Combined atomic force microscopy and voltage pulse technique to accurately measure electrostatic force

2016 ◽  
Vol 55 (8S1) ◽  
pp. 08NB05 ◽  
Author(s):  
Eiichi Inami ◽  
Yoshiaki Sugimoto
2019 ◽  
Vol 10 ◽  
pp. 617-633 ◽  
Author(s):  
Aaron Mascaro ◽  
Yoichi Miyahara ◽  
Tyler Enright ◽  
Omur E Dagdeviren ◽  
Peter Grütter

Recently, there have been a number of variations of electrostatic force microscopy (EFM) that allow for the measurement of time-varying forces arising from phenomena such as ion transport in battery materials or charge separation in photovoltaic systems. These forces reveal information about dynamic processes happening over nanometer length scales due to the nanometer-sized probe tips used in atomic force microscopy. Here, we review in detail several time-resolved EFM techniques based on non-contact atomic force microscopy, elaborating on their specific limitations and challenges. We also introduce a new experimental technique that can resolve time-varying signals well below the oscillation period of the cantilever and compare and contrast it with those previously established.


2012 ◽  
Vol 714 ◽  
pp. 147-152 ◽  
Author(s):  
Junkal Gutierrez ◽  
Agnieszka Tercjak ◽  
Iñaki Mondragon

Novel transparent multiphase nanostructured thermosetting composites with different block copolymer and sol-gel contents have been developed. Morphology of designed systems has been investigated by atomic force microscopy (AFM). Electrostatic force microscopy (EFM) has been used in order to study the conductive properties of prepared hybrid inorganic/organic nanostructured thermosetting systems. Moreover taking into account the optical properties of TiO2 nanoparticles UV-vis measurements indicate that TiO2 nanoparticles clearly enhance the UV-shielding efficiency of the inorganic/organic nanostructured thermosetting systems without losing high-visible light transparency.


2016 ◽  
Vol 116 (9) ◽  
Author(s):  
Joost van der Lit ◽  
Francesca Di Cicco ◽  
Prokop Hapala ◽  
Pavel Jelinek ◽  
Ingmar Swart

2002 ◽  
Vol 737 ◽  
Author(s):  
Tao Feng ◽  
Harry A. Atwater

ABSTRACTQuantitative understanding of charging and discharging of Si nanocrystals in SiO2 films on Si substrate is essential to their application in floating gate nonvolatile memory devices. Charge imaging by atomic force microscopy (AFM) or electrostatic force microscopy (EFM) can provide qualitative information on such system, while a further step is needed. We have developed a generalized method of images, which can solve Poisson equation for multiple dielectric layers, to simulate the charge imaging of Si nanocrystals by non-contact mode AFM under different sample geometries. Simulated images can be compared with experimental images thoroughly to estimate the total amount and distributions of trapped charges, which is also useful in the study of time evolution of charges or dissipation problems.


2018 ◽  
Vol 24 (2) ◽  
pp. 126-131 ◽  
Author(s):  
Sergey Y. Luchkin ◽  
Keith J. Stevenson

AbstractIn this work we analyzed the effect of the atomic force microscopy probe tip apex shape on Kelvin Probe Force Microscopy (KPFM) potential sensitivity and spatial resolution. It was found that modification of the apex shape from spherical to planar upon thinning of the conductive coating leads to enhanced apex contribution to the total electrostatic force between the probe and the sample. The effect results in extended potential sensitivity and spatial resolution of KPFM. Experimental results were supported by calculations.


2003 ◽  
Vol 15 (2) ◽  
pp. S14-S18 ◽  
Author(s):  
Sascha Sadewasser ◽  
Philippe Carl ◽  
Thilo Glatzel ◽  
Martha Ch Lux-Steiner

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