Determination of americium and curium by using ion-exchange in nitric acid-methanol medium for environmental analysis

Talanta ◽  
1976 ◽  
Vol 23 (11-12) ◽  
pp. 853-855 ◽  
Author(s):  
E Holm
1973 ◽  
Vol 56 (1) ◽  
pp. 213-218
Author(s):  
Edmond J Baratta ◽  
F E Knowles

Abstract A method for the determination of strontium-89 and strontium-90 in milk, involving ion exchange and purification with nitric acid, was evaluated by 11 collaborators. The accuracy of the method for strontium-89 ranged from 2 to 56% and the within-laboratory precision ranged from 11 to 76% for a concentration range of 68–480 pCi/L; values for strontium-90 in a concentration range of 50.2–116.2 pCi/L were 6.4 to 10 and 4 to 11%, respectively. The slight bias on the high side for strontium-90 was not considered serious. The collaborators had difficulty with strontium-89 analyses, as shown by the high precision and accuracy estimation values.


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