Systematic Errors in the Determination of Trace Metals by GFAAS Technique, Part I

2003 ◽  
Vol 143 (1) ◽  
pp. 13-17 ◽  
Author(s):  
Beata Godlewska-Zylkiewicz ◽  
Barbara Lesniewska ◽  
Jerzy Golimowski
Keyword(s):  
Trace Metals ◽  
Systematic Errors

Systematic Errors in the Determination of Trace Metals, Part II. Memory Effects of Quartz Vessels Used for Sample Preparation in the Determination of Ultra-Trace Levels of Platinum

2005 ◽  
Vol 150 (1) ◽  
pp. 55-58 ◽  
Author(s):  
Joanna Kowalska ◽  
Monika Asztemborska ◽  
Beata Godlewska-Żyłkiewicz ◽  
Jerzy Golimowski
Keyword(s):  
Trace Metals ◽  
Sample Preparation ◽  
Systematic Errors ◽  
Memory Effects ◽  
Ultra Trace

Statistics and parallaxes

1978 ◽  
Vol 48 ◽  
pp. 7-29
Author(s):  
T. E. Lutz
Keyword(s):  
Experimental Design ◽  
Statistical Methods ◽  
Review Paper ◽  
Systematic Errors ◽  
Past Experience ◽  
Random Errors ◽  
Trigonometric Parallaxes ◽  
Systematic And Random Errors

This review paper deals with the use of statistical methods to evaluate systematic and random errors associated with trigonometric parallaxes. First, systematic errors which arise when using trigonometric parallaxes to calibrate luminosity systems are discussed. Next, determination of the external errors of parallax measurement are reviewed. Observatory corrections are discussed. Schilt’s point, that as the causes of these systematic differences between observatories are not known the computed corrections can not be applied appropriately, is emphasized. However, modern parallax work is sufficiently accurate that it is necessary to determine observatory corrections if full use is to be made of the potential precision of the data. To this end, it is suggested that a prior experimental design is required. Past experience has shown that accidental overlap of observing programs will not suffice to determine observatory corrections which are meaningful.

Systematic errors in equilibrium composition of ternary liquid-liquid systems and their effect on the calculated number of theoretical stages of countercurrent extraction

1988 ◽  
Vol 53 (6) ◽  
pp. 1172-1180
Author(s):  
Ján Dojčanský ◽  
Soňa Bafrncová ◽  
Július Surový
Keyword(s):  
Equilibrium Composition ◽  
Systematic Errors ◽  
Liquid Equilibrium ◽  
Countercurrent Extraction ◽  
Liquid Systems ◽  
Equilibrium Concentrations ◽  
Line Slope ◽  
Tie Line ◽  
Calculated Number

The influence of magnitude of systematic errors in the determination of ternary liquid-liquid equilibrium concentrations on the accuracy of the calculated number of theoretical stages of countercurrent extraction is evaluated on using five hypothetical systems differing in the extent of mutual solubility of components, tie-line slope, and type of binodal curve.

Automated digestion and extraction apparatus for use in the determination of trace metals in foodstuffs

The Analyst ◽  
1978 ◽  
Vol 103 (1225) ◽  
pp. 317 ◽  
Author(s):  
C. J. Jackson ◽  
D. G. Porter ◽  
A. L. Dennis ◽  
P. B. Stockwell
Keyword(s):  
Trace Metals ◽  
Extraction Apparatus

Intercomparison of different methods for the determination of trace metals in seawater

1983 ◽  
Vol 13 (4) ◽  
pp. 327-339 ◽  
Author(s):  
Lutz Brügmann ◽  
Lars-Göran Danielsson ◽  
Bertil Magnusson ◽  
Stig Westerlund
Keyword(s):  
Trace Metals

scholarly journals Determination of trace metals in water from Mangueira Lagoon – RS, Brazil

2018 ◽  
Vol 13 (3) ◽  
pp. 612-620
Author(s):  
Filipe Sousa dos Santos ◽  
Eduarda Medran Rangel ◽  
Pedro José Sanches Filho
Keyword(s):  
Trace Metals ◽  
Atomic Emission ◽  
Atomic Absorption Spectrophotometry ◽  
Emission Spectrometry ◽  
Chemical Parameters ◽  
Chelex 100 ◽  
Physical Chemical ◽  
Low Degree ◽  
Copper Zinc

Abstract Determination of trace metals was carried out in Mangueira Lagoon, in the southern zone of Rio Grande do Sul. Samples were collected at five points to evaluate the concentrations of the following trace metals: copper, zinc, lead, chromium, nickel and iron. Metals were determined by digestion with concentrated nitric acid and pre-concentrated in Chelex 100 resin analyzed by atomic absorption spectrophotometry. In parallel, the physical-chemical parameters pH, chlorides, alkalinity, hardness and organic matter in the water were determined. Potassium and sodium metals were analyzed by atomic emission spectrometry. The analyzes of pH and conductance were analyzed in the field while the others were done in the laboratory of the research group of environmental contaminants (GPCA). Through the results of physical-chemical parameters of the water, the Mangueira Lagoon exhibits a low degree of contamination, but in the future may compromise the biota of the lagoon. Regarding the focus of this work, of Cu, Cr, Fe, Ni, Pb, and Zn (heavy metals), only lead and iron obtained the values above that are established in CONAMA 357/2005.

Atomic-absorption spectrometric determination of trace metals in zirconium and zircaloy by discrete sample nebulization

Talanta ◽  
1985 ◽  
Vol 32 (8) ◽  
pp. 641-644 ◽  
Author(s):  
Daniel A. Batistoni ◽  
Ligia H. Erlijman ◽  
Maria I. Fuertes
Keyword(s):  
Trace Metals ◽  
Atomic Absorption ◽  
Discrete Sample ◽  
Atomic Absorption Spectrometric
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