scholarly journals Optimization of the extrusion process through response surface methodology for improvement in functional and nutritional properties of soybean hull

2020 ◽  
Vol 57 (11) ◽  
pp. 4054-4064
Author(s):  
Forough Sadat Tabibloghmany ◽  
Mostafa Mazaheri Tehrani ◽  
Arash Koocheki
2012 ◽  
Vol 03 (10) ◽  
pp. 1516-1525 ◽  
Author(s):  
Jorge Milán-Carrillo ◽  
Alvaro Montoya-Rodríguez ◽  
Roberto Gutiérrez-Dorado ◽  
Xiomara Perales-Sánchez ◽  
Cuauhtémoc Reyes-Moreno

Polymers ◽  
2020 ◽  
Vol 12 (12) ◽  
pp. 2798
Author(s):  
Steffen Ulitzsch ◽  
Tim Bäuerle ◽  
Thomas Chassé ◽  
Günter Lorenz ◽  
Andreas Kandelbauer

Thermoplastic polymers like ethylene-octene copolymer (EOC) may be grafted with silanes via reactive extrusion to enable subsequent crosslinking for advanced biomaterials manufacture. However, this reactive extrusion process is difficult to control and it is still challenging to reproducibly arrive at well-defined products. Moreover, high grafting degrees require a considerable excess of grafting reagent. A large proportion of the silane passes through the process without reacting and needs to be removed at great expense by subsequent purification. This results in unnecessarily high consumption of chemicals and a rather resource-inefficient process. It is thus desired to be able to define desired grafting degrees with optimum grafting efficiency by means of suitable process control. In this study, the continuous grafting of vinyltrimethoxysilane (VTMS) on ethylene-octene copolymer (EOC) via reactive extrusion was investigated. Successful grafting was verified and quantified by 1H-NMR spectroscopy. The effects of five process parameters and their synergistic interactions on grafting degree and grafting efficiency were determined using a face-centered experimental design (FCD). Response surface methodology (RSM) was applied to derive a causal process model and define process windows yielding arbitrary grafting degrees between <2 and >5% at a minimum waste of grafting agent. It was found that the reactive extrusion process was strongly influenced by several second-order interaction effects making this process difficult to control. Grafting efficiencies between 75 and 80% can be realized as long as grafting degrees <2% are admitted.


Molecules ◽  
2014 ◽  
Vol 19 (12) ◽  
pp. 21066-21084 ◽  
Author(s):  
Anayansi Escalante-Aburto ◽  
Benjamín Ramírez-Wong ◽  
Patricia Torres-Chávez ◽  
Jaime López-Cervantes ◽  
Juan Figueroa-Cárdenas ◽  
...  

Author(s):  
Emmanuel K. Asare ◽  
Samuel Sefa-Dedeh ◽  
Emmanuel Ohene Afoakwa ◽  
Esther Sakyi-Dawson ◽  
Agnes S Budu

Studies were conducted to evaluate the effects of feed moisture and ingredient variations on the chemical composition and appearance of extruded sorghum-groundnut-cowpea blends using response surface methodology. Central composite rotatable design for k = 3 was used to study the combined effect of feed moisture (12 to 44 percent), groundnut concentration (zero to 10 percent) and cowpea level (zero to 20 percent) on the chemical composition and appearance of extruded ready-to-eat sorghum-legume blends in a single screw extruder. Product moisture, crude protein, crude fat, ash (minerals), crude fibre, carbohydrate and colour (L, a and b-values) were determined on the products using standard analytical methods. The results showed that irrespective of the feed moisture level, the extrusion process could reduce the product moisture to levels between six to 10 percent and low enough to extend the shelf life of the derived products. Increasing additions of cowpea and groundnut resulted in significant increases in protein, fat and ash (minerals - calcium, iron, and phosphorus) contents of the sorghum-legume extrudates. Increasing addition of cowpea decreased the redness of the sorghum extrudates, while no changes were noted with groundnut additions. Contrary, increasing groundnut addition generally increased the yellowness at all cowpea concentrations, while only minimal changes were noted with cowpea additions. The lightness of the sorghum extrudates decreased with increasing cowpea and groundnut concentrations, and this was more pronounced at higher cowpea concentrations and with increasing groundnut levels. The level of feed moisture showed no effect. Models developed for the indices gave R2-values ranging from 67.04 percent (for a-value) to 87.83 percent (for fat content), with insignificant lack of fits indicating the adequacy of the model in explaining the data. The optimal conditions likely to produce ready-to-eat puffed snack with enhanced nutritive value and appearance from sorghum-groundnut-cowpea blend extrudates was at low feed moisture (10 to 14 percent), cowpea level (18 to 20 percent) and groundnut level (six to eight percent).


Sign in / Sign up

Export Citation Format

Share Document