Influence of Heat-Treatment Cycles on the Microstructure, Mechanical Properties, and Corrosion Resistance of Co-Cr Dental Alloys Fabricated by Selective Laser Melting

Author(s):  
Konstantinos Dimitriadis ◽  
Angeliki G. Lekatou ◽  
Athanasios K. Sfikas ◽  
Maria Roumpi ◽  
Sofia Tsouli ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2468 ◽  
Author(s):  
Papula ◽  
Song ◽  
Pateras ◽  
Chen ◽  
Brandt ◽  
...  

Additive manufacturing (AM) is a rapidly growing field of technology. In order to increase the variety of metal alloys applicable for AM, selective laser melting (SLM) of duplex stainless steel 2205 powder and the resulting microstructure, density, mechanical properties, and corrosion resistance were investigated. An optimal set of processing parameters for producing high density (>99.9%) material was established. Various post-processing heat treatments were applied on the as-built predominantly ferritic material to achieve the desired dual-phase microstructure. Effects of annealing at temperatures of 950 °C, 1000 °C, 1050 °C, and 1100 °C on microstructure, crystallographic texture, and phase balance were examined. As a result of annealing, 40–46 vol.% of austenite phase was formed. Annealing decreased the high yield and tensile strength values of the as-built material, but significantly increased the ductility. Annealing also decreased the residual stresses in the material. Mechanical properties of the SLM-processed and heat-treated materials outperformed those of conventionally produced alloy counterparts. Using a scanning strategy with 66° rotation between layers decreased the strength of the crystallographic texture. Electrochemical cyclic potentiodynamic polarization testing in 0.6 M NaCl solution at room temperature showed that the heat treatment improved the pitting corrosion resistance of the as-built SLM-processed material.


NANO ◽  
2021 ◽  
Author(s):  
Qingxia Zhang ◽  
Lingtao Meng ◽  
Xiaotian Yin ◽  
Shenghai Wang ◽  
Yong Liu ◽  
...  

In previous studies, the microstructure, mechanical properties and corrosion resistance of Hastelloy X fabricated by selective laser melting (SLM) have been investigated; however, it is hoped that heat treatment will effect on its properties. Therefore, this study is to discuss heat treatment effect on Hastelloy X fabricated by SLM. It is interestingly found that fracture strain greatly increases with heat treatment, and the yield ratio decreases, which demonstrates the material is more reliable. High temperature tensile behavior is discussed; it is worth mentioning that not only fracture strain of the HT sample increases greatly at 550∘C in comparison with SLM sample, but also ultimate tensile strength increases from 632 MPa to 639 MPa; the results show that the mechanical property can be improved at medium and high temperature by heat treatment. The corrosion resistance of HT sample deteriorates slightly, which can be explained by Cr-rich precipitates. In conclusion, the material after heat treatment is suitable for applications requiring high mechanical reliability and medium and high temperature occasions, but it is not befitting for corrosive environments.


Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1012 ◽  
Author(s):  
Feng Shang ◽  
Xiaoqiu Chen ◽  
Zhiyong Wang ◽  
Zuchun Ji ◽  
Fei Ming ◽  
...  

UNS S32707 hyper-duplex stainless steel (HDSS) parts with complex shapes for ocean engineering were prepared by selective laser melting (SLM) process. In the process of SLM, the balance between austenite and ferrite was undermined due to the high melting temperature and rapid cooling rate, resulting in poor ductility and toughness. The solution annealing was carried out with various temperatures (1050–1200 °C) for one hour at a time. The evolution of microstructures, mechanical properties, and corrosion resistance of UNS S32707 samples prepared by SLM was comprehensively investigated. The results indicate that a decrease in nitrogen content during the SLM process reduced the content of austenite, and a nearly balanced microstructure was obtained after appropriate solution annealing. The ratio between ferrite and austenite was approximately 59.5:40.5. The samples with solution treated at 1150 °C and 1100 °C exhibited better comprehensive mechanical properties and pitting resistance, respectively.


2018 ◽  
Vol 24 (7) ◽  
pp. 1235-1244 ◽  
Author(s):  
Mingkang Zhang ◽  
Yongqiang Yang ◽  
Changhui Song ◽  
Yuchao Bai ◽  
Zefeng Xiao

PurposeThis study aims to focus on the heat treatment influence on the corrosion resistance, adhesion of Streptococcus mutans and mechanical properties of CoCrMo alloys manufactured by the selective laser melting (SLM). Design/methodology/approachCoCrMo alloys were manufactured using the Dimetal-100 machine. X-ray diffraction (XRD), metallographic analysis, scanning electron microscopy (SEM), electrochemical corrosion, Vickers microhardness and tensile tests were used to characterize SLM-produced CoCrMo alloys and compare them with the ones manufactured by casting and with the ASTM F75 standard. FindingsThe electrochemical results showed that SLM900 samples had the best corrosion resistance in artificial saliva. The adhesion results showed least propagation and overall quantity of Streptococcus mutans on the SLM900 sample. The microhardness, tensile and yield strength of As-SLM, SLM900 and SLM1200D samples were measured according to the ASTM F75 standard. The elongation of SLM900 was less than 8 per cent, which does not meet the standard specifications. Analysis of the fracture morphology showed that the fracture mechanisms of As-SLM and SLM1200D belong to the quasi-cleavage fracture type, and the mechanical fracture mechanism of SLM900 can be characterized as brittle fracture. Originality/valueThis paper presents the adhesion properties of Streptococcus mutans on the surface of CoCrMo alloys manufactured by SLM and proposes how to regulate the effect of the heat treatment on the corrosion resistance and mechanical properties of CoCrMo alloys manufactured by SLM.


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