Green synthesis and application of nanomagnetic molecularly imprinted polymerfor fast solid-phase extraction of brilliant blue FCF from real samples

2018 ◽  
Vol 26 (1) ◽  
Author(s):  
Naghmeh Arabzadeh ◽  
Reza Akbarzadeh ◽  
Ali Mohammadi ◽  
Maher Darwish
2019 ◽  
Vol 11 (5) ◽  
pp. 618-626 ◽  
Author(s):  
Hamid Reza Noormohamadi ◽  
Mohammad Reza Fat'hi ◽  
Mehrorang Ghaedi ◽  
Valiollah Nobakht ◽  
Sara Azizzadeh

μ-SPE procedure based on (silver(i)-CP).


2015 ◽  
Vol 7 (11) ◽  
pp. 4717-4724 ◽  
Author(s):  
Xiang-Jie Li ◽  
Xiu-Xiu Chen ◽  
Guan-Yin Sun ◽  
Yong Xin Zhao ◽  
Zhao-Sheng Liu ◽  
...  

A method for solid-phase extraction (SPE) of isoquercitrin (ISO) from natural plant extracts was proposed based on molecularly imprinted polymers (MIPs).


2015 ◽  
Vol 3 (1) ◽  
pp. 1-7 ◽  
Author(s):  
Myriam Díaz-Álvarez ◽  
Esther Turiel

AbstractIn this paper, the improvement over a novel format for selective solid-phase extraction based on a molecularly imprinted polymer (MIP) is described. A small amount of MIP has been synthesized within the superficial pores of commercial polyethylene (PE) frits and attached to its surface using benzophenone (BP), a photo-initiator capable to start the polymerization from the surface of the support material. Key properties affecting the obtainment of a proper polymeric layer, such as polymerization time and kind of cross-linker were optimized. Prepared composite material was applied to the SPE of TBZ in real samples extracts, showing an impressive clean-up ability. Calibrations showed good linearity in the concentration range of 0.05–5.00 μg g-1, referred to the original solid sample, and the regression coefficients obtained were greater than 0.998. The calculated detection limit was 0.01 μg g-1, low enough to satisfactory analysis of TBZ in real samples. Mean recoveries were about 70 % at different concentration levels with RSDs always ranged below 15% in all the cases.


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