Microstructural Evolution of Nafion During Uniaxial Deformation Monitored by X-ray Scattering

2011 ◽  
pp. 21-24
Author(s):  
Meredith N. Silberstein ◽  
J. David Londono ◽  
Mary C. Boyce
Keyword(s):  
Microstructural Evolution ◽  
Uniaxial Deformation ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Microstructural Evolution of Long-Period Stacking Ordered Structures in Mg97Y2Zn1 Alloys Examined by In-Situ Small-Angle X-ray Scattering

2014 ◽  
Vol 45 (11) ◽  
pp. 4780-4785 ◽  
Author(s):  
Hiroshi Okuda ◽  
Toshiki Horiuchi ◽  
Shoki Hifumi ◽  
Michiaki Yamasaki ◽  
Yoshihito Kawamura ◽  
...  
Keyword(s):  
Microstructural Evolution ◽  
Small Angle ◽  
Ordered Structures ◽  
X Ray ◽  
Long Period ◽  
X Ray Scattering ◽  
Ray Scattering

Uniaxial deformation of overstretched polyethylene: In-situ synchrotron small angle X-ray scattering study

Polymer ◽  
2007 ◽  
Vol 48 (17) ◽  
pp. 5125-5132 ◽  
Author(s):  
Yujing Tang ◽  
Zhiyong Jiang ◽  
Yongfeng Men ◽  
Lijia An ◽  
Hans-Friedrich Enderle ◽  
...  
Keyword(s):  
Small Angle ◽  
Uniaxial Deformation ◽  
X Ray ◽  
X Ray Scattering ◽  
Scattering Study ◽  
Ray Scattering

System forin situobservation of three-dimensional structural changes in polymer films during uniaxial deformation

2015 ◽  
Vol 48 (4) ◽  
pp. 1016-1022 ◽  
Author(s):  
Tsukasa Miyazaki ◽  
Keisuke Shimokita ◽  
Hiroki Ogawa ◽  
Katsuhiro Yamamoto
Keyword(s):  
Structural Characterization ◽  
Evaluation System ◽  
Structural Changes ◽  
Three Dimensional ◽  
Poly Vinyl Alcohol ◽  
Two Dimensional ◽  
Uniaxial Deformation ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

A simple three-dimensional structural evaluation system for a film during uniaxial deformation has been developed. The system is realized with an automatic film stretching machine, which allows the horizontally symmetric stretching of a film, and a synchrotron radiation X-ray scattering apparatus. Using this system, two-dimensional patterns of small-angle X-ray scattering and wide-angle X-ray diffraction can be obtained simultaneously during film stretching in the so-called edge and end views, together with stress–strain data. As cylindrical symmetry of the structure can be expected for a uniaxially stretched film, the two-dimensional patterns in the through view are identical to those in the edge view, indicating that three-dimensional structural characterization can be performed with a combination of edge and end views during film stretching. For amorphous poly(ethylene terephthalate) and crystalline poly(vinyl alcohol) films, the preliminary results of three-dimensional structural characterization during film stretching are shown.

scholarly journals Structural Evolution of LLDPE-LMW/HMW Blend during Uniaxial Deformation as Revealed by In Situ Synchrotron Radiation X-ray Scattering

2020 ◽  
Vol 39 (1) ◽  
pp. 102-112
Author(s):  
Pin-Zhang Chen ◽  
Hao-Yuan Zhao ◽  
Zhi-Jie Xia ◽  
Qian-Lei Zhang ◽  
Dao-Liang Wang ◽  
...  
Keyword(s):  
Synchrotron Radiation ◽  
Structural Evolution ◽  
Uniaxial Deformation ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Synchrotron X-ray scattering study on amorphous poly(ethylene furanoate) under uniaxial deformation

Polymer ◽  
2018 ◽  
Vol 139 ◽  
pp. 60-67 ◽  
Author(s):  
Yimin Mao ◽  
David G. Bucknall ◽  
Robert M. Kriegel
Keyword(s):  
Uniaxial Deformation ◽  
X Ray ◽  
X Ray Scattering ◽  
Scattering Study ◽  
Poly Ethylene ◽  
Ray Scattering

Microtubule nucleation sequence studied by time-resolved x-ray scattering and electron microscopy

1983 ◽  
Vol 41 ◽  
pp. 766-767
Author(s):  
Eva-Maria Mandelkow ◽  
Eckhard Mandelkow ◽  
Joan Bordas
Keyword(s):  
Electron Microscopy ◽  
Dynamic Equilibrium ◽  
Time Resolved ◽  
X Ray ◽  
Additional Information ◽  
X Ray Scattering ◽  
Low Concentrations ◽  
Microtubule Growth ◽  
Ray Patterns ◽  
Ray Scattering

When a solution of microtubule protein is changed from non-polymerising to polymerising conditions (e.g. by temperature jump or mixing with GTP) there is a series of structural transitions preceding microtubule growth. These have been detected by time-resolved X-ray scattering using synchrotron radiation, and they may be classified into pre-nucleation and nucleation events. X-ray patterns are good indicators for the average behavior of the particles in solution, but they are difficult to interpret unless additional information on their structure is available. We therefore studied the assembly process by electron microscopy under conditions approaching those of the X-ray experiment. There are two difficulties in the EM approach: One is that the particles important for assembly are usually small and not very regular and therefore tend to be overlooked. Secondly EM specimens require low concentrations which favor disassembly of the particles one wants to observe since there is a dynamic equilibrium between polymers and subunits.

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