scholarly journals Simplification of gel point characterization of cellulose nano and microfiber suspensions

Cellulose ◽  
2021 ◽  
Author(s):  
Jose Luis Sanchez-Salvador ◽  
M. Concepcion Monte ◽  
Carlos Negro ◽  
Warren Batchelor ◽  
Gil Garnier ◽  
...  
Keyword(s):  
Aspect Ratio ◽  
Mathematical Models ◽  
Industrial Applications ◽  
Smoothing Spline ◽  
Gel Point ◽  
Critical Information

Abstract Nanocellulose is an emerging material that needs to be well characterized to control its performance during industrial applications. Gel point (Øg) is a convenient parameter commonly used to estimate the aspect ratio (AR) of cellulose nano/microfibers (CNFs/CMFs), providing critical information on the nanofiber network. However, its estimation requires many sedimentation experiments, tedious and time consuming. In this study, a simpler and faster technique is presented to estimate Øg, based on one or two sedimentation experiments, reducing the experiments by a factor of at least 2.5. Here, this new methodology is successfully validated by using the Øg of different CNF/CMF hydrogels calculated with the traditional methodology, showing an error lower than 7%. The error in the estimation of the AR is lower than 3% in all cases. Furthermore, the two mathematical models currently used to estimate Øg, the smoothing spline and the quadratic fit, are compared and the mathematical assumptions improved. Graphical abstract

Synthesis, Characterization, and Dynamic Behavior of Well-defined Dithiomaleimide-functionalized Maltodextrins

2020 ◽  
Vol 17 (2) ◽  
pp. 85-89
Author(s):  
Francisco J. Hidalgo ◽  
Nathan A.P. Lorentz ◽  
TinTin B. Luu ◽  
Jonathan D. Tran ◽  
Praveen D. Wickremasinghe ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Dynamic Behavior ◽  
Industrial Applications ◽  
19F Nmr ◽  
Nmr Studies ◽  
Synthetic Pathway ◽  
End Groups ◽  
Sugar End

: Maltodextrins have an increasing number of biomedical and industrial applications due to their attractive physicochemical properties such as biodegradability and biocompatibility. Herein, we describe the development of a synthetic pathway and characterization of thiol-responsive maltodextrin conjugates with dithiomaleimide linkages. 19F NMR studies were also conducted to demonstrate the exchange dynamics of the dithiomaleimide-functionalized sugar end groups.

scholarly journals A Tool for the Analysis and Characterization of School Mathematical Models

Mathematics ◽  
2021 ◽  
Vol 9 (13) ◽  
pp. 1569
Author(s):  
Jesús Montejo-Gámez ◽  
Elvira Fernández-Ahumada ◽  
Natividad Adamuz-Povedano
Keyword(s):  
Mathematical Modeling ◽  
Mathematical Models ◽  
Educational Research ◽  
Analysis Procedure ◽  
Real System ◽  
The Real ◽  
School Model ◽  
Corresponding Analysis ◽  
Three Components

This paper shows a tool for the analysis of written productions that allows for the characterization of the mathematical models that students develop when solving modeling tasks. For this purpose, different conceptualizations of mathematical models in education are discussed, paying special attention to the evidence that characterizes a school model. The discussion leads to the consideration of three components, which constitute the main categories of the proposed tool: the real system to be modeled, its mathematization and the representations used to express both. These categories and the corresponding analysis procedure are explained and illustrated through two working examples, which expose the value of the tool in establishing the foci of analysis when investigating school models, and thus, suggest modeling skills. The connection of this tool with other approaches to educational research on mathematical modeling is also discussed.

Fabrication and electrical characterization of high aspect ratio poly-silicon filled through-silicon vias

2012 ◽  
Vol 22 (5) ◽  
pp. 055021 ◽  
Author(s):  
Pradeep Dixit ◽  
Tapani Vehmas ◽  
Sami Vähänen ◽  
Philippe Monnoyer ◽  
Kimmo Henttinen
Keyword(s):  
Aspect Ratio ◽  
High Aspect Ratio ◽  
Electrical Characterization ◽  
Through Silicon Vias ◽  
Poly Silicon ◽  
Silicon Vias

Seed and juice characterization of pomegranate fruits grown in Tunisia: Comparison between sour and sweet cultivars revealed interesting properties for prospective industrial applications

2011 ◽  
Vol 33 (2) ◽  
pp. 374-381 ◽  
Author(s):  
Nejib Hasnaoui ◽  
Messaoud Mars ◽  
Sana Ghaffari ◽  
Mokhtar Trifi ◽  
Pablo Melgarejo ◽  
...  
Keyword(s):  
Industrial Applications

Analysis and characterization of high-resolution and high-aspect-ratio imaging fiber bundles

2015 ◽  
Vol 54 (32) ◽  
pp. 9422 ◽  
Author(s):  
Nojan Motamedi ◽  
Salman Karbasi ◽  
Joseph E. Ford ◽  
Vitaliy Lomakin
Keyword(s):  
High Resolution ◽  
Aspect Ratio ◽  
High Aspect Ratio ◽  
Fiber Bundles ◽  
Ratio Imaging

Application of the Continuous Rheoconversion Process (CRP) to Low Temperature HPDC-Part I: Microstructure

2006 ◽  
Vol 116-117 ◽  
pp. 402-405 ◽  
Author(s):  
Qin Yue Pan ◽  
Stuart Wiesner ◽  
Diran Apelian
Keyword(s):  
Low Temperature ◽  
Scale Up ◽  
Microstructural Characterization ◽  
Industrial Applications ◽  
Primary Phase ◽  
Heat Extraction ◽  
Initial Stage ◽  
Fraction Solid ◽  
Die Castings

The continuous rheoconversion process (CRP) is a novel slurry-on-demand process that was developed at MPI/WPI in 2002. The process is based on a passive liquid mixing technique in which the nucleation and growth of the primary phase are controlled using a specially designed “reactor”. The reactor provides heat extraction, copious nucleation, and forced convection during the initial stage of solidification, thus leading to the formation of globular structures. This paper presents our recent work on the scale-up of the CRP for industrial applications. Specifically, we demonstrate an important application of the CRP to low temperature (low fraction solid) HPDC. In Part I of this paper, we present salient results on microstructural characterization of CRP processed castings vs. conventional die castings.

Bentonite Clays Characterization in the Town of Sossego – Paraiba State

2015 ◽  
Vol 820 ◽  
pp. 65-70
Author(s):  
I.D.S. Pereira ◽  
V.N.F. Lisboa ◽  
I.A. Silva ◽  
J.M.R. Figueirêdo ◽  
G.A. Neves ◽  
...  
Keyword(s):  
Industrial Applications ◽  
Particle Size Analysis ◽  
Size Analysis ◽  
Drilling Fluids ◽  
X Ray Diffraction ◽  
Mineralogical Characterization ◽  
Bentonite Clays ◽  
The Town ◽  
Petroleum Drilling

Bentonite exhibt a range of industrial applications moving millions of dollars on the market per year. Among several applications if highlights it is use for petroleum drilling fluids. Thus, this work aims to characterize physical, mineralogical and technologically, the bentonitics clays of Sossego County, Paraíba, Brazil. Mineralogical characterization of clays was done through the following techniques: particle size analysis by laser diffraction, thermogravimetric and differential thermal analysis, chemical analysis and x-ray diffraction. The clays were turned in by treatment with sodium in Na2CO3 and then determined whether the apparent viscosity, plastic and volume of filtrate of clay-water dispersions. The results showed that the samples are of polycationic, showing levels of MgO, CaO and K2O, similar to those from Boa Vista County, Paraíba, Brazil, and consist of clay mineral kaolinite, quartz and esmec. The clays showed rheological properties that indicate potential for use in drilling fluids.

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