Mechanism of synthesis of anatase TiO 2 pigment from low concentration of titanyl sulfuric–chloric acid solution under hydrothermal hydrolysis

2019 ◽  
Vol 67 (2) ◽  
pp. 277-287 ◽  
Author(s):  
Ming Tian ◽  
Yahui Liu ◽  
Weijing Wang ◽  
Wei Zhao ◽  
Desheng Chen ◽  
...  
Keyword(s):  
Acid Solution ◽  
Chloric Acid ◽  
Low Concentration ◽  
Chloric Acid Solution

scholarly journals The kinetic profile of iron dissolution from laterite ore in chloric acid solution

2019 ◽  
Vol 22 (1) ◽  
pp. 20-37
Author(s):  
Solihin Solihin ◽  
◽  
Pratama Arinaldo ◽  
Nanda Dewi ◽  
Haryadi Permana ◽  
...  
Keyword(s):  
Acid Solution ◽  
Chloric Acid ◽  
Iron Dissolution ◽  
Kinetic Profile ◽  
Chloric Acid Solution ◽  
Laterite Ore

Toxicity of reactive red 141 and basic red 14 to algae and waterfleas

2008 ◽  
Vol 58 (6) ◽  
pp. 1193-1198 ◽  
Author(s):  
S. Vinitnantharat ◽  
W. Chartthe ◽  
A. Pinisakul
Keyword(s):  
Humic Acid ◽  
Acid Solution ◽  
Chlorophyll A ◽  
Small Molecule ◽  
Textile Wastewater ◽  
Dry Weight ◽  
Bulk Solution ◽  
Low Concentration ◽  
Chlorella Sp ◽  
Cell Counts

Textile wastewater normally has a visible color although it has low concentration. This may affect the aquatic ecosystem. Two dyestuffs, Reactive Red 141 (RR141) and Basic Red14 (BR14) were used as compound models. RR 141 is an anionic dye which has a big molecule whereas BR 14 is a cationic dye and has a small molecule. The target organisms for toxicity test were green algae (Chlorella sp.) and waterfleas (Moina macrocopa). The effect of humic acid on the toxicity of dyestuffs to test organisms was also investigated. From the observation of cell counts, Chlorophyll a and dry weight of algae in the dye solutions for 4 days, it was found that all parameters increased as times increased. This revealed that algae could utilize dyestuffs as a carbon source. However, BR14 gave higher absorbance than RR141 at the wavelength of 430 nm which competed to the Chlorophyll a for algal photosynthesis. This resulted in the 96-h EC50 of BR14 and RR141 to Chlorella sp. were 10.88 and 95.55 mg/L, respectively. As for dye toxicity to waterfleas, the 48-h LC50 of BR14 and RR141 to waterfleas were 4.91 and 18.26 mg/L, respectively. The high toxicity of BR14 to waterfleas related to the small molecule of dye could pass into the cell and was absorbed by organelles of waterfleas. Toxicity of BR14 in humic acid solution to Chlorella sp. showed less toxic than RR141 in humic acid solution. This dues to the negative charge of humic acid could bound with a positive charge of BR14, resulted in low amount of BR14 remaining in the bulk solution. The toxicity of BR14 and RR141 in humic acid solution to waterfleas was increased as humic acid increased. Hence, the proper treatment of textile wastewater to yield low concentration of dyes in the effluent before discharging to the natural water is needed.

Electrochemical etching of Ti2AlC to Ti2CTx (MXene) in low-concentration hydrochloric acid solution

2017 ◽  
Vol 5 (41) ◽  
pp. 21663-21668 ◽  
Author(s):  
W. Sun ◽  
S. A. Shah ◽  
Y. Chen ◽  
Z. Tan ◽  
H. Gao ◽  
...  
Keyword(s):  
Hydrochloric Acid ◽  
Acid Solution ◽  
Hydrochloric Acid Solution ◽  
Dilute Hydrochloric Acid ◽  
Electrochemical Etching ◽  
Low Concentration ◽  
Porous Ti

In this study, we successfully demonstrate the electrochemical etching of Al from porous Ti2AlC electrodes in dilute hydrochloric acid to form a layer of Ti2CTx MXene on Ti2AlC.

CIRCULAR PAPER CHROMATOGRAPHIC METHOD FOR DETERMINING TRACE AMOUNTS OF COBALT, COPPER, NICKEL, AND ZINC IN ROCKS AND SOILS

1965 ◽  
Vol 2 (2) ◽  
pp. 33-43 ◽  
Author(s):  
D. C. Mah ◽  
S. Mah ◽  
W. M. Tupper
Keyword(s):  
Acid Solution ◽  
Paper Chromatography ◽  
Chloric Acid Solution ◽  
Rubeanic Acid ◽  
Circular Paper ◽  
Color Indicator ◽  
Higher Sensitivity ◽  
Circular Chromatography ◽  
Cobalt Copper

Ascending, descending, and horizontal (circular) methods of paper chromatography were explored and compared. Circular chromatography was found to be the most suitable; it requires shorter development time, has more definite Rf values, less tailing, higher sensitivity, and better precision than ascending or descending methods.A methyl ethyl ketone: hydrochloric acid solution (93:7 v/v) is used as a developing solvent for cobalt, copper, and nickel, and a 1-butanol: 1 N hydro–chloric acid solution (7:3 v/v) is used as a solvent for zinc. Good separations were obtained with these solvents and no critical interferences were noted. Benzidine – rubeanic acid is used as a color indicator for cobalt, copper, and nickel; and dithizone (0.01%) for zinc. This method has an absolute sensitivity of 0.005 μg for zinc, and 0.02 μg for cobalt, copper, and nickel. Precision is estimated at ± 10%.Methods have also been developed for determining bismuth, silver, and tin.The separation of elements from complex mixtures by paper chromatography and by quantitative determination of the amounts present by emission spectrography have been investigated. This rarely considered process offers promise, because the sensitivity of several elements is higher in emission spectrography than in colorimetry.

Extended Preservation of Iron for Transmission

1967 ◽  
Vol 25 ◽  
pp. 354-355
Author(s):  
E. P. Abrahamson II ◽  
M. W. Dumais
Keyword(s):  
Acid Solution ◽  
Perchloric Acid ◽  
Microscopy Study ◽  
Perchloric Acid Solution ◽  
Transmission Microscopy ◽  
Iron Base ◽  
Cold Stage

In a transmission microscopy study of iron and dilute iron base alloys, it was determined that it is possible to preserve specimens for extended periods of time. Our specimens were prepunched from 5 to 8 mil sheet to microscope size and annealed for several hours at 700°C. They were then thinned in a glacial acetic-12 percent perchloric acid solution using 10 volts and 20 milliamperes, at a temperature of 8 to 14°C.It was noted that by the use of a cold stage, the same specimen can be observed for periods up to one week without excess contamination. When removal of the specimen from the column becomes necessary, it was observed that a specimen may be kept for later observation in 1,2 dichloroethene or methanol for periods in excess of two weeks.

Deposited emulsion particles in the pores of aluminum oxide film

1978 ◽  
Vol 36 (1) ◽  
pp. 450-451
Author(s):  
Michio Ashida ◽  
Yasukiyo Ueda
Keyword(s):  
Oxide Film ◽  
Acid Solution ◽  
Barrier Layer ◽  
Colloidal Particles ◽  
Oxalic Acid Solution ◽  
Anodic Oxide ◽  
Anodic Oxide Film ◽  
Carbon Replica ◽  
Sectioning Method ◽  
Thin Sectioning

An anodic oxide film is formed on aluminum in an acidic elecrolyte during anodizing. The structure of the oxide film was observed directly by carbon replica method(l) and ultra-thin sectioning method(2). The oxide film consists of barrier layer and porous layer constructed with fine hexagonal cellular structure. The diameter of micro pores and the thickness of barrier layer depend on the applying voltage and electrolyte. Because the dimension of the pore corresponds to that of colloidal particles, many metals deposit in the pores. When the oxide film is treated as anode in emulsion of polyelectrolyte, the emulsion particles migrate onto the film and deposit on it. We investigated the behavior of the emulsion particles during electrodeposition.Aluminum foils (99.3%) were anodized in either 0.25M oxalic acid solution at 30°C or 3M sulfuric acid solution at 20°C. After washing with distilled water, the oxide films used as anode were coated with emulsion particles by applying voltage of 200V and then they were cured at 190°C for 30 minutes.

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