Improving the Vitamin-E Concentration in Crude Palm Oil Using Hot Compressed Water Technology

Author(s):  
Mohd Sharizan Md Sarip ◽  
Nor Azian Morad ◽  
Mohd Al Hafiz Mohd Nawi ◽  
Mohd Rizuan Mansor ◽  
Lokman Hakim Ibrahim
2016 ◽  
Vol 169 ◽  
pp. 103-112 ◽  
Author(s):  
Mohd Sharizan Md Sarip ◽  
Noor Azian Morad ◽  
Yoshiyuki Yamashita ◽  
Tomoya Tsuji ◽  
Mohd Azizi Che Yunus ◽  
...  

2019 ◽  
Vol 59 (8) ◽  
pp. 1491
Author(s):  
P. Areerob ◽  
W. Dahlan ◽  
K. Angkanaporn

Crude palm oil (CPO) is a valuable energy supplement for poultry diets and a rich source of vitamin A and E. Data on the effect of vitamin E tocotrienol in CPO on laying hen metabolism are limited. The present study examined the effects of dietary CPO supplementation on the performance and tissue distribution of vitamin E in laying hens and on egg quality. In total, 144 49-week old Hysex Brown hens were allocated randomly into four groups (36 per group), in single cages, and received corn–soybean basal diet supplemented with either lard at 20 g/kg (control), or CPO at 20 (CPO1), 30 (CPO2) or 40 g/kg (CPO3). Egg quality, hen performance, egg yolk cholesterol and hen tissue concentrations of vitamin E were examined. Dietary supplementation with CPO increased the egg yolk colour, egg and yolk weight compared with the control group, but not specific gravity, albumen quality, albumen weight and shell weight. Importantly, CPO supplementation significantly decreased egg yolk cholesterol concentrations (lowest level in the CPO3 group) and enhanced (P < 0.05) the total vitamin E tocopherols in CPO1 and total tocotrienols in CPO2 and CPO3. Hens fed on CPO3 had the lowest total tocopherol concentrations in their egg yolk and adipose tissue, but the highest tocotrienol in their plasma, egg yolk and adipose tissue. In addition, dietary CPO supplementation resulted in the highest deposition of tocotrienol in the hen’s adipose tissue compared with in the egg yolk, or hen’s liver and plasma. In conclusion, dietary supplementation with CPO improved the egg yolk weight and yolk colour, while it reduced the total cholesterol concentration and resulted in more vitamin E in the egg and hen’s adipose tissue, with increased concentrations of α-tocopherol, α-tocotrienol and γ-tocotrienol.


2014 ◽  
Vol 69 (4) ◽  
Author(s):  
Cici Maarasyid ◽  
Ida Idayu Muhamad ◽  
Eko Supriyanto

Vitamin E is essential in the human body which naturally found in vegetable fats and oil and their derived products. Several palm-based oils obtained from palm oil mills and refineries were revised in this paper as the raw material for vitamin E. Tocopherols and tocotrienols isomers of the vitamin E content are found nearly comparable with crude palm oil. To obtain the tocopherols and tocotrienols, various developed technologies for the extraction were also reviewed. These include the solvent-based extraction, chemical modification, adsorption, enzymatic process, molecular distillation, microwave-assisted extraction and membrane technology. Each of the technologies has the advantages as well as limitations. Therefore, process design and selection for the chosen technology are crucial in order to determine recovery of vitamin E obtained, time efficiency, cost effectiveness, safety of products and environmentally friendly impacts. A green technology approach could be further diversified and manifested for sustainable process of vitamin E.  


2016 ◽  
Vol 80 (2) ◽  
Author(s):  
Irma KRESNAWATY ◽  
Asmini BUDIANI ◽  
. TRI-PANJI ◽  
. SUHARYANTO

AbstractIn order to increase  value added  and  to support downstream industry of  palm oil, minor components of the oil such as β-carotene and vitamin E should be utilized. Vitamin E is a high value  vitamin  that could be used as material for pharmaceutical and  neutraceutical products. Technological constraints encountered in the utilization of  vitamin E from CPO are lack of optimal extraction and purification method as well as the way to stabilize of the product. The research was conducted to find optimal extraction and purification method of vitamin E from CPO and microencapsulation method of vitamin E as pharmaceutical and neutraceutical product. The research showed that vitamin E could be recovered  from CPO by several steps process including saponification using NaOH, separation of unsaponificated  solution,  followed by dissolution using 2-propanol in hexane and extraction  using methanol. Raw extract of vitamin E was then purified by coloumn chromatography with stationary phase of silica gel and mobile phase (eluent) of petroleum benzene/ diethyl ether/acetic acid 70 : 30 : 0,2. Purified vitamin E could be collected as fraction 4-8. Vitamin E obtained  had  similar antioxidant activity as in pure vitamin E (Sigma) and vitamin C. Microencapsulation method could be conducted using arabic gum as coating material followed by spray drying and resulted IC50-DPPH value 132.55  ppm which considered middle activity category.AbstrakUntuk meningkatkan nilai tambah dan mengem-bangkan industri hilir minyak kelapa sawit (CPO), komponen minor minyak tersebut seperti vitamin E dan β-karoten perlu dimanfaatkan. Vitamin E merupakan produk bernilai ekonomis tinggi sebagai bahan farmaseutikal dan neutrasetikal. Kendala yang dihadapi dalam pemanfaatan vitamin E dari CPO, yaitu belum tersedianya teknik ekstraksi dan purifikasi yang optimal dan cara memper-tahankan stabilitas vitamin E. Penelitian ini bertujuan untuk memperoleh teknik ekstraksi dan purifikasi vitamin E dari CPO dan teknik mikroenkapsulasi vitamin E sebagai bahan farmaseutikal dan neutrasetikal.  Hasil penelitian menunjukkan bahwa vitamin E dapat diproduksi dengan beberapa tahapan yakni saponifikasi dengan NaOH, pemisahan lapisan pekat tak tersabunkan, pelarutan dengan2-propanol dalam heksana, ekstraksi dengan metanol dan pelarutan ekstrak dengan 2-propanol dalam heksana. Ekstrak kasar vitamin E dimurnikan dengan kromatografi kolom dengan fasa diam silika gel dan fasa gerak petroleum benzen/dietil eter/asam asetat = 70 : 30 : 0,2. Vitamin E dapat dimurnikan pada fraksi ke-4 sampai dengan ke-8. Aktivitas antioksidan vitamin E hasil ekstraksi tersebut setara dengan vitamin E murni (Sigma). Teknik mikroenkapsulasi vitamin E hasil ekstraksi dari CPO dapat dilakukan dengan penyalut gum arab dan pengeringan dengan spray dryer  yang menghasilkan anti-oksidan dengan aktivitas IC50 DPPH = 132,55 ppm yang termasuk kategori beraktivitas sedang.


2016 ◽  
Vol 80 (2) ◽  
Author(s):  
Irma KRESNAWATY ◽  
Asmini BUDIANI ◽  
. TRI-PANJI ◽  
. SUHARYANTO

AbstractIn order to increase  value added  and  to support downstream industry of  palm oil, minor components of the oil such as β-carotene and vitamin E should be utilized. Vitamin E is a high value  vitamin  that could be used as material for pharmaceutical and  neutraceutical products. Technological constraints encountered in the utilization of  vitamin E from CPO are lack of optimal extraction and purification method as well as the way to stabilize of the product. The research was conducted to find optimal extraction and purification method of vitamin E from CPO and microencapsulation method of vitamin E as pharmaceutical and neutraceutical product. The research showed that vitamin E could be recovered  from CPO by several steps process including saponification using NaOH, separation of unsaponificated  solution,  followed by dissolution using 2-propanol in hexane and extraction  using methanol. Raw extract of vitamin E was then purified by coloumn chromatography with stationary phase of silica gel and mobile phase (eluent) of petroleum benzene/ diethyl ether/acetic acid 70 : 30 : 0,2. Purified vitamin E could be collected as fraction 4-8. Vitamin E obtained  had  similar antioxidant activity as in pure vitamin E (Sigma) and vitamin C. Microencapsulation method could be conducted using arabic gum as coating material followed by spray drying and resulted IC50-DPPH value 132.55  ppm which considered middle activity category.AbstrakUntuk meningkatkan nilai tambah dan mengem-bangkan industri hilir minyak kelapa sawit (CPO), komponen minor minyak tersebut seperti vitamin E dan β-karoten perlu dimanfaatkan. Vitamin E merupakan produk bernilai ekonomis tinggi sebagai bahan farmaseutikal dan neutrasetikal. Kendala yang dihadapi dalam pemanfaatan vitamin E dari CPO, yaitu belum tersedianya teknik ekstraksi dan purifikasi yang optimal dan cara memper-tahankan stabilitas vitamin E. Penelitian ini bertujuan untuk memperoleh teknik ekstraksi dan purifikasi vitamin E dari CPO dan teknik mikroenkapsulasi vitamin E sebagai bahan farmaseutikal dan neutrasetikal.  Hasil penelitian menunjukkan bahwa vitamin E dapat diproduksi dengan beberapa tahapan yakni saponifikasi dengan NaOH, pemisahan lapisan pekat tak tersabunkan, pelarutan dengan2-propanol dalam heksana, ekstraksi dengan metanol dan pelarutan ekstrak dengan 2-propanol dalam heksana. Ekstrak kasar vitamin E dimurnikan dengan kromatografi kolom dengan fasa diam silika gel dan fasa gerak petroleum benzen/dietil eter/asam asetat = 70 : 30 : 0,2. Vitamin E dapat dimurnikan pada fraksi ke-4 sampai dengan ke-8. Aktivitas antioksidan vitamin E hasil ekstraksi tersebut setara dengan vitamin E murni (Sigma). Teknik mikroenkapsulasi vitamin E hasil ekstraksi dari CPO dapat dilakukan dengan penyalut gum arab dan pengeringan dengan spray dryer  yang menghasilkan anti-oksidan dengan aktivitas IC50 DPPH = 132,55 ppm yang termasuk kategori beraktivitas sedang.


2018 ◽  
Vol 1019 ◽  
pp. 012088
Author(s):  
Mohd Sharizan Md Sarip ◽  
Noor Azian Morad ◽  
Syahrul Affandi Saidi ◽  
Nazmizan Muhammad

2013 ◽  
Vol 37 (3) ◽  
pp. 181 ◽  
Author(s):  
Firman Nasiu ◽  
Lies Mira Yusiati ◽  
Supadmo (Supadmo)

<p>Penelitian ini bertujuan untuk mengetahui pengaruh suplementasi vitamin E dalam ransum yang mengandung minyak sawit mentah terkapsulasi (Capsulated Crude Palm Oil-CCPO) terhadap performan ternak dan kandungan polyunsaturated fatty acid (PUFA) daging kambing Bligon. Rumput raja sebanyak 65%, bekatul 20%, dan bungkil kacang kedelai 15% dengan penambahan 3% capsulated crude palm oil (CCPO) digunakan sebagai ransum kontrol. Ternak yang digunakan adalah kambing Bligon jantan sebanyak 9 ekor yang dibagi dalam 3 kelompok perlakuan yang terdiri atas kelompok pertama hanya mendapat ransum kontrol tanpa suplementasi vitamin E, kelompok kedua mendapat ransum kontrol dengan suplementasi vitamin E 200 mg per kg bahan kering pakan, kelompok ketiga mendapat ransum kontrol dengan suplementasi vitamin E 400 mg per kg bahan kering pakan. Hasil penelitian menunjukkan bahwa suplementasi vitamin E sampai level 400 mg/kg bahan kering tidak berpengaruh terhadap performan ternak, kandungan PUFA, dan komposisi kimia, namun cenderung menurunkan kadar malondialdehyde (MDA) daging (P&lt;0,06) sebesar 67,52%, meningkatkan kandungan vitamin E sebesar 74,80% namun diikuti oleh peningkatan kandungan kolesterol daging.</p><p><br />(Kata kunci: Vitamin E, Performan ternak, PUFA daging)</p>


2019 ◽  
Vol 1 (2) ◽  
Author(s):  
Sarono Sarono

The empty fruit bunches (EFB) are by-product of crude palm oil (CPO) production, and it is not widely used optimally. One of products produced from EFB with development potentials is straw mushroom. The objective of this research was to analyze the potentials of EFB material and straw mushroom based on EFB material in Lampung province. The result showed that the EFB potential in Lampung province was 111,144 ton annually and straw mushroom was 4,835 ton annually. The biology efficiency ratio of EFB into straw mushroom in production scale was averagely 3.93%. Districts having potentials for developing straw mushroom business by using EFB material were Mesuji, Middle Lampung, Tulang Bawang, Way Kanan, and North Lampung.


2018 ◽  
Vol 17 (2) ◽  
pp. 123
Author(s):  
Noryati Ahmad ◽  
Ahmad Danial Zainudin ◽  
Fahmi Abdul Rahim ◽  
Catherine S F Ho

Since its establishment, Crude Palm Oil futures contract (FCPO) has been used to directly hedge its physical crude palm oil (CPO). However, due to the excessive speculation activities on crude palm oil futures market, it has been said to be no longer an effective hedging tool to mitigate the price risk of its underlying physical market. This triggers the need for market players to find possible alternatives to ensure that the hedging role can be executed effectively. Thus this investigation attempts to examine whether other inter-related grains and oil seed futures contracts could serve as effective cross-hedging mechanisms for the CPO. Weekly data of inter-related futures contracts from Chicago Board of Trade (CBOT) and Dalian Commodity Exchange (DCE) are employed to cross hedge the physical crude palm oil prices. The study starts from 2006 until 2016. Empirical results indicate that FCPO is still the best futures contract for hedging purposes while Chicago Soybean (CBOTBO) provides second best alternative if cross-hedging is considered. Keywords: Crude palm oil, Crude palm oil futures, Cross Hedging, Optimal Hedge Ratio, Effective Hedging


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