Interface Degradation of Ceramic‐Matrix Composites Under Thermomechanical Fatigue Loading

Ceramics ◽  
2019 ◽  
Vol 2 (2) ◽  
pp. 407-425 ◽  
Author(s):  
Ragav P. Panakarajupally ◽  
Michael J. Presby ◽  
K. Manigandan ◽  
Jianyu Zhou ◽  
George G. Chase ◽  
...  

A combustion facility which includes uniaxial mechanical loading was implemented that enables environmental conditions more akin to jet engine environments compared to conventional static environment tests. Two types of woven SiC/SiC ceramic matrix composites (CMCs), melt-infiltrated (MI) and chemical vapor infiltrated (CVI), were subjected to fatigue loading in the combustion facility and under isothermal furnace conditions. Some CVI test coupons were coated with a multilayer environmental barrier coating (EBC) of mullite + ytterbium monosilicate using slurry infiltration process to demonstrate the performance with a coating. Combustion conditions were applied using a high velocity oxy fuel gun on the front side of the specimen and mechanical loading was applied using a horizontal hydraulic MTS machine. All the specimens considered were subjected to tension-tension fatigue loading at 100 MPa, stress ratio of 0.1 and specimen front-side surface temperature of 1200 ± 20 °C. Nondestructive evaluation (NDE) methods, such as electrical resistance (ER), was used as an in-situ health monitoring technique. Similar fatigue tests were performed in an isothermal furnace for comparison. A much lower fatigue life was observed for the uncoated specimens tested under combustion conditions in comparison to isothermal furnace condition. This difference in fatigue life was attributed to damage associated with added thermal stress due to the thermal gradient and higher rate of oxidative embrittlement due to the presence of high velocity combustion gases in the combustion environment. EBC coating increased the fatigue life in combustion environment. However, EBC coated specimens experienced spallation in the high-velocity flame due to the presence of micro cracks in the coating surface. Fracture surfaces of the failed specimens were investigated under the scanning electron microscope (SEM) to determine the extent of oxidation and damage.


Ceramics ◽  
2019 ◽  
Vol 2 (2) ◽  
pp. 327-346 ◽  
Author(s):  
Longbiao Li

In this paper, the effect of cyclic fatigue loading on matrix multiple fracture of fiber-reinforced ceramic-matrix composites (CMCs) is investigated using the critical matrix strain energy (CMSE) criterion. The relationships between multiple matrix cracking, cyclic fatigue peak stress, fiber/matrix interface wear, and debonding are established. The effects of fiber volume fraction, fiber/matrix interface shear stress, and applied cycle number on matrix multiple fracture and fiber/matrix interface debonding and interface wear are discussed. Comparisons of multiple matrix cracking with/without cyclic fatigue loading are analyzed. The experimental matrix cracking of unidirectional SiC/CAS, SiC/SiC, SiC/Borosilicate, and mini-SiC/SiC composites with/without cyclic fatigue loading are predicted.


Ceramics ◽  
2019 ◽  
Vol 2 (2) ◽  
pp. 347-371 ◽  
Author(s):  
Martin R. Bache ◽  
Christopher D. Newton ◽  
John Paul Jones ◽  
Stephen Pattison ◽  
Louise Gale ◽  
...  

From a disruptive perspective, silicon carbide (SiC)-based ceramic matrix composites (CMCs) provide a considerable temperature and weight advantage over existing material systems and are increasingly finding application in aerospace, power generation and high-end automotive industries. The complex structural architecture and inherent processing artefacts within CMCs combine to induce inhomogeneous deformation and damage prior to ultimate failure. Sophisticated mechanical characterisation is vital in support of a fundamental understanding of deformation in CMCs. On the component scale, “damage tolerant” design and lifing philosophies depend upon laboratory assessments of macro-scale specimens, incorporating typical fibre architectures and matrix under representative stress-strain states. This is important if CMCs are to be utilised to their full potential within industrial applications. Bulk measurements of strain via extensometry or even localised strain gauging would fail to characterise the ensuing inhomogeneity when performing conventional mechanical testing on laboratory scaled coupons. The current research has, therefore, applied digital image correlation (DIC), electrical resistance monitoring and acoustic emission techniques to the room and high-temperature assessment of ceramic matrix composites under axial tensile and fatigue loading, with particular attention afforded to a silicon carbide fibre-reinforced silicon carbide composite (SiCf/SiC) variant. Data from these separate monitoring techniques plus ancillary use of X-ray computed tomography, in-situ scanning electron microscopy and optical inspection were correlated to monitor the onset and progression of damage during mechanical loading. The benefits of employing a concurrent, multi-technique approach to monitoring damage in CMCs are demonstrated.


Author(s):  
Li Longbiao

In this paper, comparisons of thermomechanical fatigue hysteresis loops of fiber-reinforced ceramic-matrix composites (CMCs) subjected to different phase angles of θ = 0, π/3, π/2, and π have been investigated. The shape, location, and area of fatigue hysteresis loops are affected by the phase angle under the thermomechanical cyclic loading. The effects of fiber volume fraction, fatigue peak stress, matrix crack spacing, interface frictional coefficient, and interface debonded energy on the thermomechanical fatigue hysteresis loops and fiber/matrix interface slip of different phase angles are discussed. The fatigue hysteresis loops of cross-ply CMCs under the phase angles of θ = 0 and π are predicted for different fatigue peak stresses and cycle numbers.


Author(s):  
Christopher D. Newton ◽  
J. Paul Jones ◽  
Louise Gale ◽  
Martin R. Bache

The complex structural architecture and inherent processing artefacts within ceramic matrix composites combine to induce inhomogeneous deformation and damage prior to ultimate failure. Sophisticated mechanical characterisation is vital in support of a fundamental understanding of deformation in ceramic matrix composites. On the component scale, “damage tolerant” design and lifing philosophies depend upon laboratory assessments of macro-scale specimens, incorporating typical fibre architectures and matrix under representative stress-strain states. Bulk measurements of strain via extensometry or even localised strain gauging will fail to characterise such inhomogeneity when performing conventional mechanical testing on laboratory scaled coupons. The current research project has, therefore, applied digital image correlation (DIC), electrical resistance monitoring and acoustic emission techniques to the room and high temperature assessment of a SiCf/SiC composite under axial fatigue loading. Data from these separate monitoring techniques plus ancillary use of X-Ray computed tomography and optical inspection were correlated to monitor the onset and progression of damage during cyclic loading.


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