Thermal degradation of poly(arylene sulfide sulfone)/N-methylpyrrolidone crystal solvate

2009 ◽  
Vol 28 (1) ◽  
pp. 85-91 ◽  
Author(s):  
Xiao-jun Wang ◽  
Mei-lin Zhang ◽  
Jing Liu ◽  
Gang Zhang ◽  
Jie Yang
1981 ◽  
Vol 42 (C1) ◽  
pp. C1-301-C1-307
Author(s):  
I. T. Ritchie ◽  
J. Spitz
Keyword(s):  

Author(s):  
Sh.M. Rakhimbayev ◽  
◽  
T.V. Anikanova ◽  
I.M. Kolesnikov ◽  
◽  
...  

2016 ◽  
Vol 38 (4) ◽  
pp. 302-306
Author(s):  
V.V. Boyko ◽  
◽  
O.A. Radchenko ◽  
S.V. Riabov ◽  
S.I. Sinelnikov ◽  
...  

2013 ◽  
Vol 56 (4) ◽  
pp. 133-135
Author(s):  
Yuki IKEDA ◽  
Satoru IWAMORI ◽  
Hiroyuki MATSUMOTO ◽  
Kiyoshi YOSHINO ◽  
Itsuo NISHIYAMA ◽  
...  

Author(s):  
P. Singh ◽  
G.T. Galyon ◽  
J. Obrzut ◽  
W.A. Alpaugh

Abstract A time delayed dielectric breakdown in printed circuit boards, operating at temperatures below the epoxy resin insulation thermo-electrical limits, is reported. The safe temperature-voltage operating regime was estimated and related to the glass-rubber transition (To) of printed circuit board dielectric. The TG was measured using DSC and compared with that determined from electrical conductivity of the laminate in the glassy and rubbery state. A failure model was developed and fitted to the experimental data matching a localized thermal degradation of the dielectric and time dependency. The model is based on localized heating of an insulation resistance defect that under certain voltage bias can exceed the TG, thus, initiating thermal degradation of the resin. The model agrees well with the experimental data and indicates that the failure rate and truncation time beyond which the probability of failure becomes insignificant, decreases with increasing glass-rubber transition temperature.


2017 ◽  
Vol 68 (2) ◽  
pp. 317-322
Author(s):  
Anca Mihaela Mocanu ◽  
Constantin Luca ◽  
Alina Costina Luca

The purpose of this research is to synthetize, characterize and thermal degradation of new heterolytic derivates with potential biological properties. The derivates synthesis was done by obtaining new molecules with pyralozone structure which combine two pharmacophore entities: the amidosulfonyl-R1,R2 phenoxyacetil with the 3,5-dimethyl pyrazole which can have potential biological properties. The synthesis stages of the new products are presented as well as the elemental analysis data and IR, 1H-NMR spectral measurements made for elucidating the chemical structures and thermostability study which makes evident the temperature range proper for their use and storage. The obtained results were indicative of a good correlation of the structure with the thermal stability as estimated by means of the initial degradation temperatures as well as with the degradation mechanism by means of the TG-FTIR analysis.


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