scholarly journals A reference high-pressure CH4 adsorption isotherm for zeolite Y: results of an interlaboratory study

Adsorption ◽  
2020 ◽  
Vol 26 (8) ◽  
pp. 1253-1266
Author(s):  
H. G. T. Nguyen ◽  
C. M. Sims ◽  
B. Toman ◽  
J. Horn ◽  
R. D. van Zee ◽  
...  
Keyword(s):  
High Pressure ◽  
Reference Material ◽  
Adsorption Isotherms ◽  
Zeolite Y ◽  
Interlaboratory Study ◽  
Carbon Dioxide Adsorption ◽  
Uncertainty Interval ◽  
Pressure Surface ◽  
Reference Equation ◽  
Ch4 Adsorption

Abstract This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850 (Zeolite Y), at 25 °C up to 7.5 MPa. Twenty laboratories participated in the study and contributed over one-hundred adsorption isotherms of methane on Zeolite Y. From these data, an empirical reference equation was determined, along with a 95% uncertainty interval (Uk=2). By requiring participants to replicate a high-pressure reference isotherm for carbon dioxide adsorption on NIST Reference Material RM 8852 (ZSM-5), this interlaboratory study also demonstrated the usefulness of reference isotherms in evaluating the performance of high-pressure adsorption experiments.

High pressure carbon dioxide adsorption on nanoporous carbons prepared by Zeolite Y templating

2011 ◽  
Vol 65 (12) ◽  
pp. 1772-1774 ◽  
Author(s):  
Han-Kyol Youn ◽  
Jun Kim ◽  
Govindasamy Chandrasekar ◽  
Hangkyo Jin ◽  
Wha-Seung Ahn
Keyword(s):  
Carbon Dioxide ◽  
High Pressure ◽  
Zeolite Y ◽  
Carbon Dioxide Adsorption ◽  
Nanoporous Carbons

Determination of adsorption isotherms and solute activities from spreading pressure-surface charge data

1977 ◽  
Vol 62 (3) ◽  
pp. 454-460 ◽  
Author(s):  
Sherril D Christian ◽  
Glenn Dryhurst ◽  
Viktor Brabec ◽  
James G Baker
Keyword(s):  
Surface Charge ◽  
Adsorption Isotherms ◽  
Spreading Pressure ◽  
Pressure Surface

scholarly journals Production of Surface Layer with Gradient Microstructure and Microhardess on Copper by High Pressure Surface Rolling

Metals ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 73
Author(s):  
Juying Li ◽  
Qingsong Mei ◽  
Yana Li ◽  
Beihai Wang
Keyword(s):  
High Pressure ◽  
Surface Layer ◽  
Pure Copper ◽  
X Ray Diffraction ◽  
Electronic Microscopy ◽  
X Ray ◽  
Pressure Surface ◽  
Surface Gradient ◽  
Pressure Time ◽  
Gradient Microstructure

Pure copper was subjected to high-pressure surface rolling (HPSR) to obtain a surface gradient layer. Effects of HPSR parameters on the surface microstructure and microhardness of Cu were investigated by using optical microscopy, transmission electronic microscopy, X-ray diffraction, and the microhardness test. The HPSR surface layer has a gradient microstructure consisting of increasingly refined grains with decreasing depth from the treated surface (DFS). The thicknesses of the refined surface layer can be up to ~1.8 mm, and the grain size of the topmost surface is down to ~88 nm, depending on the HPSR parameters including pressure, time, and temperature. Microhardness of HPSR samples increases with decreasing DFS, with a maximum of ~2.4 times that of the undeformed matrix. The present results indicated that HPSR could be an effective method for the production of a mm-thick surface layer on Cu with gradient microstructure and property.

Conjugate Heat Transfer Analysis to Assess Overall Cooling Effectiveness of High Pressure Turbine Nozzle With Optimized Film Cooling Hole Arrangements

2019 ◽  
Author(s):  
Young Seok Kang ◽  
Dong-Ho Rhee ◽  
Sanga Lee ◽  
Bong Jun Cha
Keyword(s):  
Heat Transfer ◽  
High Pressure ◽  
Film Cooling ◽  
Conjugate Heat Transfer ◽  
Heat Transfer Analysis ◽  
Internal Cooling ◽  
Cooling Effectiveness ◽  
Film Cooling Effectiveness ◽  
Baseline Design ◽  
Pressure Surface

Abstract Conjugate heat transfer analysis method has been highlighted for predicting heat exchange between fluid domain and solid domain inside high-pressure turbines, which are exposed to very harsh operating conditions. Then it is able to assess the overall cooling effectiveness considering both internal cooling and external film cooling at the cooled turbine design step. In this study, high-pressure turbine nozzles, which have three different film cooling holes arrangements, were numerically simulated with conjugate heat transfer analysis method for predicting overall cooling effectiveness. The film cooling holes distributed over the nozzle pressure surface were optimized by minimizing the peak temperature, temperature deviation. Additional internal cooling components such as pedestals and rectangular rib turbulators were modeled inside the cooling passages for more efficient heat transfer. The real engine conditions were given for boundary conditions to fluid and solid domains for conjugate heat transfer analysis. Hot combustion gas properties such as specific heat at constant pressure and other transport properties were given as functions of temperature. Also, the conductivity of Inconel 718 was also given as a function of temperature to solve the heat equation in the nozzle solid domain. Conjugate heat transfer analysis results showed that optimized designs showed better cooling performance, especially on the pressure surface due to proper staggering and spacing hole-rows compared to the baseline design. The overall cooling performances were offset from the adiabatic film cooling effectiveness. Locally concentrated heat transfer and corresponding high cooling effectiveness region appeared where internal cooling effects were overlapped in the optimized designs. Also, conjugate heat transfer analysis results for the optimized designs showed more uniform contours of the overall cooling effectiveness compared to the baseline design. By varying the coolant mass flow rate, it was observed that pressure surface was more sensitive to the coolant mass flow rate than nozzle leading edge stagnation region and suction surface. The CHT results showed that optimized designs to improve the adiabatic film cooling effectiveness also have better overall cooling effectiveness.

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