Heavy metal mobility and potential availability in animal manure: using a sequential extraction procedure

2015 ◽  
Vol 18 (3) ◽  
pp. 563-572 ◽  
Author(s):  
Ali Sungur ◽  
Mustafa Soylak ◽  
Selehattin Yilmaz ◽  
Hasan Ozcan
Keyword(s):  
Heavy Metal ◽  
Sequential Extraction ◽  
Extraction Procedure ◽  
Animal Manure ◽  
Metal Mobility ◽  
Sequential Extraction Procedure ◽  
Heavy Metal Mobility ◽  
Potential Availability

scholarly journals Multi-Elemental Inductively Coupled Plasma-Optical Emission Spectroscopic Calibration Problems of the Sequential Extraction Procedure for the Fractionation of the Heavy Metal Content from Aquatic Sediments

2015 ◽  
Vol 43 (1) ◽  
pp. 7-14 ◽  
Author(s):  
György Heltai ◽  
Ilona Fekete ◽  
Gábor Halász ◽  
Katalin Kovács ◽  
Márk Horváth ◽  
...  
Keyword(s):  
Heavy Metal ◽  
Sequential Extraction ◽  
Inductively Coupled Plasma ◽  
Heavy Metal Contamination ◽  
Matrix Effects ◽  
Extraction Procedure ◽  
Optical Emission ◽  
Sequential Extraction Procedure ◽  
Aquatic Sediments ◽  
Inductively Coupled

Abstract For the characterisation of the environmental mobility of heavy metal contamination in aquatic sediments, the EU Bureau of Reference has proposed a fractionation by sequential extraction procedure. For its validation, the CRM-701 sample is available containing Cd, Cr, Cu, Ni, Pb, and Zn. In this paper, the matrix-matched calibration problems are presented. A multi-elemental inductively coupled plasma-optical emission technique is employed for the detection of heavy metals in the extracts. It was established that the sensitivities are strongly influenced by the extractants, which causes significant matrix effects: the sensitivities are strongly influenced by the solvents applied in extraction steps; the summarised recoveries show an acceptable agreement with the certified values; however, in the individual extraction steps for certain elements significant differences may occur due to the neglected interferences. Therefore, further optimisation is required utilising the flexible line selection possibility offered by the HORIBA Jobin Yvon ACTIVA-M instrument.

scholarly journals Mobility of lead, zinc and cadmium in alluvial soils heavily polluted by smelting industry

2011 ◽  
Vol 51 (No, 7) ◽  
pp. 316-321 ◽  
Author(s):  
A. Vaněk ◽  
L. Borůvka ◽  
O. Drábek ◽  
M. Mihaljevič ◽  
M. Komárek
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Czech Republic ◽  
Extraction Procedure ◽  
Metal Mobility ◽  
Alluvial Soils ◽  
Mobility Factor ◽  
Heavy Metal Mobility ◽  
Profile Distribution ◽  
Lead Zinc

In order to determine the mobility of Pb, Zn and Cd in soils from the Př&iacute;bram region (Czech Republic) heavily contaminated by metallurgy, two profiles of alluvial soils were closely studied. Total contents of heavy metals were determined after digestion with a mixture of HF and HClO<sub>4</sub>. Heavy metal mobility was assessed using the mobility factor (MF) that represents the proportion of heavy metals present in the exchangeable and carbonate bound fraction based on the Tessier&rsquo;s sequential extraction procedure. The MF ranged from 2 to 46% for lead, 19 to 62% for zinc and 61 to 94% for cadmium. The profile distribution of zinc and cadmium showed a variable development with depth, which is caused by high amounts of these metals present in labile forms. The profile distribution of lead (the least mobile metal) is characterized by a gradual decrease with depth. The results indicate a higher contamination of the soil profile situated 2.5 km away from the smelter in comparison with the profile in its close vicinity. This fact confirms the existence of extreme fluvial contamination.

Heavy metal mobility assessment in sediments from the Odiel River (Iberian Pyritic Belt) using sequential extraction

2010 ◽  
Vol 61 (7) ◽  
pp. 1493-1503 ◽  
Author(s):  
Rafael Beltrán ◽  
J. D. de la Rosa ◽  
J. C. Santos ◽  
M. Beltrán ◽  
J. L. Gómez-Ariza
Keyword(s):  
Heavy Metal ◽  
Sequential Extraction ◽  
Metal Mobility ◽  
Odiel River ◽  
Mobility Assessment ◽  
Heavy Metal Mobility
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