DEFORMATION OF ULTRA-HARD NITRIDE THIN FILMS STUDIED BY NANO-INDENTATION METHOD

Author(s):  
R. NOWAK ◽  
C.L. LI ◽  
T. SOGA ◽  
M. UMENO ◽  
S. MARUNO
2011 ◽  
Vol 284-286 ◽  
pp. 884-888
Author(s):  
Jun Du ◽  
Ping Zhang ◽  
Xiao Ying Zhu ◽  
Zhi Hai Cai

ZrAlN/Cu coating has been deposited onto Ti-6Al-4V substrates by reactive magnetron sputtering. The morphology of films was investigated by FESEM, the microstructure was studied by XRD, XPS and TEM. The plastic deformation characteristic of thin films were analysised from loading/unloading curves measured by nano-indentation method. Erosion tests were conducted to evaluate anti-erosion ability. Erosion rates were measured and characteristic damage features were identified on the surface of eroded specimens. The mechanisms of erosion are discussed in order to explain the promising performance of materials in erosive conditions. It was found that there is an significant increase of erosion resistance because of the increase of hardness and toughness.


2003 ◽  
Vol 108 (1-3) ◽  
pp. 20-27 ◽  
Author(s):  
Jong-Hoon Kim ◽  
Soon-Chang Yeon ◽  
Yun-Kwang Jeon ◽  
Jeong-Gil Kim ◽  
Yong-Hyup Kim

2009 ◽  
Vol 1239 ◽  
Author(s):  
Yong Sun ◽  
Zaiwang Huang ◽  
Xiaodong Li

AbstractA facile electrophoretic deposition method was successfully applied to achieve novel nanoclay-reinforced polyacrylamide nanocomposite thin films. A special curled architecture of the re-aggregated nanoclay-platelets was identified, providing a possible source for realizing the interlocking mechanism in the nanocomposites. The curled architecture could be the result from strain releasing when the thin films were peeled off from the substrates. Through micro-/nano-indentation and in situ observation of the deformation during tensile test with an atomic force microscope (AFM), the localized deformation mechanism of the synthesized materials was investigated in further details. The results implied that a localized crack diversion mechanism worked in the synthesized nanocomposite thin films, which resembled its nature counterpart-nacre. The deformation behavior and fracture mechanism were discussed with reference to lamellar structure, interfacial strength between the nanoclays and the polyacrylamide matrix, and nanoclay agglomeration.


2021 ◽  
Vol 736 ◽  
pp. 138906
Author(s):  
Zenglu Song ◽  
Xiao Tang ◽  
Xiang Chen ◽  
Tao Fu ◽  
Huanping Zheng ◽  
...  

2002 ◽  
Vol 750 ◽  
Author(s):  
Koichiro Hattori ◽  
Junhua Xu ◽  
Hidetoshi Nakano ◽  
Isao Kojima

ABSTRACTWe have evaluated the hardness and elastic properties of thin films by using a simple procedure to calibrate the tip shape effect of the nano-indentation data. For the simplification, a truncated-shape approximation and linear fit are used to estimate the tip-shape and contact stiffness, respectively, substituting for polynomial area-function and power-law fit. The parameters used in the correction were determined by a fused silica and a single crystal silicon (100) surface. Different film/substrate systems are designed in order to assess these fitted parameters used in the correction. The transition behavior observed from the film to the substrate is well coincide with the other film thickness results, where the indentation depth above 50nm.


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