An intumescent flame retardant system using β-cyclodextrin as a carbon source in polylactic acid (PLA)

2011 ◽  
Vol 22 (7) ◽  
pp. 1115-1122 ◽  
Author(s):  
Jian-Xiang Feng ◽  
Sheng-Pei Su ◽  
Jin Zhu
Keyword(s):  
Carbon Source ◽  
Flame Retardant ◽  
Polylactic Acid ◽  
Intumescent Flame Retardant

scholarly journals Investigation of melt spinnability of plasticized polylactic acid biocomposites-containing intumescent flame retardant

2019 ◽  
Vol 139 (1) ◽  
pp. 305-318 ◽  
Author(s):  
Muhammad Maqsood ◽  
Fabian Langensiepen ◽  
Gunnar Seide
Keyword(s):  
Flame Retardant ◽  
Polylactic Acid ◽  
Intumescent Flame Retardant

scholarly journals Preparation of β-Cyclodextrin Inclusion Complex and Its Application as an Intumescent Flame Retardant for Epoxy

Polymers ◽  
2019 ◽  
Vol 11 (1) ◽  
pp. 71 ◽  
Author(s):  
Xueying Shan ◽  
Kuanyu Jiang ◽  
Jinchun Li ◽  
Yan Song ◽  
Ji Han ◽  
...  
Keyword(s):  
Carbon Source ◽  
Inclusion Complex ◽  
Flame Retardant ◽  
1H Nmr ◽  
Intumescent Flame Retardant ◽  
Molar Ratio ◽  
Gravimetric Analysis ◽  
X Ray ◽  
Cone Calorimeter Test ◽  
The Impact

A new P-N containing the flame retardant, which was namely N,N′-dibutyl-phosphate diamide (DBPDA), was synthesized and it was assembled into the cavity of β-cyclodextrin (β-CD) to form an inclusion complex (IC). The structure and properties of IC were characterized by Fourier transform infraredspectroscopy (FTIR), wide-angle X-ray diffraction (WAXD), 1H nuclear magnetic resonance (1H NMR), scanning electron microscopy with X-ray microanalysis (SEM-EDS), differential scanning calorimeter (DSC) and thermal gravimetric analysis (TGA). 1H NMR and SEM-EDS were also used to identify the molar ratio of β-CD/DBPDA in IC and the results from the analyses indicated that their molar ratio was 1:1. In order to test the flame retardant effect of IC, it was added to epoxy (EP). IC was proposed to be able to act as an intumescent flame retardant (IFR) system in EP through a combination of β-CD and DBPDA properties during the combustion process. β-CD is a biomass carbon source, which has the advantages of environmental protection and low cost. Furthermore, DBPDA is both a source of acid and gas. When IC was heated, IC had the advantage of acting as both a carbon source and foam forming agent, while the DBPDA component were able to directly generate phosphoric acid and NH3 in situ. The impact of IC in low additive amounts on flame retardancy of EP was studied by the cone calorimeter test. When only 3 wt % IC was incorporated, the peak values of heat release rate (pHRR) and smoke production rate (pSPR) of EP were reduced by 22.9% and 33.3% respectively, which suggested that IC could suppress the heat and smoke release efficiently.

The Preparation of an Intumescent Flame Retardant by Ion Exchange and Its Application in Polylactic Acid

2019 ◽  
Vol 1 (4) ◽  
pp. 755-764 ◽  
Author(s):  
Xiaodong Jin ◽  
Suping Cui ◽  
Shibing Sun ◽  
Xiaoyu Gu ◽  
Hongfei Li ◽  
...  
Keyword(s):  
Ion Exchange ◽  
Flame Retardant ◽  
Polylactic Acid ◽  
Intumescent Flame Retardant

Study on Rheological Properties of Polylactic Acid Retardant System

2014 ◽  
Vol 488-489 ◽  
pp. 293-296
Author(s):  
Dong Ze Li ◽  
Xiao Chuan Jia ◽  
Xiu Ping Lu ◽  
Sheng Jia Zhai
Keyword(s):  
Flame Retardant ◽  
Rheological Properties ◽  
Polylactic Acid ◽  
Flow Rate ◽  
Flame Retardants ◽  
Complex Viscosity ◽  
Intumescent Flame Retardant ◽  
Melt Flow ◽  
Melt Flow Rate ◽  
Scanning Frequency

A series of polylactic acid (PLA)/IFR composites was prepared by melt blending method.Capillary rheometer and rotary rheometer were applied to investigate the effects of and flame retardants on rheological properties. The results of the rheological test show that the melt flow rate increases with the increasing of content of Intumescent flame retardant. Intumescent flame retardant joined making PLA system flow rate is larger than pure PLA, melt flow rate increases, apparent viscosity decreases, relaxation time decreases, and the complex viscosity decreases gradually with the increase of scanning frequency.

Effect of nickel phytate on flame retardancy of intumescent flame retardant polylactic acid

2020 ◽  
Author(s):  
Weiguang Gong ◽  
Min Fan ◽  
Ji Luo ◽  
Juan Liang ◽  
Xin Meng
Keyword(s):  
Flame Retardant ◽  
Polylactic Acid ◽  
Flame Retardancy ◽  
Intumescent Flame Retardant

The fire performance of polylactic acid containing a novel intumescent flame retardant and intercalated layered double hydroxides

2017 ◽  
Vol 52 (20) ◽  
pp. 12235-12250 ◽  
Author(s):  
Xiaodong Jin ◽  
Xiaoyu Gu ◽  
Chen Chen ◽  
Wufei Tang ◽  
Hongfei Li ◽  
...  
Keyword(s):  
Flame Retardant ◽  
Polylactic Acid ◽  
Layered Double Hydroxides ◽  
Intumescent Flame Retardant ◽  
Fire Performance ◽  
Double Hydroxides

A green intumescent flame retardant system using inositol‐based carbon source: Preparation and characteristics in polypropylene

2021 ◽  
Author(s):  
Siyin Ding ◽  
Peng Liu ◽  
Shimin Zhang ◽  
Yanfen Ding ◽  
Feng Wang ◽  
...  
Keyword(s):  
Carbon Source ◽  
Flame Retardant ◽  
Intumescent Flame Retardant ◽  
Source Preparation
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