Anodic oxidation of pitch-precursor carbon fibres in ammonium sulphate solutions: the effect of fibre surface treatment on composite mechanical properties

Composites ◽  
1991 ◽  
Vol 22 (5) ◽  
pp. 380-387 ◽  
Author(s):  
T.R. King ◽  
D.F. Adams ◽  
D.A. Buttry
1989 ◽  
Vol 170 ◽  
Author(s):  
D J Hodge ◽  
B A Middlemiss ◽  
J A Peacock

AbstractSurface energies of carbon fibres at different levels at surface treatment have been determined by a wetting force technique and related to fibre-matrix adhesion in carbon fibre reinforced PEEK composite. The effect of oxidative surface treatment on the surface free energy is detailed, along with the changes in surface oxygen and nitrogen content, as determined by X-ray photoelectron spectroscopy (XPS). The work of adhesion has been calculated for the carbon fibres and thermoplastic, which correlate well with experimental determination of interfacial strength. The technique can therefore be used to predict adhesion levels in fibre reinforced composites.


Polymers ◽  
2021 ◽  
Vol 13 (21) ◽  
pp. 3842
Author(s):  
Adnan Amjad ◽  
M. Shukur Zainol Abidin ◽  
Hassan Alshahrani ◽  
Aslina Anjang Ab Rahman

Natural fibre-based materials are gaining popularity in the composites industry, particularly for automotive structural and semi-structural applications, considering the growing interest and awareness towards sustainable product design. Surface treatment and nanofiller addition have become one of the most important aspects of improving natural fibre reinforced polymer composite performance. The novelty of this work is to examine the combined effect of fibre surface treatment with Alumina (Al2O3) and Magnesia (MgO) nanofillers on the mechanical (tensile, flexural, and impact) behaviour of biotex flax/PLA fibre reinforced epoxy hybrid nanocomposites. Al2O3 and MgO with a particle size of 50 nm were added in various weight proportions to the epoxy and flax/PLA fibre, and the composite laminates were formed using the vacuum bagging technique. The surface treatment of one set of fibres with a 5% NaOH solution was investigated for its effect on mechanical performance. The results indicate that the surface-treated reinforcement showed superior tensile, flexural, and impact properties compared to the untreated reinforcement. The addition of 3 wt. % nanofiller resulted in the best mechanical properties. SEM morphological images demonstrate various defects, including interfacial behaviour, fibre breakage, fibre pullout, voids, cracks, and agglomeration.


2017 ◽  
Vol 40 (S1) ◽  
pp. E214-E226 ◽  
Author(s):  
M.S. Salim ◽  
Dody Ariawan ◽  
M.F. Ahmad Rasyid ◽  
M.Z. Ahmad Thirmizir ◽  
R. Mat Taib ◽  
...  

Author(s):  
J Li

Polyacrylonitrile (PAN)-based carbon fibres were surface treated by ozone modification method and air-oxidation treatment. The interfacial properties of carbon fibre reinforced polyamide 6 (CF/PA6) composites were investigated by means of the single fibre pull-out tests. The surface characteristics of carbon fibres were characterized by X-ray photoelectron spectroscopy (XPS). As a result, it was found that interfacial shear strength values of the composites with ozone-treated carbon fibre are greatly increased. XPS results show that ozone treatment increases the amount of carboxyl groups on the carbon fibre surface, thus the interfacial adhesion between carbon fibre and PA6 matrix is effectively promoted. The effect of surface treatment of carbon fibres on the tribological properties of CF/PA6 composites was comparatively investigated. Experimental results revealed that surface treatment can effectively improve the interfacial adhesion between carbon fibre and PA6 matrix. Thus the wear resistance was significantly improved.


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