analytical microscopy
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Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1423
Author(s):  
Liza-Anastasia DiCecco ◽  
Mehdi Mehdi ◽  
Afsaneh Edrisy

In this work, fatigue improvement through shot peening of an additive manufactured Ti–TiB block produced through Plasma Transferred Arc Solid Free-Form Fabrication (PTA-SFFF) was investigated. The microstructure and composition were explored through analytical microscopy techniques such as scanning and transmission electron microscopy (SEM, TEM) and electron backscatter diffraction (EBSD). To investigate the isotropic behavior within the additive manufactured Ti–TiB blocks, tensile tests were conducted in longitudinal, diagonal, and lateral directions. A consistent tensile behavior was observed for all the directions, highlighting a nearly isotropic behavior within samples. Shot peening was introduced as a postmanufacturing treatment to enhance the mechanical properties of AM specimens. Shot peening led to a localized increase in hardness at the near-surface where stress-induced twins are noted within the affected microstructure. The RBF-200 HT rotating-beam fatigue machine was utilized to conduct fatigue testing on untreated and shot-peened samples, starting at approximately 1/2 the ultimate tensile strength of the bulk material and testing within low- (<105 cycles) to high-cycle (>105 cycles) regimes. Shot-peened samples experienced significant improvement in fatigue life, increasing the fitted endurance limit from 247.8 MPa for the untreated samples to 318.3 MPa, leading to an increase in fatigue resistance of approximately 28%.


2021 ◽  
Vol 27 (S1) ◽  
pp. 3196-3198
Author(s):  
Geronimo Perez ◽  
André Pimenta ◽  
Jefferson F. D. F de Araujo ◽  
Juan Pardal ◽  
Sergio Maior Tavares ◽  
...  

2020 ◽  
Vol 2 (12) ◽  
pp. 5710-5727
Author(s):  
Gábor Csiszár ◽  
Helena Solodenko ◽  
Robert Lawitzki ◽  
Wenhao Ma ◽  
Christopher Everett ◽  
...  

Iron-oxides form an important class by providing potential solutions in many areas. The accurate composition- and structure analysis is crucial to describe the mechanical aspects and optimize strategy for the design of multi-component core-shell NWs.


Author(s):  
K. Hono

Atomic Probe Field Ion Microscopy (APFIM) is used to solve many critical problems related to microstructures of metallic materials such as nanostructures that are composed of nanoscale precipitates dispersed in a matrix phase. The atom probe technique provides unique information on metallic nanostructures not attainable with other analytical microscopy techniques such as Transmission Electron Microscopy (TEM). In this article the an overview of the contribution of the atom probe technique to enhance the current understanding of solute clustering and characterization of fine precipitates of aluminum alloys.


2017 ◽  
Vol 23 (S1) ◽  
pp. 932-933
Author(s):  
Nestor J. Zaluzec ◽  
Arne Janssen ◽  
Matthew A. Kulzick ◽  
M.G. Burke

2017 ◽  
Vol 41 (1) ◽  
pp. 115-117
Author(s):  
Peter Ingram ◽  
Ann LeFurgey

2016 ◽  
Vol 6 (01) ◽  
pp. 1504
Author(s):  
Shilpa Dinda ◽  
Souradut Ray ◽  
Amal Kumar Mondal*

Plants have unique capability to deposit silicon (si) with and between the cells and thus creating casts of the cells commonly known as silica bodies (plant stones). Silicon are very abundantly present only in the family Poaceae among monocotyledon. These silica bodies contain the composition of silicon to form different structural diversity of stone cells like long or short bar with rounded or semi rounded spheres dumbbell shaped, sinuous elongated rectangular, narrow elliptical rectangular, randle, polylobed and cross shaped etc. Light (LM), Polarized (PM), Fluorescence Microscopy (FM) and Scanning Electron Microscope (SEM) were used for better micro-morphological study. These micro characters might be applied numerically by UPGMA method to solve different taxonomic problems within familial, generic and species level and compared to other systematics.


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