scholarly journals Microwave-mediated synthesis of silver nanoparticles on various metal-alginate composites: evaluation of catalytic activity and thermal stability of the composites in solvent-free acylation reaction of amine and alcohols

2020 ◽  
Vol 2 (2) ◽  
Author(s):  
Supriya ◽  
Ravikant Kaspate ◽  
Chandan Kumar Pal ◽  
Sonali Sengupta ◽  
Jayanta Kumar Basu
1994 ◽  
Vol 119 (2) ◽  
pp. 223-240 ◽  
Author(s):  
Hak Soo Kim ◽  
Chae Ho Shin ◽  
Guy Bugli ◽  
Monique Bureau-Tardy ◽  
Gerald Djega-Mariadassou

2020 ◽  
Author(s):  
O. S. Bezkrovnyi ◽  
P. Kraszkiewicz ◽  
W. Mista ◽  
L. Kepinski

Abstract The thermal stability of Au nanoparticles on ceria support of various morphology (nanocubes, nanooctahedra, and {111}-nanofacetted nanocubes) in oxidizing and reducing atmospheres was investigated by electron microscopy. A beneficial effect of the reconstruction of edges of ceria nanocubes into zigzagged {111}-nanofacetted structures on the inhibition of sintering of Au nanoparticles was shown. The influence of different morphology of Au particles on various ceria supports on the reducibility and catalytic activity in CO oxidation, and CO PROX of Au/ceria catalysts was also investigated and discussed. It was shown, that ceria nanocubes with flat {110} terminated edges are more suitable as a support for Au nanoparticles, used to catalyze CO oxidation, than zigzagged {111}- nanofacetted structures. Graphic Abstract


2018 ◽  
Vol 930 ◽  
pp. 224-229
Author(s):  
Marcos Antônio Guerra ◽  
Jeferson Prado Swerts ◽  
Mei Abe Funcia ◽  
Neide Aparecida Mariano ◽  
Maria Gabriela Nogueira Campos

Polyethylene terephthalate (PET) fiber is a very versatile fiber that can be produced with different properties, such as antimicrobial activity. This study aims to synthesize antimicrobial PET filaments incorporated with silver nanoparticles immobilized in silica (NPAg-Si) by bulk additive method. Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX) characterized the obtained filaments at concentrations (w/w) of 0.008%, 0.016%, 0.032%, 0.047% and 0.063% NPAg-Si, in order to identify the nanoparticles and analyze their dispersion in the polymeric matrix. Moreover, thermogravimetric analysis (TGA) was carry out to confirm the presence and concentration of the silver nanoparticles in the filaments as well as the thermal stability of the nanocomposites. The bulk addition method was efficient to produce PET-Silver filaments with silver nanoparticles homogeneously dispersed in the PET matrix.


2015 ◽  
Vol 15 (11) ◽  
pp. 8494-8501 ◽  
Author(s):  
Young Eun Jeong ◽  
Pullur Anil Kumar ◽  
Hee Lack Choi ◽  
Kwan-Young Lee ◽  
Heon Phil Ha

2011 ◽  
Vol 694 ◽  
pp. 73-78
Author(s):  
Dan Li

Hydrophobic silver nanoparticles have been carried out by use of ascorbic acid in cyclohexylamine and aqueous medium. Nanosilver can be effectively coated with oleic acid and possesses oil-soluble property. Oleic acid as an extractant is also effective at stabilizing particles of similar size in an oil phase when the AgNO3 is reduced in a coexisting aqueous phase. Stable spherical silver nanoparticles 15~25 nm in diameter with a well-crystallized structure were obtained at 120 °C. The thermal stability of surface-coated silver prepared in cyclohexylamine solution was monitored by UV-vis spectral analysis.


RSC Advances ◽  
2018 ◽  
Vol 8 (36) ◽  
pp. 20347-20352
Author(s):  
Akane Yamada ◽  
Kai Kamada ◽  
Taro Ueda ◽  
Takeo Hyodo ◽  
Yasuhiro Shimizu ◽  
...  

The present study reports the preferable effects of binding of lipase to titanate nanosheets. The binding largely enhanced biocatalytic activity and thermal stability of lipase especially at diluted concentrations.


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