In situ analysis of dendritic equiaxed microstructure formation in Al-Cu alloys by synchrotron X-ray radiography

2009 ◽  
Vol 62 (4-5) ◽  
pp. 427-431 ◽  
Author(s):  
A. Bogno ◽  
H. Nguyen-Thi ◽  
B. Billia ◽  
N. Bergeon ◽  
N. Mangelinck-Noël ◽  
...  
2018 ◽  
Vol 127 (2) ◽  
pp. 371-389 ◽  
Author(s):  
Tyler Oesch ◽  
Frank Weise ◽  
Dietmar Meinel ◽  
Christian Gollwitzer

JOM ◽  
2020 ◽  
Vol 73 (1) ◽  
pp. 201-211 ◽  
Author(s):  
Benjamin Gould ◽  
Sarah Wolff ◽  
Niranjan Parab ◽  
Cang Zhao ◽  
Maria Cinta Lorenzo-Martin ◽  
...  

Author(s):  
Kyuya Nakagawa ◽  
Shinri Tamiya ◽  
Shu Sakamoto ◽  
Gabsoo Do ◽  
Shinji Kono ◽  
...  

X-ray computed tomography technique was used to observe microstructure formation during freeze-drying. A specially designed vacuum freeze-drying stage was equipped at the X-ray CT stage, and the frozen and dried microstructures of dextrin solutions were successfully observed. It was confirmed that the many parts of the pore microstructures formed as a replica of the original ice microstructures, whereas some parts formed as a consequence of the dehydration dependent on the relaxation level of the glassy phases, suggesting that the post-freezing annealing is advantageous for avoiding quality loss that relates to the structural deformation of glassy matters. Keywords: freeze-drying; X-ray CT; ice microstructure; glassy state


2018 ◽  
Vol 53 (8) ◽  
pp. 6021-6032 ◽  
Author(s):  
J. Nellesen ◽  
R. Laquai ◽  
B. R. Müller ◽  
A. Kupsch ◽  
M. P. Hentschel ◽  
...  

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