 ◽  
Author(s):  
Han Gao ◽  
Gui Fang Xu ◽  
Yuan Yuan Fan ◽  
Hai Juan Nan ◽  
Su Fang Fu

The fermentation process of pear vinegar was optimized to maximize the amount of acetate in this study. A central composite design of response surface methodology involving inoculation rate, temperature, time was used, and second-order model for the amount of acetate was employed to generate the response surface. The optimum condition for the fermentation process was determined as follows: inoculation rate 8.65 %, temperature 30.17 °C, time 7.44 d. The obtained amount of acetate at the optimum condition was 9.53%.


2016 ◽  
Vol 5 (4) ◽  
pp. 22
Author(s):  
Mary Paschal Iwundu

The equiradial designs are studied as alternative second-order N-point spherical Response Surface Methodology designs in two variables, for design radius ρ = 1.0. These designs are seen comparable with the standard second-order response surface methodology designs, namely the Central Composite Designs. The D-efficiencies of the equiradial designs are evaluated with respect to the spherical Central Composite Designs. Furthermore, D-efficiencies of the equiradial designs are evaluated with respect to the D-optimal exact designs defined on the design regions of the Circumscribed Central Composite Design, the Inscribed Central Composite Design and the Face-centered Central Composite Design. The D-efficiency values reveal that the alternative second-order N-point spherical equiradial designs are better than the Inscribed Central Composite Design though inferior to the Circumscribed Central Composite Design with efficiency values less than 50% in all cases studied. Also, D-efficiency values reveal that the alternative second-order N-point spherical equiradial designs are better than the N-point D-optimal exact designs defined on the design region supported by the design points of the Inscribed Central Composite Design. However, the N-point spherical equiradial designs are inferior to the N-point D-optimal exact designs defined on the design region supported by the design points of the Circumscribed Central Composite Design and those of the Face-centered Central Composite Design, with worse cases with respect to the design region of the Circumscribed Central Composite Design.


2012 ◽  
Vol 524-527 ◽  
pp. 2306-2309
Author(s):  
Guang Lei Li ◽  
Su Juan Du ◽  
Jie Zeng

The preparation of sweet potato distarch phosphates which possess low digestibility was optimized in this study. A central composite design of response surface methodology involving STMP concentration, pH, phosphorylation temperature and time was used, and second-order model for starch digestibility was employed to generate the response surface. The optimum condition for preparation of sweet potato distarch phosphates was as follows: STMP concentration 3%, pH 10, phosphorylation temperature 40°C, and phosphorylation time 3h. The starch digestibility of sweet potato distarch phosphates was yield of 0.5508±0.0003 (n=3) under these conditions.


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