scholarly journals Swelling of individual cellulose nanofibrils in water, role of crystallinity: an AFM study

Cellulose ◽  
2020 ◽  
Author(s):  
Vegar Ottesen ◽  
Kristin Syverud
Keyword(s):  
Atomic Force Microscopy ◽  
Cellulose Nanofibrils ◽  
Platinum Nanowires ◽  
Force Microscopy ◽  
Atomic Force ◽  
Water Swelling ◽  
Fibril Diameter

Abstract Atomic force microscopy (AFM) can be used to quantitatively study nanomaterials in different media, e.g. vacuum, air, or submerged in a liquid. A technique was developed to study swelling of individual cellulose nanofibrils (CNFs) using AFM. As a case study, CNFs with different degrees of crystallinity (DoC) were examined for swellability going from dry to wet (submerged in de-ionized water). Swelling was found to depend on DoC, but no significant correlation between fibril diameter and swellability was seen. Upon introduction of de-ionized water high DoC samples ($$65\pm 2\%$$ 65 ± 2 % ) were found to have a diameter increase of 34% on average, whereas low DoC ($$44\pm 2\%$$ 44 ± 2 % ) were found to have a diameter increase of 44% on average. A tested control, consisting of platinum nanowires on silisium, did not swell. Graphic abstract

Die-Level Scanning Capacitance Microscopy Fault Isolation on SOI Fin-FET Devices for Advanced Semiconductor Nodes

2018 ◽  
Author(s):  
Lucile C. Teague Sheridan ◽  
Tanya Schaeffer ◽  
Yuting Wei ◽  
Satish Kodali ◽  
Chong Khiam Oh
Keyword(s):  
Atomic Force Microscopy ◽  
Failure Analysis ◽  
Fault Isolation ◽  
Scanning Capacitance Microscopy ◽  
Force Microscopy ◽  
Atomic Force

Abstract It is widely acknowledged that Atomic force microscopy (AFM) methods such as conductive probe AFM (CAFM) and Scanning Capacitance Microscopy (SCM) are valuable tools for semiconductor failure analysis. One of the main advantages of these techniques is the ability to provide localized, die-level fault isolation over an area of several microns much faster than conventional nanoprobing methods. SCM, has advantages over CAFM in that it is not limited to bulk technologies and can be utilized for fault isolation on SOI-based technologies. Herein, we present a case-study of SCM die-level fault isolation on SOI-based FinFET technology at the 14nm node.

The role of cross-linking in the scratch resistance of organic coatings: An investigation using Atomic Force Microscopy

Wear ◽  
2019 ◽  
Vol 418-419 ◽  
pp. 151-159 ◽  
Author(s):  
Juan F. Gonzalez-Martinez ◽  
Erum Kakar ◽  
Stefan Erkselius ◽  
Nicola Rehnberg ◽  
Javier Sotres
Keyword(s):  
Atomic Force Microscopy ◽  
Scratch Resistance ◽  
Organic Coatings ◽  
Cross Linking ◽  
Force Microscopy ◽  
Atomic Force

scholarly journals Morphometric characterization of fibrinogen's αC regions and their role in fibrin self-assembly and molecular organization

Nanoscale ◽  
2017 ◽  
Vol 9 (36) ◽  
pp. 13707-13716 ◽  
Author(s):  
Anna D. Protopopova ◽  
Rustem I. Litvinov ◽  
Dennis K. Galanakis ◽  
Chandrasekaran Nagaswami ◽  
Nikolay A. Barinov ◽  
...  
Keyword(s):  
Atomic Force Microscopy ◽  
Self Assembly ◽  
Molecular Organization ◽  
Microscopy Imaging ◽  
Force Microscopy ◽  
Atomic Force ◽  
Atomic Force Microscopy Imaging ◽  
Morphometric Characterization

High-resolution atomic force microscopy imaging reveals the role of fibrinogen αC regions in the early stages of fibrin self-assembly.

Preparation of Cellulose Nanofibrils by High-Pressure Homogenizer and Zein Composite Films

2013 ◽  
Vol 829 ◽  
pp. 534-538 ◽  
Author(s):  
Alireza Shakeri ◽  
Sattar Radmanesh
Keyword(s):  
Atomic Force Microscopy ◽  
High Pressure ◽  
Food Packaging ◽  
Cellulose Nanofibrils ◽  
Composite Films ◽  
Average Diameter ◽  
Nanocomposite Films ◽  
Force Microscopy ◽  
Atomic Force ◽  
High Pressure Homogenizer

Cellulose nanofibrils ( NF ) have several advantages such as biodegradability and safety toward human health. Zein is a biodegradable polymer with potential use in food packaging applications. It appears that polymer nanocomposites are one of the most promising applications of zein films. Cellulose NF were prepared from starting material Microcrystalline cellulose (MCC) by an application of a high-pressure homogenizer at 20,000 psi and treatment consisting of 15 passes. Methods such as atomic force microscopy were used for confirmation of nanoscale size production of cellulose. The average diameter 45 nm were observed. Zeincellulose NF nanocomposite films were prepared by casting ethanol suspensions of Zein with different amounts of cellulose NF in the 0% to 5%wt. The nanocomposites were characterized by using Fourier transform infrared spectroscopy ( FTIR ), Atomic force microscopy ( AFM ) and X-ray diffraction ( XRD ) analysis. From the FTIR spectra the various groups present in the Zein blend were monitored. The homogeneity, morphology and crystallinity of the blends were ascertained from the AFM and XRD data, respectively. The thermal resistant of the zein nanocomposite films improved as the nanocellulose content increased. These obtained materials are transparent, flexible and present significantly better physical properties than the corresponding unfilled Zein films.

scholarly journals Potential role of atomic force microscopy in systems biology

2011 ◽  
Vol 3 (6) ◽  
pp. 702-716 ◽  
Author(s):  
Srinivasan Ramachandran ◽  
Fernando Teran Arce ◽  
Ratnesh Lal
Keyword(s):  
Atomic Force Microscopy ◽  
Systems Biology ◽  
Potential Role ◽  
Force Microscopy ◽  
Atomic Force
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