scholarly journals Mechanical Stress Effects on 550 °C Hot Corrosion Propagation Rates in Precipitation Hardened Ni-Base Superalloys: CMSX-4, CM247LC DS and IN6203DS

2021 ◽  
Author(s):  
Neil Chapman ◽  
Simon Gray ◽  
Joy Sumner ◽  
John Nicholls
Keyword(s):  
Mechanical Stress ◽  
Corrosion Fatigue ◽  
Hot Corrosion ◽  
Fatigue Testing ◽  
Propagation Rate ◽  
Eutectic Structure ◽  
Corrosion Propagation ◽  
R Ratio ◽  
Environmentally Assisted Cracking ◽  
The Matrix

AbstractCombinations of temperature, stress and hot corrosion may cause environmentally-assisted cracking in precipitation-hardened Ni-base superalloys, which is little understood. This research aims to increase current understanding by investigating the effects of mechanical stress on the hot corrosion propagation rate during corrosion-fatigue testing of CMSX-4, CM247LC DS and IN6203DS. The parameters used during the tests included a high R-ratio, high frequency, and a temperature of 550 °C. The results showed CMSX-4 experienced a predictable increase in the hot corrosion rate, CM247LC DS also experienced increased rates, but no obvious trend was apparent; whilst IN6203DS showed no evidence of an increased rate. These different behaviours appear to be a result of an interaction between the mechanical stress and microstructural features, which include gamma-prime volume fractions in both the matrix and eutectic regions, along with the distribution of the eutectic structure. The different behaviours in the hot corrosion propagation rate subsequently affected the respective corrosion fatigue results, with both CMSX-4 and CM247LC DS experiencing fracture but with significantly more scatter involved in the CM247LC DS results. All IN6203DS corrosion-fatigue specimens completed the respective tests without fracture and showed no evidence of cracking. It, therefore, appears that precipitation hardened Ni-base superalloys, which are susceptible to environmentally-assisted cracking, also experience increased hot corrosion propagation rates.

Lifetime Enhancement of Propulsion Shafts Against Corrosion-Fatigue by Laser Peening

2018 ◽  
Author(s):  
Lloyd A. Hackel ◽  
Jon E. Rankin
Keyword(s):  
Corrosion Fatigue ◽  
Fatigue Testing ◽  
Salt Water ◽  
Fatigue Cracks ◽  
Water Immersion ◽  
High Energy ◽  
General Corrosion ◽  
Laser Peening ◽  
Corrosion Pits ◽  
Deep Pits

This paper reports substantially enhanced fatigue and corrosion-fatigue lifetimes of propulsion shaft materials, 23284A steel and 23284A steel with In625 weld overlay cladding, as a result of shot or laser peening. Glass reinforced plastic (GRP) coatings and Inconel claddings are used to protect shafts against general corrosion and corrosion pitting. However salt water leakage penetrating under a GRP can actually enhance pitting leading to crack initiation and growth. Fatigue coupons, untreated and with shot or laser peening were tested, including with simultaneous salt water immersion. Controlled corrosion of the surfaces was simulated with electric discharge machining (EDM) of deep pits enabling evaluation of fatigue and corrosion-fatigue lifetimes. Results specifically show high energy laser peening (HELP) to be a superior solution, improving corrosion-fatigue resistance of shaft and cladding metal, reducing the potential for corrosion pits to initiate fatigue cracks and dramatically slowing crack growth rates. At a heavy loading of 110% of the 23284A steel yield stress and with 0.020 inch deep pits, laser peening increased fatigue life of the steel by 1370% and by 350% in the corrosion-fatigue testing.

Manufacture of Continuous Metal Matrix Composite Strip Reinforced by Particulate Materials from the Semisolid Processing

2019 ◽  
Vol 285 ◽  
pp. 189-196
Author(s):  
Antonio de Pádua Lima Filho ◽  
Bruno Katsuyoshi Silama Ueda ◽  
Tales Paschoalino de Castro ◽  
Rodrigo Alessandro Nunes de Oliveira
Keyword(s):  
Metal Matrix ◽  
Surface Defects ◽  
Cast Alloy ◽  
Eutectic Structure ◽  
Nucleation Agent ◽  
Alloy Matrix ◽  
Cooling Slope ◽  
Α Phase ◽  
The Matrix ◽  
Graphite Nanoparticles

Strip casting is a new method of producing metal matrix composites. Two-roll melt dragged processing (TRMD-ing) and single-roll melt dragged processing (SRMD-ing) methods were used to study the manufacture of 2-mm-thick composite strips by using PbSn (≈ 11.3 g/cm3) eutectic alloy matrix reinforced with iron (≈ 7.86 g/cm3) powder (≈ 70 μm) at a rate of 0.3 m/s. The metallic powder stored in the feed hopper (≈ 90 g) was pushed during the pouring operation of the cast alloy (≈ 4 kg) at 260 oC on the cooling slope to produce a mixture of metallic slurry and particles to feed the nozzle to be dragged by the lower roll. Various surface defects occurred during processing, such as the failure of the powder particle to be embedded in the matrix by SRMD-ing with and without stirrer into the nozzle, and the rolling up of the strip into the nozzle by TRMD-ing. Graphite nanoparticles formed inside the α-Pb grain revealed a complicate eutectic structure in both the processing methods. The colloidal graphite used to coat the crucible, cooling slope, and nozzle could act as a nucleation agent for preferential centre segregation in the α-Pb grain. This suggests that the graphite nanoparticles functioned as nucleation points in the lead-rich α phase. Thus, another type of composite was formed in the presence of graphite nanoparticles within the lead-rich α-phase surrounded by β-Sn. An electron probe microanalysis and scanning electronic microscopy were used to investigate the composition and distribution and identify the different phases. Several types of particulate reinforcements may be added to the matrix to obtain composites for mechanical, electronic, and magnetic applications using these technologies.

Corrosion Fatigue Mechanisms and Fracture Mechanics Based Modelling for Subsea Pipeline Steels

2017 ◽  
Author(s):  
Ankang Cheng ◽  
Nian-Zhong Chen
Keyword(s):  
Fracture Mechanics ◽  
Crack Propagation ◽  
Corrosion Fatigue ◽  
Fatigue Cracking ◽  
Crack Propagation Rate ◽  
Propagation Rate ◽  
Propagation Time ◽  
Loading Frequency ◽  
Pipeline Steels ◽  
Driving Mechanisms

Subsea structures such as pipelines are vulnerable to environment-assisted crackings (EACs). As a type of EAC, corrosion fatigue (CF) is almost inevitable. For such a process, stress corrosion (SC) and hydrogen-assisted cracking (HAC) are the two mainly driving mechanisms. And it was further pointed out that slip dissolution (SD) and hydrogen embrittlement (HE) should be responsible for SC and HAC respectively. Based on such a fact, a two-component physical model for estimating the CF crack propagation rate was proposed. The proposed model was built in a frame of fracture mechanics integrated with a dissolution model for C-Mn steel and a newly established model by the authors accounting for the influence from HE upon crack propagation. The overall CF crack propagation rate is the aggregate of the two rates predicted by the two sub-individual models, and then the crack propagation time is calculated accordingly. The model has been proven to be capable of capturing the features of HE influenced fatigue cracking behaviour as well as taking mechanical factors such as the loading frequency and stress ratio into account by comparison with the experimental data of X42 and X65 pipeline steels.

scholarly journals Study of the Microstructure and Crack Evolution Behavior of Al-5Fe-1.5Er Alloy

Materials ◽  
2019 ◽  
Vol 12 (1) ◽  
pp. 172 ◽  
Author(s):  
Ming Li ◽  
Zhiming Shi ◽  
Xiufeng Wu ◽  
Huhe Wang ◽  
Yubao Liu
Keyword(s):  
Electron Microscopy ◽  
Crack Initiation ◽  
Tensile Tests ◽  
Eutectic Structure ◽  
Interface Structure ◽  
X Ray ◽  
Transmission Electron ◽  
The Matrix ◽  
Evolution Behavior

In this work, the microstructure of Al-5Fe-1.5Er alloy was characterized and analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDS) techniques. The effect of microstructure on the behavior of crack initiation and propagation was investigated using in situ tensile testing. The results showed that when 1.5 wt.% Er was added in the Al-5Fe alloy, the microstructure consisted of α-Al matrix, Al3Fe, Al4Er, and Al3Fe + Al4Er eutectic phases. The twin structure of Al3Fe phase was observed, and the twin plane was {001}. Moreover, a continuous concave and convex interface structure of Al4Er was observed. Furthermore, Al3Fe was in the form of a sheet with a clear gap inside. In situ tensile tests of the alloy at room temperature showed that the crack initiation mainly occurred in the Al3Fe phase, and that the crack propagation modes included intergranular and trans-granular expansions. The crack trans-granular expansion was due to the strong binding between Al4Er phases and surrounding organization, whereas the continuous concave and convex interface structure of Al4Er provided a significant meshing effect on the matrix and the eutectic structure.

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